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1.
Materials (Basel) ; 15(8)2022 Apr 14.
Artículo en Inglés | MEDLINE | ID: mdl-35454576

RESUMEN

The aim of the work is to investigate the effectiveness of selected classification algorithms and their extensions in assessing microstructure of castings. Experiments were carried out in which the prepared algorithms and machine learning methods were tested in various conditions and configurations, as well as for various input data, which are photos of castings (photos of the microstructure) or information about the material (e.g., type, composition). As shown by the literature review, there are few scientific papers on this subject (i.e., in the use of machine learning to assess the quality of the microstructure and the obtained strength properties of cast iron). The effectiveness of machine learning algorithms in assessing the quality of castings will be tested using the most universal methods. Results obtained by classic machine learning methods and by neural networks will be compared with each other, taking into account aspects such as interpretability of results, ease of model implementation, algorithm simplicity, and learning time.

2.
Materials (Basel) ; 15(4)2022 Feb 12.
Artículo en Inglés | MEDLINE | ID: mdl-35207895

RESUMEN

Magnesium alloys, due to their unique properties, low density and high strength properties, are becoming more frequently used in industrial applications. However, a limitation of their use may be the need to ensure high abrasive wear resistance and corrosion resistance. Therefore, magnesium alloys are often protected by applying protective coatings. The paper presents the influence of the modification of the electrolyte composition, with or without the addition of borax, on the morphology (observed by SEM method) and phase composition (analyzed by EDS and XRD) of the formed layers on the AZ91 magnesium alloy, and their abrasive wear (determined with Ball-on-Disc method) and corrosion resistance (evaluated using the immersion method and by electrochemical tests), especially in chloride solutions. It has been clearly demonstrated that the modification of the electrolyte composition significantly impacts the final properties of the protective coatings on the AZ91 alloy formed by the plasma electrolytic oxidation (PEO) process. On the basis of the results, it was found that the new type of PEO coatings with the borax addition, compared to base PEO coatings, showed significantly higher abrasion resistance and an order of magnitude lower corrosion rate.

3.
Materials (Basel) ; 14(12)2021 Jun 14.
Artículo en Inglés | MEDLINE | ID: mdl-34198565

RESUMEN

Recent work indicates that the high-velocity oxy-fuel (HVOF) thermal spraying WC-Co coatings have been used to enhance the wear resistance of various engineering components in a variety of industrial environments. In the present work, WC-Co powder, containing Cr particles in an amount of 10%, was deposited on ductile cast iron with the HVOF thermal spray coating technique. An investigation was conducted to determine the role of Cr particles in the WC-Co coating produced with the HVOF technique on microstructure, mechanical, and wear properties in a system of type: WC-Co coating/ductile cast iron. The microstructure of the HVOF-sprayed WC-Co + Cr coating was characterised by light microscopy, X-ray diffraction (XRD), scanning electron microscope (SEM), transmission electron microscope (TEM), and energy-dispersive X-ray spectroscopy (EDS). The analysis of the microstructure showed the formation of a coating with low porosity, compact structure, and good adhesion to the substrate with a typical lamellar structure composed of fine molten Cr particles and finely fragmented WC grains embedded in a Co matrix, reaching the size of nanocrystalline. The scratch test was applied for the analysis of the adhesion of coatings to the substrate. The erosion behaviour and mechanism of material removal was studied and discussed based on microstructural examinations. Moreover, the results were discussed in relation to the bending strength test, including cracks and delamination in the system of the WC-Co + Cr/ductile cast iron, as microhardness and erosion resistance of the coating. It was found that the addition of Cr particles to the WC-Co powder, which causes hardening of the binder phase is a key influence on increased mechanical and wear properties in the studied system. Additionally, due to the construction of nanostructured coatings, suitable proportion of hard and soft phases, the technique sprayed HVOF coatings have advantageous properties such as high density and good slurry erosion resistance.

4.
Materials (Basel) ; 13(18)2020 Sep 16.
Artículo en Inglés | MEDLINE | ID: mdl-32948062

RESUMEN

Alumina oxide coatings are widely used in many industrial applications to improve corrosion protection, wear and erosion resistances, and thermal insulation of metallic surfaces. The paper presents study of the microstructure, mechanical, and wear properties of HVOF (high velocity oxy-fuel process) sprayed of Al2O3-15 wt.% TiO2 coating with the NiAl interlayer on the surface of Al-Si alloy castings. The microstructure of Al2O3-15 wt.% TiO2/NiAl coating was characterized by light microscopy, X-ray diffraction (XRD), scanning electron microscope (SEM), and energy dispersive X-ray spectroscopy (EDS). The analysis of the microstructure showed the formation of coating with low porosity, compact structure, good adhesion to the substrate with typical lamellar structure composed of a solid phase consisting of compounds included in the coating material and their phase variations. For analysis of the adhesion of coatings to the substrate, the scratch test was applied. An assessment of the erosive wear resistance of coatings was also carried out, confirming the significant impact of the interlayer as well as the microstructure and phase composition of the oxide coating on the wear resistance of the tested coating system. Moreover, the results were discussed in relation to the bending strength test, including cracks and delamination in the system of the Al2O3-15 wt.% TiO2/NiAl/Al-Si alloy as microhardness and erosion resistance of the coating. It was found that the introduction of the NiAl metallic interlayer significantly increased resistance to cracking and wear behavior in the studied system.

5.
Materials (Basel) ; 14(1)2020 Dec 30.
Artículo en Inglés | MEDLINE | ID: mdl-33396840

RESUMEN

The purpose of this work was to systematically assess the distribution of thermoluminescence (TL) and optically stimulated luminescence (OSL) properties along the length of crystals grown by the micro-pulling-down method, in relation to the microstructure and distribution of activators. We analyzed lithium magnesium phosphate (LiMgPO4; LMP) crystals doped with terbium (Tb; 0.8 mol%) or with a combination of thulium (Tm; 0.8 mol% or 1.2 mol%) and boron (B; 10 mol%). Crystals of several centimeters in length and 3 mm in diameter were cut into 20-40 slices, depending on length. For each sample, TL glow curves and OSL decay curves were examined. Optical microscopy and scanning electron microscopy were used to assess the microstructure and elemental composition of several selected samples. Two-dimensional TL readouts were performed to identify the areas with higher and lower signal emission. Our study showed that there may be significant differences not only in LMP sensitivity along the crystal's axis but also on the surface of the slice. The distribution of activators varies depending on the type of crystals and strongly affects luminescence properties.

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