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1.
Oper Dent ; 47(4): 461-472, 2022 Jul 01.
Article in English | MEDLINE | ID: mdl-35917240

ABSTRACT

This study investigated the fatigue failure load of simplified monolithic yttria partially stabilized zirconia polycrystal restorations cemented to a dentin-like substrate using different luting systems. Disc-shaped ceramic (Zenostar T, 10 mm Ø × 0.7 mm thick) and dentin-like substrate (10 mm Ø × 2.8 mm thick) were produced and randomly allocated into eight groups, without or with thermocycling (TC=5-55°C/12,000×): "cement" (RelyX Luting 2 - glass ionomer cement [Ion], [Ion/TC]; RelyX U200 - self-adhesive resin cement [Self], [Self/TC]; Single Bond Universal+RelyX Ultimate - MDP-containing adhesive + resin cement [MDPAD + RC], [MDP-AD + RC/TC]; ED Primer II+Panavia F 2.0 - Primer + MDP-containing resin cement [PR + MDP-RC], [PR + MDP-RC/TC])). Each luting system was used as recommended by the manufacturer. Staircase methodology (20 Hz; 250,000 cycles) was applied for obtaining the fatigue failure loads. Fractographic characteristics were also assessed. At baseline, the Ion group presented the lowest fatigue load, although it was statistically similar to the Self group. The resin-based cement systems presented the highest fatigue performance, with the Ion group being only statistically equal to the Self group. Thermocycling influenced the groups differently. After aging, the MDP-AD + RC presented the highest mean, followed by the PR + MDP-RC and Self groups, while the Ion group had the lowest mean. Fractographic analysis depicted all failures as radial cracks starting at the zirconia intaglio surface. The luting system with MDP-containing adhesive applied prior to the resin cement presented the highest fatigue failure load after aging, presenting the best predictability of stable performance. Despite this, monolithic zirconia presents high load-bearing capability regardless of the luting agent.


Subject(s)
Dental Bonding , Resin Cements , Ceramics/chemistry , Dental Cements/chemistry , Dental Cements/therapeutic use , Dental Materials , Dental Stress Analysis , Glass Ionomer Cements , Materials Testing , Resin Cements/chemistry , Resin Cements/therapeutic use , Surface Properties , Zirconium/chemistry
2.
Oper Dent ; 45(1): E21-E31, 2020.
Article in English | MEDLINE | ID: mdl-31794339

ABSTRACT

OBJECTIVE: To evaluate the effect of hydrofluoric acid (HF) etching and thermocycling (Tc) on fatigue failure load of feldspathic ceramic restorations cemented with two resin cements. METHODS: Disc-shaped feldspathic ceramic (Vitablocs Mark II; Ø=10 mm, 1.0-mm thick) and G10 epoxy resin (Ø=10 mm, 2.5-mm thick) specimens were made and randomly allocated considering three factors: ceramic etching (ie, with vs without 10% HF plus silane application), resin cement (ie, self-adhesive [RelyX U200; U200] or conventional [Multilink Automix; MA]), and Tc (ie, with vs without 5-55°C/12,000 cycles). Adhesive cementation followed each manufacturer's instructions. The fatigue test (n=20) was based on the staircase approach (250,000 cycles; 20 Hz). Contact angle, surface topography, and fractography analysis were also executed. Specific statistical tests were employed for each outcome (α=0.05). RESULTS: The interaction of HF and Tc factors decreased the fatigue resistance for both cements (U200 542.63>U200/HF-Tc 495.00; MA 544.47>MA/HF-Tc 506.84). Comparing the cements associated with HF or Tc, there was statistical superiority for MA (U200-Tc 537.37

Subject(s)
Ceramics , Dental Bonding , Acid Etching, Dental , Dental Porcelain , Dental Stress Analysis , Hydrofluoric Acid , Materials Testing , Resin Cements , Surface Properties
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