Neutron radiography of an anisotropic drainage flow.

Liquid drainage through foam is dominated by gravity, capillary, and viscous forces. The liquid is conducted by an isotropic network of Plateau borders; however, imposed stress changes the alignment of the foam's structural elements. Previous numerical simulations predicted that a vertical drainage flow will be deflected horizontally if the foam is sheared. We investigated this phenomenon by measuring the distribution of the liquid fraction within a foam formed in a flat rectangular cell. The foam was subjected to shear stress under a forced liquid supply from the top of the cell. Neutron radiographies of unchanged and sheared foam were analyzed to extract measurements of the liquid fraction. Deflections in the distribution of the drainage liquid were detected and found to be positively correlated with increasing foam shear.

Effect of Retrofit Design Modifications on the Macroturbulence of a Three-Phase Flotation Tank-Flow Characterization Using Positron Emission Particle Tracking (PEPT).

Turbulence in stirred tank flotation tanks impacts the bulk transport of particles and has an important role in particle-bubble collisions. These collisions are necessary for attachment, which is the main physicochemical mechanism enabling the separation of valuable minerals from ore in froth flotation. Modifications to the turbulence profile in a flotation tank, therefore, can result in improvements in flotation performance. This work characterized the effect of two retrofit design modifications, a stator system and a horizontal baffle, on the particle dynamics of a laboratory-scale flotation tank. The flow profiles, residence time distributions, and macroturbulent kinetic energy distributions were derived from positron emission particle tracking (PEPT) measurements of tracer particles representing valuable (hydrophobic) mineral particles in flotation. The results show that the use of both retrofit design modifications together improves recovery by increasing the rise velocity of valuable particles and decreasing turbulent kinetic energy in the quiescent zone and at the pulp-froth interface.

A methodology to implement a closed-loop feedback-feedforward level control in a laboratory-scale flotation bank using peristaltic pumps.

This paper describes the implementation of a level control strategy in a laboratory-scale flotation system. The laboratory-scale system consists of a bank of three flotation tanks connected in series, which mimics a flotation system found in mineral processing plants. Besides the classical feedback control strategy, we have also included a feedforward strategy to better account for process disturbances. Results revealed that the level control performance significantly improves when a feedforward strategy is considered. This methodology uses peristaltic pumps for level control, which has not been extensively documented even though: (1) peristaltic pumps are commonly used in laboratory-scale systems, and (2) the control implementation is not as straightforward as those control strategies that use valves. Therefore, we believe that this paper, which describes a proven methodology that has been validated in an experimental system, can be a useful reference for many researchers in the field.•Preparation of reagents to ensure that the froth stability of the froth layer is representative of an industrial flotation froth.•Calibration of instruments - convert the electrical signal from PLCs to engineering units.•Tuning PI parameters using SIMC rules by performing step-changes in each flotation cell.

Standard method for performing positron emission particle tracking (PEPT) measurements of froth flotation at PEPT Cape Town.

Positron emission particle tracking (PEPT) is a technique for measuring the motion of tracer particles in systems of flow such as mineral froth flotation. An advantage of PEPT is that tracer particles with different physical properties can be tracked in the same experimental system, which allows detailed studies of the relative behaviour of different particle classes in flotation. This work describes the standard operating protocol developed for PEPT experiments in a flotation vessel at PEPT Cape Town in South Africa. A continuously overflowing vessel with constant air recovery enables several hours of data acquisition at steady state flow and consistent flotation conditions. Tracer particles are fabricated with different coatings to mimic mineral surface hydrophobicity and size, and a data treatment derived from a rotating disk study is utilized to produce high frequency (1 kHz) location data relative to the tracer activity. Time averaging methods are used to represent the Eulerian flow field and occupancy of the tracer behaviour based on voxel schemes in different co-ordinate systems. The average velocity of the flow in each voxel is calculated as the peak of the probability density function to represent the peak of asymmetrical or multimodal distributions.•A continuously overflowing flotation vessel was developed for extended data acquisition at steady state flow.•The data treatment enabled the direct comparison of different particle classes in the flotation vessel.•The solids flow fields was described by the probability density function of tracer particle velocity measured in different voxel schemes.

Coalescence Dynamics of Particle-Laden Bubbles.

Understanding the coalescence of particle-laden bubbles is crucial to our understanding of the role of particles in stabilizing liquid foams. In this work, the coalescence of microparticle-laden bubbles is studied experimentally using high-speed photography. In particular, the interparticle forces in the neck region during the early stage of bubble coalescence are calculated. The results indicate that a monolayer of silica particles coating the bubble surfaces hinders the growth dynamics of the air neck formed between the coalescing bubbles. We postulate that the decrease in the growth dynamics is due to the surface pressure caused by the particle interaction after the initiation of bubble coalescence. We identify that the apparent surface tension in the neck region increases with time for particle-laden bubbles and is lower for larger particle sizes. These findings enhance our understanding of the role of particles on the dynamics of fast deforming interfaces.

Effect of Particle Size on the Rising Behavior of Particle-Laden Bubbles.

The rising behavior of bubbles, initially half and fully coated with glass beads of various sizes, was investigated. The bubble velocity, aspect ratio, and oscillation periods were determined using high-speed photography and image analysis. In addition, the acting forces, drag modification factor, and modified drag coefficient were calculated and interpreted. Results show that the aspect ratio oscillation of the rising bubbles is similar, irrespective of the attached particle size. As the particle size is increased, the rising bubbles have a lower velocity and aspect ratio amplitude, with the time from release to each aspect ratio peak increasing. Higher particle coverage is shown to decrease the bubble velocity and dampen the oscillations, reducing the number of aspect ratio peaks observed. The highest rise velocities correspond to the lowest aspect ratios and vice versa, whereas a constant aspect ratio yields a constant rise velocity, independent of the particle size. Force analysis shows that the particle drag modification factor increases with the increased particle size and is greatest for fully laden bubbles. The modified drag coefficient of particle-laden bubbles increases with the increased particle size, although it decreases with the increased Reynolds number independent of the particle size. The drag force exerted by the particles plays a more dominant role in decreasing bubble velocities as the particle size increases. The results and interpretation produced a quantitative description of the behavior of rising particle-laden bubbles and the development of correlations will enhance the modeling of industrial applications.

A Multicriteria Decision Framework for the Selection of Biomass Separation Equipment.

For the first time, a two-stage decision support framework for equipment selection, applied to biomass separation, is presented. In the first stage, the framework evaluates from a number of equipment based on the process requirements and outputs only those that offer a technically feasible separation. In the second stage, the analytic hierarchy process is applied for performing a multicriteria decision analysis to select amongst the feasible equipment based on separation performance and energy consumption criteria. This approach systematically considers the relative importance of those different alternatives and selection criteria by pairwise comparisons. The output of the framework is an overall ranking of equipment as well as a sensitivity analysis of the results for different weighting of the criteria. These results can be used to equip practitioners in the field of bioseparations with a tool for making more consistent and better-informed equipment selection decisions.

Influence of Design Parameters on Biomass Separation in Mini-hydrocyclones.

Small hydrocyclones are an attractive technology for biomass separation from fermentation processes. The interactive effect of design parameters on the performance of mini-hydrocyclones is, however, not fully explored and studies are often limited by the challenges in manufacturing such small units. Here, 10-mm mini-hydrocyclones are produced by 3D printing and the impact of spigot diameter, vortex finder diameter and height on separation performance is studied. A central composite rotatable design was adopted to obtain information on the relation between the variables and their influence on concentration ratio and recovery of yeast from a highly diluted system. A Pareto front for separation performance was generated and shown to be suitable to select an optimal design for a set of process constraints.

Geometry and Topology of Two-Dimensional Dry Foams: Computer Simulation and Experimental Characterization.

Pseudo-two-dimensional (2D) foams are commonly used in foam studies as it is experimentally easier to measure the bubble size distribution and other geometric and topological properties of these foams than it is for a 3D foam. Despite the widespread use of 2D foams in both simulation and experimental studies, many important geometric and topological relationships are still not well understood. Film size, for example, is a key parameter in the stability of bubbles and the overall structure of foams. The relationship between the size distribution of the films in a foam and that of the bubbles themselves is thus a key relationship in the modeling and simulation of unstable foams. This work uses structural simulation from Surface Evolver to statistically analyze this relationship and to ultimately formulate a relationship for the film size in 2D foams that is shown to be valid across a wide range of different bubble polydispersities. These results and other topological features are then validated using digital image analysis of experimental pseudo-2D foams produced in a vertical Hele-Shaw cell, which contains a monolayer of bubbles between two plates. From both the experimental and computational results, it is shown that there is a distribution of sizes that a film can adopt and that this distribution is very strongly dependent on the sizes of the two bubbles to which the film is attached, especially the smaller one, but that it is virtually independent of the underlying polydispersity of the foam.