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Self-assembly of an organometallic Fe9O6 cluster from aerobic oxidation of (tmeda)Fe(CH2tBu)2.
Kephart, Jonathan A; Hecht, Zachary; Livesay, Brooke N; Bhowmick, Indrani; Shores, Matthew P; Popescu, V Codrina; Arulsamy, Navamoney; Hulley, Elliott B.
Chem Commun (Camb) ; 56(37): 4994-4997, 2020 May 07.
Article in English | MEDLINE | ID: mdl-32239066

ABSTRACT

Aerobic oxidation of (tmeda)Fe(CH2tBu)2 in toluene or THF solution leads to the self-assembly of a magic-sized all-ferrous oxide cluster containing the Fe9O6 subunit and bearing organometallic and diamine ligands. Mössbauer studies of the cluster are consistent with an all-ferrous assignment and magnetometry reveals complex intracluster and intercluster magnetic interactions.

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