Exploring differences in the physicochemical and nutritional properties of mango flours and starches.

Mangoes contain several components that are beneficial for health, in addition to being potential sources of starch for the food industry. However, a substantial amount of fruit is lost in the field because it does not meet commercial standards, resulting in food losses and environmental damage. Herein, the physicochemical properties of mango flours and starches obtained from different parts of the fruit of two cultivars were evaluated. Mango peel flours have higher levels of proteins, fibers, minerals, carotenoids, ascorbic acid, and antioxidant activity than pulp flours, in addition to a higher yellowing index and water and oil-holding capacity, and can be used as a functional flour. The pulp flours, with the higher starch content, showed characteristics that make them valuable as a potential ingredient in soft baking and gluten-free products. Mango starches have circular and oval shapes, with a bimodal distribution. All starches showed an A-type crystallinity pattern. Pulp starches showed a higher peak viscosity and breakdown, with a lower setback, and can be used as a thickening or gelling agent. The higher thermal stability of kernel starch suggests its application in sauces, baking, dairy products, and canned foods.

Unmodified cassava starches with high phosphorus content.

Our study was based on the fact that physiological changes in the plant resulting from the growth conditions alter the properties of the starch. An experimental trial was installed with cassava plants in poor phosphorus soil. A part of plants received phosphate fertilization at a level three times higher than the recommended dose, in order to provide high availability of phosphorus in the soil. The plants grew for two years and the starches were isolated at three times in the second vegetative cycle. The starches had A-type X-ray pattern. Starches isolated from cassava plants grown in soils with high phosphorus had increases of more than 100% in the content of bound phosphorus, which caused changes in the size of the granules, amylose, swelling power, solubility, pasting and thermal properties. These results indicate possibilities of increasing the commercial value of native cassava starch due to the expansion of use, considering the range of uses of phosphate starches for food and non-food purposes.

Preparation and properties of phosphate starches from tuberous roots.

The diversification of raw materials in the starch industries is a current strategy. However, the production of native starches does not meet market demand, and it is essential to expand the knowledge about chemical modifications in the same production line for different sources of starch. Phosphate starches are one of the most abundantly produced and widely used chemically modified starches. However, the effects of this modification may vary with the starch source and the reaction conditions. In this study, arrowroot, cassava and sweet potato starches were modified with sodium trimetaphosphate (STMP)/sodium tripolyphosphate (STPP) mixture under same conditions. The reaction time ranged from 7.5 to 120 min. Unmodified and modified starches were analyzed for phosphorus, amylose, morphology, X-ray diffraction pattern, crystallinity, swelling power, solubility, pasting and thermal properties. Phosphorus content linked to the starches increased with the reaction time, which affected the physicochemical properties of the three starches. The changes were more significant in all reaction times for cassava starch, followed by arrowroot. Due to its intrinsic characteristics, longer reaction times were necessary for more significant changes in sweet potato starch. Regardless of the starch source, as the reaction time increased, the average starch granule diameter, swelling power, solubility and peak viscosity increased. There was a decrease in setback in the longer reaction times for cassava and arrowroot starches. The changes in the reaction times allowed obtaining phosphate tuberous starches with different properties which can meet the demands of the food and non-food industries.

Orange-fleshed Sweet Potato Chips: Processing Effect on Carotenoid Content and Resistant Starch and Sensory Acceptance

HIGHLIGHTS Chips from orange-fleshed sweet potato have a good acceptability. Drying process showed retention of carotenoids total content. Chips from drying or frying process showed high resistant starch content.

Abstract There is currently a great demand for industrialized products with functional properties, together with the increase in consumption of roots and sweet potato products. Sweet potatoes have a high content of resistant starch, while only the orange-fleshed roots also have a high content of carotenoids. Due to these, this work aimed to produce orange-fleshed sweet potato chips, by two processes: drying oven and immersion frying. The chips were evaluated for the content of resistant starch and carotenoids in nature and chips sweet potatoes, and evaluations of the physical attributes and sensory analysis of the chips. The drying process retained a greater content of total carotenoids. Fried chips can be considered high resistant starch content, even with a decrease in the content after this processing; they also showed more intense coloring and pleasant texture. There was a statistical difference between the varieties only regarding the content of carotenoids and resistant starch. Thereby, it can be concluded that the chips of both processing have good technological and functional qualities, and that the frying process presented best hardness which led to greater acceptability and purchase intention.

Banana fruits with high content of resistant starch: Effect of genotypes and phosphorus fertilization.

Banana fertilization practices aim to increase agricultural yield and the effects of these practices on fruit components have not been well explored. This study aimed to evaluate the effects of phosphate fertilizer levels on production parameters and accumulation of dry matter, phosphorus, starch and resistant starch in green fruits. Four banana genotypes were cultivated under the same cultural practices, with varying levels of phosphate fertilizers during three production cycles. Bunches were harvested and evaluated for total fruit mass, average finger mass and yield. Fresh green fruit pulps were analyzed for dry matter, phosphorus, starch and resistant starch content. The results showed that the effects of phosphate fertilizer were genotype dependent and that the increase of P2O5 rates applied in banana fertilization promoted an increase in fruit production with higher levels of phosphorus, starch and resistant starch.

Gelatinized sweet potato starches obtained at different preheating temperatures in a spray dryer.

Native sweet potato starch was gelatinized at temperatures between 57 and 69 °C and then spray dried, to verify the changes caused by this process. The spray dried starch granules initially swelled with the increase in preheating temperature, displaying a larger diameter, but shrank upon colling. There was an increase in the gelatinization temperature and a decrease in the enthalpy change of the spray dried starches relative to those of native starch. Spray dried starch preheating at 69 °C showed highly reduced enthalpy change (80%) and relative crystallinity. Based on the parameters studied, the best preheating temperature was 67 °C. Under this condition, the starch can be applied in more viscous products that require a greater thickness, and with great process yield (65%). This study showed the feasibility of the application of this process to produce sweet potato starches with specific properties for different purposes in the food and non-food industries.

Harvest time optimization leads to the production of native cassava starches with different properties.

The starch market is very diverse and demanding regarding the functional characteristics of the product. However, no technique based on the management of cassava root harvest time has been applied to obtain starches with different properties. Thus, in this study, cassava roots were harvested at different times and the structure and physicochemical properties of their starches were analyzed. Results indicated the time points in the first growth cycle of plants when all parameters associated with root growth were at their highest values. It was also observed that changes in the time of harvest leads to the production of starches with different granule size, crystallinity, and content of amylose and phosphorus, which resulted in changes in the thermal and pasting properties, as well as in the solubility of the starches and swelling power; that is, on the main determinant characteristics for applicability of the starches. Planned agricultural production monitoring, coupled with the analysis of the main starches characteristics for large-scale cassava crops, can provide commercial benefits for both farmers and industry, as it is possible to obtain starches with desired physicochemical characteristics for varied applications.

Effect of spray-drying and extrusion on physicochemical characteristics of sweet potato starch.

This study aimed to understand the physicochemical characteristics of sweet potato starch following spray-drying and extrusion processes for desirable applications. Spray-dried starch showed formation of agglomerates and decreased in average granular size from 16.5 µm of the native starch granules to 14.1 µm. Spray-drying reduced the percentage crystallinity from 25.3 to 22.6% and showed a slight decrease in the molecular weight of amylopectin from 3.1 to 2.6 × 108 g mol-1. In addition, changes in the pasting and gelatinization properties, higher final viscosity (454.4 RVU), and less enthalpy change (8.73 J g-1) were reported after spray-drying. Thus, spray-drying resulted in partially gelatinized starch, which can be selected for making more viscous products. Extruded sweet potato starch displayed an amorphous structure, showed total loss of crystallinity, and significant reduction in molecular weight of amylopectin to 0.41 × 108 g mol-1, reflecting complete gelatinization of starch granules during extrusion. Extruded starch showed significant changes in pasting properties, including a display cold viscosity (9.4 RVU). Therefore, extruded starch was suitable for products that require quick solubility and a low final viscosity. Thus, the spray-drying and extrusion processes produce sweet potato starches with particular characteristics that can be used for different and potential applications in industries.

Phosphate fertilization changes the characteristics of 'Maçã' banana starch.

The unripe banana has been studied as a potential source of starch for use in various applications. Considering the importance of phosphorus in the biosynthesis of the starch and also the interference of this mineral in starch properties, in this study it was evaluated the effect of rates of phosphate fertilizer applied in the cultivation of 'Maçã' banana on the characteristics of the starch. Starches extracted from fruits from different treatments were analyzed for morphological characteristics, X-ray diffraction pattern, relative crystallinity, granule size, amylose, resistant starch and phosphorus levels, as well as, for pasting and thermal properties. Results showed that the phosphate fertilization has interference on the characteristics of the banana starch led to increase of phosphorus content and size of the granules, reduction of crystallinity and resistant starch content, decrease of viscosity peak, breakdown, final viscosity, setback, transitions temperatures and enthalpy. These changes caused by phosphate fertilizer conditions can be increase the applications of the 'Maçã' banana starch.

Chemical composition of potato tubers: the effect of cultivars and growth conditions.

The aim of the study involved evaluating the chemical composition of tubers of five potato cultivars that were grown under the same cultural practices in soils with low, medium, and high availability of phosphorus. The experimental designs corresponded to a randomized block with four replicates. Tuber samples were analyzed in terms of moisture, ash, protein, lipid, total sugar, fiber, starch, and phosphorus contents. The results suggested that increased availability of phosphorus in soil allowed the production of tubers with higher dry matter content, lower total sugar content, and a higher percentage of starch and protein. Hence, the aforementioned parameters constitute important factors corresponding to the nutritional and industrial quality of potatoes. Increased phosphorus availability in soil can promote significant changes in the composition of potato tubers, and thereby in potential uses of tubers.

Cassava derivatives in ice cream formulations: effects on physicochemical, physical and sensory properties.

In the present study, the effects of derivatives of cassava, maltodextrin and bagasse, on the physicochemical, physical and sensory properties of ice creams were investigated. The content of cassava maltodextrin increased significantly the content of carbohydrate and total soluble solids and decreased lipids content. The effect of cassava bagasse was more pronounced than the maltodextrin on physical and sensory parameters. Increased percentage of cassava bagasse in formulation led to decrease of overrun, melting and luminosity, but increased hardness and unfreezable water. Sensory attributes were mainly influenced by cassava bagasse inclusion. The results suggested the potential use of cassava derivatives in ice cream formulations. Ice creams with low percentage of cassava bagasse (1.5) and intermediate values of cassava maltodextrin (3.65%) had good nutritional, technological and sensorial acceptance.

Characterization of banana starches obtained from cultivars grown in Brazil.

The starch market is constantly evolving and studies that provide information about the physical and rheological properties of native starches to meet the diverse demands of the sector are increasingly necessary. In this study starches obtained from five cultivars of banana were analyzed for size and shape of granules, crystallinity, chemical composition, resistant starch, swelling power, solubility, thermal and paste properties. The granules of starch were large (36.58-47.24µm), oval, showed crystallinity pattern type B and the index of crystallinity ranged from 31.94 to 34.06%. The phosphorus content ranged from 0.003 to 0.011%, the amylose ranged from 25.13 to 29.01% and the resistant starch ranged from 65.70 to 80.28%. The starches showed high peak viscosity and breakdown, especially those obtained from 'Nanicão' and 'Grand Naine'. Peak temperature of gelatinization was around 71°C, the enthalpy change (ΔH) ranged from 9.45 to 14.73Jg(-1). The starch from 'Grand Naine' showed higher swelling power (15.19gg(-1)) and the starch from 'Prata-Anã' higher solubility (11.61%). The starches studied are highlighted by their physical and chemical characteristics and may be used in several applications.

Instant blend from cassava derivatives produced by extrusion / Mistura instantânea de derivados de mandioca produzida por extrusão

ABSTRACT: The current research aimed to evaluate the effects of extrusion parameters on the physical characteristics of extruded blends of cassava leaf flour and starch. A factorial central composite design with four independent variables and the response surface methodology were used to evaluate the results of color parameters (L*, a*, b*), water absorption index, water solubility index and paste properties, according to the variations in the leaf flour percentage (1.5 to 7.5%), extrusion temperature (60 to 100ºC), screw speed (175 to 231rpm) and moisture (20 to 30%). Extrusion conditions affect color, water absorption and water solubility indexes and paste properties of blends. The intermediate tested conditions of variable parameters lead to obtain extruded products with higher cold viscosity and water absorption index and light color, desirable qualities for rapid preparation products.

RESUMO: Este trabalho teve por objetivo avaliar os efeitos dos parâmetros de extrusão sobre as características físicas de misturas extrusadas de farinha de folhas de mandioca e amido. O delineamento central composto rotacional, com quatro variáveis independentes, e a metodologia de superfície de resposta foram utilizados para avaliar os resultados dos parâmetros de cor (L*, a*, b*), índice de absorção de água, índice de solubilidade em água e propriedades de pasta, de acordo com as variações da percentagem de farinha de folha (1,5 a 7,5%), da temperatura de extrusão (60 a 100ºC), da rotação da rosca (175-231rpm) e da umidade (20 a 30%). As condições do processo de extrusão afetaram a cor, os índices de absorção de água e solubilidade em água e as propriedades de pasta das misturas. As intermediárias testadas dos parâmetros variáveis levaram à obtenção de produtos extrusados com maior viscosidade fria e índice de absorção de água e de cor clara, qualidades desejáveis para produtos de preparação rápida.

Nitrogênio no crescimento da planta e na qualidade de raízes da mandioquinha-salsa / Nitrogen on plant growth and storage root quality of Arracacha

RESUMO: O nitrogênio (N) é o segundo nutriente mais absorvido pela mandioquinha-salsa. No entanto, ainda existem dúvidas sobre a influência que esse nutriente pode exercer sobre o crescimento da planta e a qualidade das raízes de reserva. Assim, objetivou-se com este trabalho avaliar a influência da adubação nitrogenada no crescimento da planta e na qualidade físico-química e nutricional das raízes de mandioquinha-salsa. O experimento foi conduzido em um Latossolo Vermelho distrófico de textura arenosa, no delineamento experimental de blocos ao acaso, com quatro repetições. Os tratamentos foram constituídos pelas doses de 0, 50, 100 e 200kg ha-1 de N. O crescimento das partes vegetativas da planta de mandioquinha-salsa aumentou linearmente com a adubação nitrogenada, mas a massa média e a produtividade das raízes de reserva aumentaram até as doses estimadas de 121 e 148kg ha-1 de N, respectivamente. A adubação nitrogenada aumentou os teores de amido e de proteína das raízes e diminuiu os teores de açúcares totais, porém, sem influenciar a qualidade nutricional delas.

ABSTRACT: Nitrogen (N) is the second most absorbed nutrient by Arracacha. However, there are still doubts about the influence that this nutrient can have on plant growth and the quality of the storage roots. Thus, the aim of this research was to evaluate the influence of nitrogen fertilization on plant growth and physical-chemical and nutritional quality of storage roots of Arracacha. The experiment was conducted on an Oxisol of sandy texture, in a randomized complete block design, with four replications. The treatments consisted of rates of 0, 50, 100, and 200kg ha-1 N. Growth of vegetative parts of Arracacha increased linearly with nitrogen fertilization, but the storage root mean weight and the yield of storage roots increased up to estimated rates of 121 and 148kg ha-1 N, respectively. Nitrogen fertilization increased the starch and protein content of the storage roots and reduced the content of total sugar, but without affecting the nutritional quality of the same.

Crystallinity, thermal and pasting properties of starches from different potato cultivars grown in Brazil.

Starches from different potato cultivars were characterized as amylose and phosphorus content, crystallinity, thermal and paste properties. Statistical analysis of amylose content showed difference between starches samples and the cultivars Asterix and BRS Clara showed higher contents than others. Phosphorus content ranged from 633 to 966.7 mg kg(-1). The X-ray diffraction analysis showed that the crystallization of potato starches can be classified as B-type X-ray pattern, presenting crystallinity index ranging from 20.02% to 21.59%. Regarding thermal properties, the onset temperature did not show statistical difference between starch samples, in gelatinization and retrogradation analysis. As expected there was a significant decrease in peak temperature and enthalpy after the retrogradation of starches. For the pasting properties results showed significant difference in all cultivars. Pearson correlation coefficients showed that amylose content was negatively correlated to the onset, peak and final temperature of gelatinization, final temperature of retrogradation and pasting temperature. Phosphorus content was positively correlated to crystallinity index, peak viscosity and breakdown. Starches extracted from potato varieties showed different characteristics which can be useful to food and related industries that make use of potato starch, allowing wide options of use in various sectors of industrial application in Brazil.

Physico-chemical properties of starches isolated from potato cultivars grown in soils with different phosphorus availability.

BACKGROUND: Starch is the major component of potato tubers, amounting approximately to 150-200 g kg (-1) of the tuber weight. Starch is considered to be a major factor for the functionality of the potato in food applications. This study evaluated the physical characteristics of potato starches isolated from tubers of different potato cultivars grown in soil with three levels of phosphorus (P) availability. All potatoes were growing according the same method. The starches were isolated by physical methods and the samples were analyzed for the amylose, P content, paste properties (RVA) and thermal properties of gelatinization and retrogradation (DSC). Experimental data were analyzed considering the potato cultivars and the three soil P availability. RESULTS: For all measured parameters significant impact of cultivar and soil P availability was determined. Phosphorus contents in potato starches ranged from 0.252 to 0.647 g kg(-1) and amylose from 27.18 to 30.8%. Starches from different potato cultivars independent of soil showed a small range of gelatinization temperature. All starches showed low resistance heating and shear stress. CONCLUSION: The results showed the influence of growing conditions (soil P availability) and also of the differences between the potato cultivars on important characteristics of applicability of starches.

Physical characteristics of potato flour from 'Ibituaçú' cv. under different extrusion parameters / Características físicas de farinha de batata cv 'Ibituaçú' submetida a diferentes parâmetros de extrusão

ABSTRACT:This study aimed to evaluate potato flour from 'Ibituaçú' cultivar as raw material for extrudates. Potato flour was processed in a single-screw extruder following central composite rotational design for three factors, being considered as independent parameters: temperature in the third zone, humidity and screw speed. The products obtained were characterized by expansion index (EI), specific volume (SV), water solubility index (WSI), water absorption index (WAI), hardness (H), color (L*, a* and b*). Results showed an effect of the independent parameters on the extruded physical characteristics. The parameters varied from: 3.22 to 5.47 (EI); 2.08 to 11.23 mL g-1(SV), 32.88 to 63.72% (WSI), 4.02 to 8.97 g gel g-1(WAI), 7.54 to 29.85 kgf (H), 53.89 to 68.72 (L*), 5.59 to 6.92 (a*), 16.6 to 22.6 (b*). It was concluded that expanded products with desired physical characteristics are obtained at high temperature; low humidity and intermediate screw speed.

RESUMO:O objetivo deste trabalho foi avaliar a farinha de batata cultivar 'Ibituaçu' como matéria prima para o desenvolvimento de produtos extrusados. A farinha de batata foi processada em extrusor mono-rosca seguindo delineamento central composto rotacional para três fatores, sendo considerados como variáveis independentes a temperatura na 3ª zona, a umidade e a rotação da rosca. Os produtos obtidos foram caracterizados quanto ao índice de expansão (IE), volume específico (VE), índice de solubilidade em água (ISA), índice de absorção de água (IAA), dureza (D) e cor (L*, a* e b*). Os resultados mostraram efeito das variáveis independentes sobre as características físicas dos produtos. O IE dos produtos variou de 3,22 a 5,47, o VE de 2,08 e 11,23mL.g-1, o ISA de 32,88 a 63,72%, o IAA de 4,02 a 8,97 g gel.g-1, D de 7,54 a 29,85kgf, L* de 53,89 a 68,72, a* de 5,59 a 6,92, b* de 16,6 a 22,6. Nas condições de elevada temperatura, baixa umidade, e rotação da rosca intermediária são obtidos produtos extrusados com características físicas desejadas para produtos expandidos.

Potencialidade de processamento industrial de cultivares de batatas / Industrial processing potential of potato cultivars

A industrialização da batata tem sido limitada no Brasil, devido à falta de matéria-prima adequada, sendo a demanda suprida pelas importações de produtos processados. Oito cultivares de batata, adaptadas às condições da região serrana de Minas Gerais, safra 2011, foram avaliadas quanto a sua composição centesimal, cor e conteúdo de amilose. Os resultados obtidos mostraram que as cultivares 'Marcy' e 'Colorado' apresentam características importantes para o cozimento. As cultivares 'Marlen' e 'Pirassu' apresentam atributos requeridos para o processamento na forma de chips e/ou palha e a cultivar 'BRS Ana' para a forma de palitos pré-fritos.

The industrialization of potato in Brazil has been limited because of the low availability of tubers with adequate quality, being supplied by imports of processed products demand. Eight cultivars of potato, adapted to the mountainous conditions of Minas Gerais state, harvest of 2011, were evaluated for their centesimal composition, color and amylose content.The results demonstrated that 'Marcy' and 'Colorado' cultivars showed important characteristic for cooking. The 'Marlen' and 'Pirassu' cultivars showed required attributes for processing in the form of chips or straw and the cultivar 'BRS Ana' for pre-fried sticks.

Características físicas, reológicas e sensorial de produtos extrusados de misturas de farinha de maracujá e fécula de mandioca / Physical, rheological and sensory characteristics of extruded products from mixtures of passion fruit flour and cassava starch

Este trabalho teve por objetivo avaliar o efeito da temperatura de extrusão e da rotação da rosca sobre as propriedades físicas, reológicas e sensoriais de snacks de mandioca e maracujá produzidos em extrusor mono-rosca. Foi utilizado o delineamento central composto rotacional, com 11 tratamentos, considerando como variáveis dependentes: índice de expansão (IE), volume específico (VE), índice de solubilidade em água (ISA), índice de absorção em água (IAA), cor (L*, a*, b*) e propriedades de pasta (RVA). Os produtos foram aromatizados e analisados para a aceitação global. Os resultados obtidos demonstraram efeitos significativos da temperatura e da rotação sobre as propriedades estudadas e boa aceitação dos produtos sabor chocolate.

This research had as objective to evaluate the effect of extrusion temperature and screw speed on physical and rheological properties, as well as, the sensory acceptance of cassava and passion fruit snacks produced in single-screw extruder. A central composite design with 11 treatments was used, considering as dependent variables: expansion index (EI), specific volume (SV), water solubility index (WSI), water absorption index (WAI), color (L*, a*, b*) and pasting properties (RVA). The products were flavored and analyzed for global acceptance. The results showed significant effects of temperature and screw speed on the dependent variables. The chocolate flavored snacks obtained good acceptance.