Microtensile bond strength of silorane-based composite specific adhesive system using different bonding strategies.

OBJECTIVES: The aim of this study was to evaluate the effect of pre-etching on the bond strength of silorane-based composite specific adhesive system to dentin. MATERIALS AND METHODS: Thirty human molars were randomly divided into 5 groups according to the different bonding strategies. For teeth restored with silorane-based composite (Filtek Silorane, 3M ESPE), the specific self-etching adhesive system (Adhesive System P90, 3M ESPE) was used with and without pre-etching (Pre-etching/Silorane and Silorane groups). Teeth restored with methacrylate based-composite (Filtek Z250, 3M ESPE) were hybridized with the two-step self-etching system (Clearfil SE Bond, Kuraray), with and without pre-etching (Pre-etching/Methacrylate and Methacrylate groups), or three-step adhesive system (Adper Scotchbond Multi-Purpose, 3M ESPE) (Three-step/Methacrylate group) (n = 6). The restored teeth were sectioned into stick-shaped test specimens (1.0 × 1.0 mm), and coupled to a universal test machine (0.5 mm/min) to perform microtensile testing. RESULTS: Pre-etching/Methacrylate group presented the highest bond strength values, with significant difference from Silorane and Three-step/Methacrylate groups (p < 0.05). However, it was not significantly different from Preetching/Silorane and Methacrylate groups. CONCLUSIONS: Pre-etching increased bond strength of silorane-based composite specific adhesive system to dentin.

Color stability of modern composites subjected to different periods of accelerated artificial aging

The aim of this study was to evaluate the color stability of composites subjected to different periods of accelerated artificial aging (AAA). A polytetrafluorethylene matrix (10 x 2 mm) was used to fabricate 24 test specimens of three different composites (n=8): Tetric Ceram (Ivoclar/Vivadent); Filtek P90 and Z250 (3M ESPE), shade A3. After light activation for 20 s (FlashLite 1401), polishing and initial color readout (Spectrophotometer PCB 687; BYK Gardner), the test specimens were subjected to AAA (C-UV; Comexim), in 8-h cycles: 4 h exposure to UV-B rays at 50°C and 4 h condensation at 50°C. At the end of each cycle, color readouts were taken and the test ended when the mean value of ΔE attained a level ≥3.30. Tetric Ceram presented alteration in ΔE equal to 3.33 in the first aging cycle. For Filtek P90 and Z250, two (ΔE=3.60) and four (ΔE=3.42) AAA cycles were necessary. After each cycle, there was a reduction of luminosity in all the samples (ΔL). It was concluded that a short period of AAA was sufficient to promote clinically unacceptable color alteration in composites, and that this alteration was material-dependent.

O objetivo deste estudo foi avaliar estabilidade de cor de compósitos submetidos a diferentes períodos de envelhecimento artificial acelerado (EAA). Foram confeccionados, em matriz de teflon (10x2 mm), 24 corpos-de-prova de três compósitos (n=8): Tetric Ceram (Ivoclar/Vivadent); Filtek P90 e Z250 (3M ESPE), cor A3. Após fotoativação por 20 s (FlashLite 1401), polimento e leitura inicial de cor (espectrofotômetro PCB 687; BYK Gardner), os corpos-de-prova foram submetidos ao EAA (C-UV, Comexim), com ciclos de 8 h: 4 h de exposições a raios UV-B a 50°C e 4 h de condensação a 50°C. Ao final de cada ciclo, leituras de cor eram realizadas e quando o valor médio de ΔE atingisse índice ≥3,30, o ensaio era encerrado. Observou-se que Tetric Ceram apresentou alteração de ΔE igual a 3,33 já no primeiro ciclo de envelhecimento. Com Filtek P90 foram necessários dois ciclos de EAA (ΔE=3,60) e para Z250 quatro (ΔE=3,42). Observou-se que a cada ciclo ocorria diminuição na luminosidade de todas as amostras (ΔL). Concluiu-se que um curto período de EAA já é suficiente para que compósitos apresentem alteração de cor inaceitável clinicamente e que esta alteração é material dependente.

Color stability of modern composites subjected to different periods of accelerated artificial aging.

The aim of this study was to evaluate the color stability of composites subjected to different periods of accelerated artificial aging (AAA). A polytetrafluorethylene matrix (10 x 2 mm) was used to fabricate 24 test specimens of three different composites (n=8): Tetric Ceram (Ivoclar/Vivadent); Filtek P90 and Z250 (3M ESPE), shade A3. After light activation for 20 s (FlashLite 1401), polishing and initial color readout (Spectrophotometer PCB 687; BYK Gardner), the test specimens were subjected to AAA (C-UV; Comexim), in 8-h cycles: 4 h exposure to UV-B rays at 50°C and 4 h condensation at 50°C. At the end of each cycle, color readouts were taken and the test ended when the mean value of ΔE attained a level ≥3.30. Tetric Ceram presented alteration in ΔE equal to 3.33 in the first aging cycle. For Filtek P90 and Z250, two (ΔE=3.60) and four (ΔE=3.42) AAA cycles were necessary. After each cycle, there was a reduction of luminosity in all the samples (ΔL). It was concluded that a short period of AAA was sufficient to promote clinically unacceptable color alteration in composites, and that this alteration was material-dependent.

Polymerization shrinkage stress of composites photoactivated by different light sources.

The purpose of this study was to compare the polymerization shrinkage stress of composite resins (microfilled, microhybrid and hybrid) photoactivated by quartz-tungsten halogen light (QTH) and light-emitting diode (LED). Glass rods (5.0 mm x 5.0 cm) were fabricated and had one of the surfaces air-abraded with aluminum oxide and coated with a layer of an adhesive system, which was photoactivated with the QTH unit. The glass rods were vertically assembled, in pairs, to a universal testing machine and the composites were applied to the lower rod. The upper rod was placed closer, at 2 mm, and an extensometer was attached to the rods. The 20 composites were polymerized by either QTH (n=10) or LED (n=10) curing units. Polymerization was carried out using 2 devices positioned in opposite sides, which were simultaneously activated for 40 s. Shrinkage stress was analyzed twice: shortly after polymerization (t40s) and 10 min later (t10min). Data were analyzed statistically by 2-way ANOVA and Tukey's test (alpha=5%). The shrinkage stress for all composites was higher at t10min than at t40s, regardless of the activation source. Microfilled composite resins showed lower shrinkage stress values compared to the other composite resins. For the hybrid and microhybrid composite resins, the light source had no influence on the shrinkage stress, except for microfilled composite at t10min. It may be concluded that the composition of composite resins is the factor with the strongest influence on shrinkage stress.

Polymerization shrinkage stress of composites photoactivated by different light sources

The purpose of this study was to compare the polymerization shrinkage stress of composite resins (microfilled, microhybrid and hybrid) photoactivated by quartz-tungsten halogen light (QTH) and light-emitting diode (LED). Glass rods (5.0 mm x 5.0 cm) were fabricated and had one of the surfaces air-abraded with aluminum oxide and coated with a layer of an adhesive system, which was photoactivated with the QTH unit. The glass rods were vertically assembled, in pairs, to a universal testing machine and the composites were applied to the lower rod. The upper rod was placed closer, at 2 mm, and an extensometer was attached to the rods. The 20 composites were polymerized by either QTH (n=10) or LED (n=10) curing units. Polymerization was carried out using 2 devices positioned in opposite sides, which were simultaneously activated for 40 s. Shrinkage stress was analyzed twice: shortly after polymerization (t40s) and 10 min later (t10min). Data were analyzed statistically by 2-way ANOVA and Tukey's test (a=5 percent). The shrinkage stress for all composites was higher at t10min than at t40s, regardless of the activation source. Microfilled composite resins showed lower shrinkage stress values compared to the other composite resins. For the hybrid and microhybrid composite resins, the light source had no influence on the shrinkage stress, except for microfilled composite at t10min. It may be concluded that the composition of composite resins is the factor with the strongest influence on shrinkage stress.

Este estudo comparou a contração de polimerização de resinas compostas fotoativadas por luz halógena (QTH) e diodo emissor de luz (LED). Foram confeccionados bastões de vidro (5,0 mm x 5,0 cm), e uma de suas extremidades sofreu jateamento com óxido de alumínio, sobre a qual foi aplicado um adesivo e fotoativado com luz halógena. Os bastões de vidro foram acoplados verticalmente, em pares, em uma máquina universal de ensaios (EMIC DL-2000) e as resinas compostas aplicadas no bastão inferior. A distância entre os bastões foi padronizada em 2 mm e um extensômetro foi acoplado a eles. As resinas foram fotoativadas (n=20), sendo 10 por QTH e 10 por LED utilizando dois aparelhos posicionados em lados opostos, acionados simultaneamente por 40 s. A tensão de contração foi analisada em dois momentos: logo após a polimerização (t40s) e 10 min após (t10min). A tensão de contração apresentada por todas as resinas foi maior em t10min do que em t40s, independente da fonte ativadora. A resina de micropartículas apresentou menores valores de tensão de contração com valores estatisticamente significantes em relação às demais resinas. Para as resinas híbrida e microhíbrida não houve influência da unidade ativadora sobre a tensão de contração, com exceção para a resina de micropartículas em t10min. Concluiu-se que a composição da resina composta foi o fator que mais interferiu na tensão de contração da resina composta.