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1.
Materials (Basel) ; 16(7)2023 Mar 23.
Article in English | MEDLINE | ID: mdl-37048840

ABSTRACT

Lesions of the articular cartilage are frequent in all age populations and lead to functional impairment. Multiple surgical techniques have failed to provide an effective method for cartilage repair. The aim of our research was to evaluate the effect of two different compression forces on three types of cartilage repair using finite element analysis (FEA). Initially, an in vivo study was performed on sheep. The in vivo study was prepared as following: Case 0-control group, without cartilage lesion; Case 1-cartilage lesion treated with macro-porous collagen implants; Case 2-cartilage lesion treated with collagen implants impregnated with bone marrow concentrate (BMC); Case 3-cartilage lesion treated with collagen implants impregnated with adipose-derived stem cells (ASC). Using the computed tomography (CT) data, virtual femur-cartilage-tibia joints were created for each Case. The study showed better results in bone changes when using porous collagen implants impregnated with BMC or ASC stem cells for the treatment of osseocartilaginous defects compared with untreated macro-porous implant. After 7 months postoperative, the presence of un-resorbed collagen influences the von Mises stress distribution, total deformation, and displacement on the Z axis. The BMC treatment was superior to ASC cells in bone tissue morphology, resembling the biomechanics of the control group in all FEA simulations.

2.
Polymers (Basel) ; 15(23)2023 Nov 30.
Article in English | MEDLINE | ID: mdl-38232028

ABSTRACT

Polyethylene terephthalate (PET) recycling is one of the most important environmental issues, assuring a cleaner environment and reducing the carbon footprint of technological products, taking into account the quantities used year by year. The recycling possibilities depend on the quality of the collected material and on the targeted product. Current research aims to increase recycling quantities by putting together recycled PET in an innovative way as a filler for the additive manufactured metallic lattice structure. Starting from the structures mentioned above, a new range of composite materials was created: IPC (interpenetrating phase composites), materials with a complex architecture in which a solid phase, the reinforcement, is uniquely combined with the other phase, heated to the temperature of melting. The lattice structure was modeled by the intersection of two rings using Solid Works, which generates the lattice structure, which was further produced by an additive manufacturing technique from 316L stainless steel. The compressive strength shows low values for recycled PET, of about 26 MPa, while the stainless-steel lattice structure has about 47 MPa. Recycled PET molding into the lattice structure increases its compressive strength at 53 MPa. The Young's moduli are influenced by the recycled PET reinforcement by an increase from about 1400 MPa for the bare lattice structure to about 1750 MPa for the reinforced structure. This sustains the idea that recycled PET improves the composite elastic behavior due to its superior Young's modulus of about 1570 MPa, acting synergically with the stainless-steel lattice structure. The morphology was investigated with SEM microscopy, revealing the binding ability of recycled PET to the 316L surface, assuring a coherent composite. The failure was also investigated using SEM microscopy, revealing that the microstructural unevenness may act as a local tensor, which promotes the interfacial failure within local de-laminations that weakens the composite, which finally breaks.

3.
J Prosthet Dent ; 128(3): 421-429, 2022 Sep.
Article in English | MEDLINE | ID: mdl-33610328

ABSTRACT

STATEMENT OF PROBLEM: The selective laser melting (SLM) process has become popular for the fabrication of frameworks for metal-ceramic restorations, although their surface roughness is greater than with cast or milled frameworks. Limited information is available regarding the surface mechanical characteristics of cobalt-chromium (Co-Cr) SLM-manufactured restorations. PURPOSE: The purpose of this in vitro study was to adapt the laser parameters for a remelting strategy, scanning the outer boundary of Co-Cr specimens, to reduce surface roughness and solidification defects, to determine microhardness, to investigate surface morphology and microstructure, and to establish surface mechanical characteristics. MATERIAL AND METHODS: Co-Cr specimens were SLM manufactured by using a typical melting (TM) strategy and an adaptive remelting (AR) strategy. The AR strategy involves rescanning 50% of the contour, varying the laser parameters. The roughness parameters considered were Ra and Rz. Vickers hardness was measured by microindentation with a 9.81-N force (ASTM E384-17). The surface morphology was investigated by scanning electron microscopy, the chemical composition by energy-dispersive X-ray spectroscopy, and the phase identification by using X-ray diffraction. The mechanical surface properties measured were the nanohardness, elastic modulus, and dissipation energy. One-way ANOVA with the Tukey procedure was used to compare the groups (α=.05). RESULTS: The innovative AR strategy reduced the surface roughness by 45% compared with TM, comparable with their cast counterpart. The smoothest AR surface was obtained by using 75 W and 350 mm/s for the first scanning of the contour, followed by a second remelting with 80 W and 700 mm/s. The microstructure of AR specimens had limited solidification defects, a chemical composition similar to that of raw powder, and a surface microhardness over 600 HV1. A fine grain structure in a single matrix phase was detected both on TM and AR specimens. The mechanical characteristics of the smoothest Co-Cr surface were 218 GPa elastic modulus, 746 HVIT Vickers nanohardness, 21 243 pJ plastic energy, and 26% nanoindentation work ratio. Significant differences were observed between the melting strategies (P<.05) both for surface roughness and microhardness. CONCLUSIONS: The laser scanning strategy affects both the surface roughness and the hardness of SLM-manufactured specimens. The results show that using the AR strategy and proper laser parameters can reduce the roughness and increase the surface hardness of Co-Cr specimens made of conventional powder feedstock.


Subject(s)
Chromium Alloys , Cobalt , Chromium , Chromium Alloys/chemistry , Cobalt/chemistry , Lasers , Materials Testing , Plastics , Powders , Surface Properties
4.
Materials (Basel) ; 13(18)2020 Sep 16.
Article in English | MEDLINE | ID: mdl-32948067

ABSTRACT

The demand of lattice structures for medical applications is increasing due to their ability to accelerate the osseointegration process, to reduce the implant weight and the stiffness. Selective laser melting (SLM) process offers the possibility to manufacture directly complex lattice applications, but there are a few studies that have focused on biocompatible Ti6Al7Nb alloy. The purpose of this work was to investigate the physical-mechanical properties and the microstructure of three dissimilar lattice structures that were SLM-manufactured by using Ti6Al7Nb powder. In particular, the strut morphology, the fracture characterization, the metallographic structure, and the X-ray phase identification were analyzed. Additionally, the Gibson-Ashby prediction model was adapted for each lattice topology, indicating the theoretical compressive strength and Young modulus. The resulted porosity of these lattice structures was approximately 56%, and the pore size ranged from 0.40 to 0.91 mm. Under quasi-static compression test, three failure modes were recorded. Compared to fully solid specimens, the actual lattice structures reduce the elastic modulus from 104 to 6-28 GPa. The struts surfaces were covered by a large amount of partial melted grains. Some solidification defects were recorded in struts structure. The fractographs revealed a brittle rupture of struts, and their microstructure was mainly α' martensite with columnar grains. The results demonstrate the suitability of manufacturing lattice structures made of Ti6Al7Nb powder having unique physical-mechanical properties which could meet the medical requirements.

5.
Materials (Basel) ; 13(4)2020 Feb 18.
Article in English | MEDLINE | ID: mdl-32085482

ABSTRACT

To manufacture custom medical parts or scaffolds with reduced defects and high mechanical characteristics, new research on optimizing the selective laser melting (SLM) parameters are needed. In this work, a biocompatible powder, 316L stainless steel, is characterized to understand the particle size, distribution, shape and flowability. Examination revealed that the 316L particles are smooth, nearly spherical, their mean diameter is 39.09 µm and just 10% of them hold a diameter less than 21.18 µm. SLM parameters under consideration include laser power up to 200 W, 250-1500 mm/s scanning speed, 80 µm hatch spacing, 35 µm layer thickness and a preheated platform. The effect of these on processability is evaluated. More than 100 samples are SLM-manufactured with different process parameters. The tensile results show that is possible to raise the ultimate tensile strength up to 840 MPa, adapting the SLM parameters for a stable processability, avoiding the technological defects caused by residual stress. Correlating with other recent studies on SLM technology, the tensile strength is 20% improved. To validate the SLM parameters and conditions established, complex bioengineering applications such as dental bridges and macro-porous grafts are SLM-processed, demonstrating the potential to manufacture medical products with increased mechanical resistance made of 316L.

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