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1.
Heliyon ; 10(13): e33967, 2024 Jul 15.
Article in English | MEDLINE | ID: mdl-39071718

ABSTRACT

Magnesium, valued for its lightweight, recyclability, and biocompatibility, faces challenges like its poor wear behavior and mechanical properties that limit its adaptation for a multitude of applications. In this study, various statistical analyses, and machine learning (ML) techniques were employed to optimize equal channel angular pressing (ECAP) process parameters for improving the wear behavior of Mg-3wt.% Zn-0.7 wt% Ca alloy. ECAP was conducted up to four passes via route Bc at 250 °C. Wear testing of both as-annealed (AA) and ECAP-processed alloys was performed using the dry ball-on-flat wear method under varying loads, speeds, and time. One pass (1P) and 4Bc-ECAP resulted in a notable uniform grain refinement of 86 % and 91 %, respectively, compared to the AA. X-ray diffraction (XRD) analysis confirmed a refined structure attributed to extensive dynamic recrystallization. Mechanical wear testing revealed a significant reduction in volume loss (VL), up to 56 % and 28.5 % after 1P and 4Bc samples, respectively, compared to the AA sample, supported by the observed texture intensity. The coefficient of friction (COF) stabilizes at 0.30-0.45, indicating low friction characteristics. Next, by adjusting wear load and speed through design of experiments (DOE), the wear output responses, VL and COF, were experimentally investigated. The output responses were predicted in the second step using ML, 3D response surface plots, and statistical analysis of variance (ANOVA). According to the regression model, the minimal VL was attained at a 5 N applied load. Also, the wear speed and VL at different passes are inversely proportional. On the other hand, the optimal COF was obtained at applied load about 2-3 N and 250 mm/s at different passes. The wear process variables were then optimized using different optimization techniques namely, genetic algorithm (GA), hybrid DOE-GA, and multi-objective genetic algorithm (MOGA) approaches.

2.
ACS Biomater Sci Eng ; 10(6): 3718-3726, 2024 06 10.
Article in English | MEDLINE | ID: mdl-38716490

ABSTRACT

The performance of dental resin composites is crucially influenced by the sizes and distributions of inorganic fillers. Despite the investigation of a variety of functional particles, glass fillers and nanoscale silica are still the predominant types in dental materials. However, achieving an overall improvement in the performance of resin composites through the optimization of their formulations remains a challenge. This work introduced a "dense" microhybrid filler system with 85 wt % filler loading, leading to the preparation of self-developed resin composites (SRCs). Comparative evaluations of these five SRCs against four commercial products were performed, including mechanical property, polymerization conversion, and shrinkage, along with water sorption and solubility and wear resistance. The results showed that among all SRC groups, SRC3 demonstrated superior mechanical performance, high polymerization conversion, reduced shrinkage, low water absorption and solubility, and acceptable wear resistance. In contrast to commercial products, this optimal SRC3 material was comparable to Z350 XT in flexural and diametral tensile strength and better in flexural modulus and surface hardness. The use of a "dense" microhybrid filler system in the development of resin composites provides a balance between physicochemical property and wear resistance, which may be a promising strategy for the development of composite products.


Subject(s)
Composite Resins , Materials Testing , Composite Resins/chemistry , Solubility , Tensile Strength , Dental Materials/chemistry , Polymerization , Polyurethanes/chemistry , Surface Properties , Hardness , Acrylic Resins/chemistry
3.
Materials (Basel) ; 17(7)2024 Mar 28.
Article in English | MEDLINE | ID: mdl-38612061

ABSTRACT

In recent decades, batch hot-dip galvanized (HDG) steel has proven itself in practical applications due to the good corrosion resistance of its components. Despite the importance of the mechanical-load-bearing capacity of these coatings, the wear behavior has, so far, only been investigated very sporadically and not systematically, so a quantification of the wear behavior and statements on the mechanisms are vague. Therefore, two body wear tests with bonded abrasive grain were carried out. Varying the friction rolls, load, and total number of cycles, the wear behavior was investigated. The mass loss and the layer thickness reduction were measured at different intervals. After the test, the microstructure in the cross-section and the hardness according to Vickers (0.01 HV) were evaluated. The results showed that the wear behavior of HDG coatings against abrasive loads can be characterized with the selected test conditions. Initially, the applied load removed the soft η-phase. As the total number of cycles increases, the η- and ζ-phases deform plastically, resulting in a lower mass reduction compared to that expected from the measured layer thickness. The characteristic structure of a batch HDG coating with hard intermetallic Zn-Fe phases and an outer pure zinc phase has demonstrated effective resistance to abrasion.

4.
Materials (Basel) ; 17(1)2024 Jan 04.
Article in English | MEDLINE | ID: mdl-38204116

ABSTRACT

In this paper, Ni60/WC wear-resistant coatings have been created on the Ti6Al4V substrate surface using a pre-layered powder laser cladding method by deploying various scanning speeds of 8, 10, 12, and 14 mm/s. The coatings are characterized through X-ray diffraction (XRD), scanning electron microscopy (SEM), and a high-speed reciprocating fatigue wear tester. It is found that the phase composition of the coating comprises the synthesized, hard phase TiC and TiB2, the silicides WSi2 and W5Si3, and NiTi and γ-Ni solid solutions. At different scanning speeds, there is a metallurgical fusion line in the bonding area of the fused cladding layer, indicating a good metallurgical bonding between the substrate and the powder. At a low scanning speed, the coating develops into coarse dendrites, which shows significant improvement with scanning speed. The microhardness first increases and then decreases with the scanning speed, and the coating's average microhardness was 2.75-3.13 times higher than that of the substrate. The amount of mass wear has been reduced by 60.1-79.7% compared to the substrate. The wear behavior of the coatings was studied through detailed analysis of wear surfaces' microstructures and the amount of wear to identify the optimum scanning speed.

5.
Materials (Basel) ; 16(21)2023 Oct 24.
Article in English | MEDLINE | ID: mdl-37959436

ABSTRACT

The wear of enamel and crown restorative materials often occur by occlusion. The purpose of this study was to evaluate the wear volume between glass-ceramics used for CAD/CAM blocks (lithium disilicate: Initial LiSi block (LIS), IPS e.max CAD (IPS), zirconia-reinforced lithium silicate glass-ceramics: Celtra DUO (DUO), VITA Suprinity (VITS) and feldspar-based glass-ceramics: Vitablocs Mark II (MAK)) and bovine tooth enamel using a two-body wear test, the hardness, three-point bending strength, micro-structure and the element components of glass-ceramics. The data were analyzed using a one-way analysis of variance and Tukey's multiple comparison test (α = 0.05). IPS and DUO with relatively large size crystal gain had significantly larger abrader wear volumes. Zirconia-reinforced lithium silicate glass-ceramics (DUO, VITS) caused significantly greater wear volume in antagonist enamel. MAK with scale-shape crystals grains produced distinct scratches after wear tests, both in the material itself and in the enamel. A strong correlation between the mechanical properties (hardness, three-point bending strength) and wear volume could not be confirmed. The type of glass-ceramic, size, and shape of the crystal grains affected the wear behavior of the glass-ceramics for CAD/CAM blocks. Therefore, dentists should consider that wear behavior varies with crystal structure, size, and shape in glass-ceramics for CAD/CAM blocks.

6.
Int J Comput Dent ; 0(0): 0, 2023 Oct 12.
Article in English | MEDLINE | ID: mdl-37823541

ABSTRACT

AIM: The adjustment and transfer of a stable occlusion can be a major challenge in prosthetic rehabilitations. The aim of this study was to assess a non-invasive treatment option for complex prosthetic rehabilitations and occlusal analyses using 3D-printed restorations clinically. MATERIALS AND METHODS: Eleven patients received a partial or complete rehabilitation with the aid of 3D-printed restorations (n=171). After 12 months of clinical service, all restorations were analyzed using the United States Public Health Service (USPHS) criteria. RESULTS: The 12-month clinical data revealed that 3D-printed restorations showed a survival rate of 84.4%. Complications occurred mostly regarding the anatomical form (7%) or marginal integrity (6AC%) and were consequently rated "Charlie" or "Delta." Color stability and color match of 3D-printed restorations were rated "Alpha" in 83% and 73%, respectively, of all restorations. Marginal inflammation was rated "Alpha" in 89% of all restorations. An excellent surface texture and no secondary caries or postoperative sensitivities (100%) were observed. CONCLUSIONS: 3D-printed restorations might be an alternative treatment option for initiating complex prosthetic rehabilitations. Technical complications rarely occurred. Biological complications did not occur at all. The color stability showed promising results after 12 months of clinical service. However, the results should be interpreted with caution. Long-term results with a high number of restorations should be awaited.

7.
Materials (Basel) ; 16(5)2023 Feb 26.
Article in English | MEDLINE | ID: mdl-36903058

ABSTRACT

In this study, a newly developed high-strength cast Fe81Cr15V3C1 (wt%) steel with a high resistance against dry abrasion and chloride-induced pitting corrosion is presented. The alloy was synthesized through a special casting process that yielded high solidification rates. The resulting fine, multiphase microstructure is composed of martensite, retained austenite and a network of complex carbides. This led to a very high compressive strength (>3800 MPa) and tensile strength (>1200 MPa) in the as-cast state. Furthermore, a significantly higher abrasive wear resistance in comparison to the conventional X90CrMoV18 tool steel was determined for the novel alloy under very harsh wear conditions (SiC, α-Al2O3). Regarding the tooling application, corrosion tests were conducted in a 3.5 wt.% NaCl solution. Potentiodynamic polarization curves demonstrated a similar behavior during the long-term testing of Fe81Cr15V3C1 and the X90CrMoV18 reference tool steel, though both steels revealed a different nature of corrosion degradation. The novel steel is less susceptible to local degradation, especially pitting, due to the formation of several phases that led to the development of a less dangerous form of destruction: galvanic corrosion. In conclusion, this novel cast steel offers a cost- and resource-efficient alternative to conventionally wrought cold-work steels, which are usually required for high-performance tools under highly abrasive as well as corrosive conditions.

8.
J Dent ; 130: 104450, 2023 03.
Article in English | MEDLINE | ID: mdl-36773741

ABSTRACT

OBJECTIVES: To investigate the influence of thermal cycling and mechanical loading (TCML) aging on fracture resistance and wear behavior of various chairside computer-aided-designed/computer-assisted-manufactured (CAD/CAM) premolar crowns cemented on standardized tooth abutments. METHODS: Eighty chairside CAD/CAM crowns were prepared using lithium disilicate (IPS e.max CAD; EM), zirconia-infiltrated lithium silicate (Celtra Duo; CD), polymer-infiltrated ceramic network (Vita Enamic; VE), and resin nanoceramics (Cerasmart; CS) (n = 20). The specimens were divided into two groups (n = 10). In one group, they were subjected to TCML: thermocycling (6000 cycles in distilled water at 5-55 °C) and mechanical loading (50 N for 1.2 × 106 cycles), while in control group they were stored in distilled water (37 °C for 24 h). The fracture load, height loss, and volume wear of the crowns were measured after TCML. Fractography was performed on fractured specimens. Data were analyzed using analysis of variance and multiple comparison tests (α=0.05). RESULTS: The mean fracture loads of EM and CD were significantly higher than those of EC and CS (p<0.05). There was no significant change in the fracture load of any CAD/CAM crowns after TCML (p>0.05). CS exhibited a significantly higher volume wear than the other materials investigated. The wear tracts of all TCML crowns acted as failure origins during the fracture test. CONCLUSIONS: The fracture resistance of glass-ceramic CAD/CAM crowns was significantly higher than that of resin composite crowns. A 5-year TCML aging did not affect the fracture resistance of CAD/CAM crowns investigated. However, TCML treatment produces a larger wear track in CS than in other materials. CLINICAL SIGNIFICANCE: Appropriate chairside CAD/CAM restorative material should be selected for successful clinical practice after considering the fracture and wear resistance of the crowns.


Subject(s)
Ceramics , Dental Restoration Failure , Dental Porcelain , Crowns , Dental Materials , Composite Resins , Computer-Aided Design , Water , Materials Testing , Dental Stress Analysis
9.
Materials (Basel) ; 17(1)2023 Dec 24.
Article in English | MEDLINE | ID: mdl-38203954

ABSTRACT

Titanium alloys are widely used in various structural materials due to their lightweight properties. However, the low wear resistance causes significant economic losses every year. Therefore, it is necessary to implement wear-resistant protection on the surface of titanium alloys. In this study, four types of in situ composite ceramic coatings with two-layer gradient structures were prepared on a Ti-6Al-4V (TC4) substrate using laser cladding. In order to reduce the dilution rate, a transition layer (Ti-40SiC (vol.%)) was first prepared on TC4 alloy. Then, a high-volume-fraction in situ composite ceramic working layer (Ti-xFe-80SiC (vol.%)) with different contents of Fe-based alloy powder (x = 0, 5, 10 and 15 vol.%) was prepared. The working surface of Ti-40SiC (TL) exhibited a typical XRD pattern of Ti, TiC, Ti5Si3, and Ti3SiC2. In comparison, both Ti-80SiC (WL-F0) and Ti-5Fe-80SiC (WL-F5) exhibited similar phase compositions to the TL coating, with no new phase identified in the coatings. However, the TiFeSi2 and SiC phases were presented in Ti-10Fe-80SiC (WL-F10) and Ti-15Fe-80SiC (WL-F15). It is proven that the addition of the Fe element could regulate the in situ reaction in the original Ti-Si-C ternary system to form the new phases with high hardness and good wear resistance. The hardness of the WL-F15 (1842.9 HV1) is five times higher than that of the matrix (350 HV1). Due to the existence of self-lubricating phases such as Ti5Si3 and Ti3SiC2, a lubricating film was presented in the WL-F0 and WL-F5 coatings, which could block the further damage of the friction pair and enhance the wear resistance. Furthermore, a wear-transition phenomenon was observed in the WL-F10 and WL-F15 coatings, which was similar to the friction behavior of structural ceramics. Under the load of 10 N and 20 N, the wear volume of WL-F15 coating is 5.2% and 63.7% of that in the substrate, and the depth of friction of WL-15 coating is only 14.4% and 80% of that in the substrate. The transition of wear volume and depth can be attributed to the wear mechanism changing from oxidation wear to adhesive wear.

10.
Polymers (Basel) ; 14(19)2022 Oct 04.
Article in English | MEDLINE | ID: mdl-36236119

ABSTRACT

To reduce the use of carbon components sourced from fossil fuels, hemp fibers were pyrolyzed and utilized as filler to prepare EVA-based composites for automotive applications. The mechanical, tribological, electrical (DC and AC) and thermal properties of EVA/fiber biochar (HFB) composites containing different amounts of fibers (ranging from 5 to 40 wt.%) have been thoroughly studied. The morphological analysis highlighted an uneven dispersion of the filler within the polymer matrix, with poor interfacial adhesion. The presence of biochar fibers did not affect the thermal behavior of EVA (no significant changes of Tm, Tc and Tg were observed), notwithstanding a slight increase in the crystallinity degree, especially for EVA/HFB 90/10 and 80/20. Conversely, biochar fibers enhanced the thermo-oxidative stability of the composites, which increased with increasing the biochar content. EVA/HFB composites showed higher stiffness and lower ductility than neat EVA. In addition, high concentrations of fiber biochar allowed achieving higher thermal conductivity and microwave electrical conductivity. In particular, EVA/HFB 60/40 showed a thermal conductivity higher than that of neat EVA (respectively, 0.40 vs. 0.33 W·m-1 ·K-1); the same composite exhibited an up to twenty-fold increased microwave conductivity. Finally, the combination of stiffness, enhanced thermal conductivity and intrinsic lubricating features of the filler resulted in excellent wear resistance and friction reduction in comparison with unfilled EVA.

11.
Materials (Basel) ; 15(17)2022 Aug 31.
Article in English | MEDLINE | ID: mdl-36079403

ABSTRACT

Wire arc additively manufactured (WAAM) Ni-based materials have good properties but are costly and hard to cut, leading to difficulties in machining after welding and wasting the materials. To overcome these shortcomings, this work proposes a method of surfacing Fe-based alloy layers on WAAM Ni-based material. The effect of this method on the microstructure and wear properties of WAAM Ni-based materials is discussed. In this work, a Fe-based alloy (JX103) was welded as the last layers of the WAAM Ni-based superalloy (JX201) material. The hardness, microstructure, and wear behavior of the material with different residual Fe-based materials were tested and analyzed. Our results indicate that the surface hardness was smoothly increased from HV350 to HV400 by overlaying Fe-based alloy layers. Microstructure analysis shows that γ-Fe gradually disappears, and the carbide form changes from WAAM Ni-based superalloys to Fe-based alloys. In the fusion boundary, the occurrence of cellular dendritic growth, a type -Ⅱ boundary, and low dilution indicate good crack resistance and good connection performance between these two materials. The wear test showed that the wear resistance of JX201 was decreased by changing the last layer to JX103. However, as the residual thickness of JX103 decreased, the influence gradually reduced. Meanwhile, the wear mechanism changed from severe abrasive and adhesive wear to light abrasive wear. When the thickness is less than 0.5 mm, the wear weight per minute is at the same level as the sample without JX103.

12.
Materials (Basel) ; 15(16)2022 Aug 16.
Article in English | MEDLINE | ID: mdl-36013769

ABSTRACT

Coatings are now frequently used on cutting tool inserts in the metal production sector due to their better wear resistance and heat barrier effect. Protective hard coatings with a thickness of a few micrometers are created on cutting tools using physical or chemical vapor deposition (PVD, CVD) to increase their application performance. Different coating materials are utilized for a wide range of cutting applications, generally in bi-or multilayer stacks, and typically belong to the material classes of nitrides, carbides, carbonitrides, borides, boronitrides, or oxides. The current study examines typical hard coatings deposited by PVD and CVD in the corresponding material classes. The present state of research is reviewed, and pioneering work on this subject as well as recent results leading to the construction of complete "synthesis-structure-property-application performance" correlations of the different coatings are examined. When compared to uncoated tools, tool coatings prevent direct contact between the workpiece and the tool substrate, altering cutting temperature and machining performance. The purpose of this paper is to examine the effect of cutting-zone temperatures on multilayer coating characteristics during the metal-cutting process. Simplified summary and comparisons of various coating types on cutting tools based on distinct deposition procedures. Furthermore, existing and prospective issues for the hard coating community are discussed.

13.
Materials (Basel) ; 15(15)2022 Jul 28.
Article in English | MEDLINE | ID: mdl-35955169

ABSTRACT

Tooth enamel wear occurs because of daily mastication and occlusion. This study investigated the wear behavior of bovine teeth against aesthetic restorative materials in vitro. Abrader specimens were fabricated using four tooth-colored restorative materials (zirconia, lithium disilicate glass ceramic, dental porcelain, and resin composite), with bovine tooth enamel as a control. Flattened bovine tooth enamel was used as the substrate specimen. These materials were characterized by Vickers hardness tests and surface roughness measurements. Two-body wear tests between the abrader and substrate specimens were performed, and the worn topographies were evaluated using a contour-measuring instrument and 3D laser microscope. The restorative materials and bovine tooth enamel had similar surface roughness but different hardness and wear behaviors. Bovine teeth showed the largest wear in tooth-tooth contact as the abrader and substrate specimens. Compared to bovine teeth, zirconia, lithium disilicate glass ceramic, and dental porcelain showed greater hardness and less wear on their surfaces, and less substrate wear of the opposite tooth enamel. The lowest hardness resin composite showed intermediate wear on its surface, resulting in the lowest substrate wear. Accordingly, dentists should pay attention to the selection of restorative materials to reconstruct their morphologies owing to different wear behaviors.

14.
Photobiomodul Photomed Laser Surg ; 40(5): 355-361, 2022 May.
Article in English | MEDLINE | ID: mdl-35559712

ABSTRACT

Objective: Herein, a feasible strategy based on a femtosecond laser (fs-laser) was provided to decelerate dentin wear, and the effect of wear resistance improvement and its potential mechanism were explored. Background: Tooth wear is a common phenomenon that exists throughout life. While once dentin is exposed, it wears away very quickly. Decelerating tooth wear, especially dentin wear, is an important issue, but there is no ideal treatment. Materials and methods: Sixteen third molar dentin samples were randomly divided into the amalgam (N1 = 8) and polymer infiltrated ceramic network (PICN) (N2 = 8) groups. One half of the sample was used as the experimental object and the other for the blank self-control. Array microcavities were fabricated on the experimental parts of all the samples with an fs-laser and then filled with the corresponding materials. The experimental and control parts of all the samples were subjected to 3600 cycles of sliding wear tests with titanium balls. The coefficients of friction (COFs) of every friction pair and the temperature rise were recorded in real time. The wear volume and depth were measured by a laser confocal microscopy. Statistical differences of wear volume and depth between the experimental and self-control parts were calculated by paired t-test. The wear mode was observed with scanning electron microscopy (SEM). Results: The COFs in the two experimental groups were significantly decreased. The maximum temperature rise on the dentin surface was 2.0°C. The wear resistance in the amalgam and PICN groups was 4.48 and 3.53 times higher than blank dentin, respectively (p < 0.001). The SEM images showed fewer plough grooves and cracks in dentin after microtexturing. Conclusions: This method could significantly improve tooth wear resistance by reducing the COFs between the friction pairs and reducing the dentin's ploughing effect and provide new treatment ideas for slowing the loss of severely worn dentin.


Subject(s)
Ceramics , Tooth Wear , Dentin , Humans , Lasers , Microscopy, Electron, Scanning , Polymers/pharmacology
15.
Materials (Basel) ; 15(6)2022 Mar 10.
Article in English | MEDLINE | ID: mdl-35329509

ABSTRACT

Ti-based alloys are an important class of materials suitable especially for medical applications, but they are also used in the industrial sector. Due to their low tribological properties it is necessary to find optimal technologies and alloying elements in order to develop new alloys with improved properties. In this paper, a study on the influence of sintering treatments on the final properties of a titanium alloy is presented. The alloy of interest was obtained using the powders in following weight ratio: 80% wt Ti, 8% wt Mn, 3% wt Sn, 6% wt Aluminix123, 2% wt Zr and 1% wt graphite. Two sintering methods were used, namely two-step sintering (TSS) and multiple-step sintering (MSS), as alternatives to conventional sintering which uses a single sintering dwell time. Evolution of sample morphology, composition and crystalline structure with sintering method was evidenced. The lower values for the friction coefficient and for the wear rate was attained in the case of the sample obtained by TSS.

16.
Materials (Basel) ; 15(6)2022 Mar 17.
Article in English | MEDLINE | ID: mdl-35329686

ABSTRACT

A porous metal-bonded diamond grinding wheel has an excellent performance in precision grinding. In this research, a novel manufacturing process of porous metal-bonded diamond coating was presented. Firstly, the diamond/Ni/Al coatings (400-600 µm) were fabricated via low-pressure cold spraying and their microstructures were studied. The diamond particles in the feedstock had a core-shell structure. Secondly, the post-spray heat-treatments were set at 400 °C and 500 °C to produce pores in the cold-sprayed coatings via Ni-Al diffusion. The porosities of 400 °C and 500 °C heated coating were 8.8 ± 0.8% and 16.1 ± 0.7%, respectively. Finally, the wear behavior of porous heated coating was tested in contrast with cold-sprayed coating under the same condition via a ball-on-disc tribometer. The wear mechanism was revealed. The porous heated coating had better wear performance including chip space and slight clogging. The surface roughness of wear counterpart ground by the porous heated coating was smaller (Sa: 0.30 ± 0.07 µm) than that ground by cold-sprayed coating (Sa: 0.37 ± 0.09 µm). After ultrasonic clean, the average exposure height of diamond particles in the wear track of porous heated coating was 44.5% higher than that of cold-sprayed coating. The presented manufacturing process can contribute to fabricate high performance grinding wheels via cold spraying and porous structure controlling through Ni-Al diffusion-reaction.

17.
Materials (Basel) ; 15(3)2022 Jan 19.
Article in English | MEDLINE | ID: mdl-35160692

ABSTRACT

The present work aimed to investigate the dry sliding wear behaviors of hybrid polymer matrix composites made up of Kevlar, bamboo, palm, and Aloe vera as reinforcement materials of varying stacking sequences, along with epoxy as the matrix material. Three combinations of composite laminates with different stacking sequences such as AB, BC, and CA were fabricated by a vacuum-assisted compression molding process. The influence of composite laminates fabricated through various stacking sequences and dry sliding wear test variables such as load, sliding distance, and sliding velocity on the specific wear rate and co-efficient of friction were investigated. Experiments were designed and statistical validation was performed through response surface methodology-based D-optimal design and analysis of variance. The optimization was performed using grey relational analysis (GRA) to identify the optimal parameters to enhance the wear resistance of hybrid polymer composites under dry sliding conditions. The optimal parameters, such as composite combinations of CA, a load of 5 N, a sliding velocity of 3 m/s, and a sliding distance of 1500 m, were obtained. Furthermore, the morphologies of worn-out surfaces were investigated using SEM analysis.

18.
Materials (Basel) ; 15(3)2022 Feb 06.
Article in English | MEDLINE | ID: mdl-35161163

ABSTRACT

4145H steel is a commonly used material for downhole tools. However, up to now the wear behavior of 4145H drilling tool steel under real drilling fluid environment conditions is still not clear. In this work, this was investigated using a modified ASTM B611 rubber ring wet grinding test system, in which six kinds of abrasives (talc, dolomite or fluorite, as well as their mixed abrasive with quartz) with metal hardness-to-abrasive hardness ratios (H/HA) ranging from 0.25 to 6.25 were used in the drilling fluid for experiments. The results show that the H/HA value determined the wear mechanism of 4145H steel. When a single soft abrasive was used (with H/HA higher than 1.3-1.5), polishing was the dominantly observed mechanism. While mixed abrasives were applied, a microcutting mechanism due to the ploughing of hard abrasive particles on the steel surface was also observed. The increase in mass fraction of the soft abrasives has little effect on the wear rate of 4145H steel, but its wear rate will significantly increase as the mass fraction of hard abrasives increases. Therefore, in order to extend the life of drilling tools and reduce downhole accidents, the mass fraction of hard particles in the drilling fluid should be reduced as much as possible.

19.
Polymers (Basel) ; 14(2)2022 Jan 12.
Article in English | MEDLINE | ID: mdl-35054708

ABSTRACT

The wear of acrylic denture teeth is a serious problem that can change the vertical dimensions of dentures. This study evaluates the effect of adding salinized nano ZrO2 particles on the microstructure, hardness, and wear resistance of acrylic denture teeth. Heat polymerizing polymethyl methacrylate resin was mixed with salinized ZrO2 at concentrations of 5 wt.% and 10 wt.%. Acrylic resin specimens without filler addition were used as a control group. SEM/EDS analyses were performed and the Vickers' hardness was evaluated. Two-body wear testing was performed using a chewing simulator with a human enamel antagonist. After subjecting the samples to 37,500 cycles, both height loss and weight loss were used to evaluate the wear behavior. The microstructural investigation of the reinforced-denture teeth indicates sound nanocomposite preparation using the applied regime without porosity or macro defects. The addition of zirconium oxide nanofillers to PMMA at both 5% and 10% increased the microhardness, with values of up to 49.7 HV. The wear mechanism in the acrylic base material without nanoparticle addition was found to be fatigue wear; a high density of microcracks were found. The addition of 5 wt.% ZrO2 improved the wear resistance. Increasing the nanoparticles to 10 wt.% ZrO2 further improved the wear resistance, with no microcracks found.

20.
Materials (Basel) ; 14(22)2021 Nov 20.
Article in English | MEDLINE | ID: mdl-34832447

ABSTRACT

In this study, the wear behavior of a heat-treatable Al-7Si-0.5Mg-0.5Cu alloy fabricated by selective laser melting was investigated systematically. Compared with the commercial homogenized AA2024 alloy, the fine secondary phase of the SLM Al-Cu-Mg-Si alloy leads to a low specific wear rate (1.8 ± 0.11 × 10-4 mm3(Nm)-1) and a low average coefficient of friction (0.40 ± 0.01). After the T6 heat treatment, the SLM Al-Cu-Mg-Si alloy exhibits a lower specific wear rate (1.48 ± 0.02 × 10-4 mm3(Nm)-1), but a similar average coefficient of friction (0.34 ± 0.01) as the heat-treated AA2024 alloy. Altogether, the SLM Al-3.5Cu-1.5Mg-1Si alloy is suitable for the achievement of not only superior mechanical performance, but also improved tribological properties.

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