Biaxial flexural strength of zirconia: A round robin test with 12 laboratories.

OBJECTIVE: The aim of this interlaboratory round robin test was to prove the robustness of the DIN EN ISO 6872:2019 and to identify the influence of processing and testing variations. METHODS: Each of the 12 laboratories participated (A-L) received 60 (n = 720) assigned zirconia specimens. All participants seperated the specimens from the blanks, sintered them, polished half of all specimens and performed the biaxial flexural test (DIN EN ISO 6872:2019). The surface roughness was determined by using tactile measuring device. Fractographic examination was performed under scanning-electron-microscopy (SEM). Data was analysed using Kolmogorov-Smirnov-, Kruskal-Wallis-, Mann-Whitney-U-test and two-parametric Weibull statistic (p < 0.05). RESULTS: The results for both preparation methods (as-fired and polished) showed significant differences for some participants. The values for as-fired groups ranged between 513 (I) and 659 (E) MPa. H showed higher Weibull modulus than C, E and I. Within polished groups flexural strengths values from 465 (L) to 1212 (E) MPa were observed, with a tendency to clustered groups A, I, J, L (465-689 MPa) and remaining groups (877-1212 MPa). E presented the highest and H the lowest Weibull modulus. Within A and J, no impact of the preparation method on flexural strength values was observed. Within L, as-fired specimens showed higher flexural strength than polished ones. The flexural strength increase did only associate to a certain extent with measured surface roughness. Fractography showed defect populations depending on polishing techniques, associated to the strength level, especially for polished groups. Reduced strength is related to machining defects, regardless of the surface state. SIGNIFICANCE: DIN EN ISO 6872:2019 can be seen as guidance to biaxial flexural strength testing but additional effort is necessary to ensure interlaboratory comparability. Calibrated furnaces and reliable sintering conditions are mandatory requirements together with detailed specifications on finishing or polishing procedures. Biaxial flexural testing is really a matter of understanding specimen preparation, alignment and mechanical testing by itself. DIN EN ISO 6872:2019 should further recommend reporting of mean surface roughness along with any biaxial flexural strength data. Fractography is a mandatory tool in interpretation and understanding of strength data.

The effect of different occlusal contact situations on peri-implant bone stress - A contact finite element analysis of indirect axial loading.

Implant restoration is one of the basic treatments in dentistry today, yet implant loss from occlusal overload is still a problem. Complex biomechanical problems such as occlusal overload are often analyzed by means of the finite element method. This numerical method makes it possible to analyze in detail the influence that different loading situations have upon implants and tissues, which is a key element in optimizing these dental procedures. This study was designed to investigate the stress distribution in peri-implant bone of a single-tooth implant crown using the finite element method. The load was applied indirectly via an occluding tooth through a three and five contact setup into the implant crown. The friction coefficient values between the crown and antagonist were varied between 0.1 and 1.0. Additionally, three crowns with cusp inclinations of 20°, 30° and 40° were modeled. Non-linear contact computations indicated that an increase in friction changed the direction and magnitude of contact forces, which also led to reduced stresses in the bone. Furthermore, the stress magnitudes were higher when cusps of a greater inclination were used. The intensity of stress alterations was strongly dependent on the distribution and number of contacts, and the contact force vector. In maximum intercuspation, a resulting axial load due to well-distributed contacts prevented high stresses in bone even with high cusp inclinations and low friction. Therefore for long-term clinical success, particular attention should be paid to occlusal adjustment so as to prevent oblique loading onto dental implant restorations.