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Int J Biol Macromol ; 263(Pt 1): 130286, 2024 Apr.
Article in English | MEDLINE | ID: mdl-38382795

ABSTRACT

This study evaluated the physicochemical and antioxidant properties of clove essential oil (0, 0.2, 0.4, 0.6, 0.8, 1.0 % v/v) nanoemulsion (CEON) loaded chitosan-based films. With the increasing concentrations of the CEON, the thickness, b* and ΔE values of the films increased significantly (P < 0.05), while L* and light transmission dropped noticeably (P < 0.05). The hydrogen bonds formed between the CEON and chitosan could be demonstrated through Fourier-transform infrared spectra, indicating their good compatibility and intermolecular interactions. Furthermore, the added CEON considerably reduced the crystallinity and resulted in a porous structure of the films, as observed through X-ray diffraction plots and scanning electron microscopy images, respectively. This eventually led to a drop in both tensile strength and moisture content of the films. Moreover, the antioxidant properties were significantly enhanced (P < 0.05) with the increase in the amount of clove essential oil (CEO) due to the encapsulation of CEO by the nanoemulsion. Films containing 0.6 % CEO had higher elongation at break, higher water contact angle, lower water solubility, lower water vapor permeability, and lower oxygen permeability than the other films; therefore, such films are promising for application in meat preservation.


Subject(s)
Chitosan , Oils, Volatile , Syzygium , Chitosan/chemistry , Oils, Volatile/pharmacology , Clove Oil/pharmacology , Antioxidants/pharmacology , Antioxidants/chemistry , Syzygium/chemistry , Spectroscopy, Fourier Transform Infrared , Permeability , Food Packaging/methods , Steam
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