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Anal Sci ; 22(1): 35-8, 2006 Jan.
Artículo en Inglés | MEDLINE | ID: mdl-16429769

RESUMEN

An electrochemical cell coupled with disposable screen-printed electrodes (SPEs) that is specifically designed for use in flow injection analysis (FIA) is described in this study. The cell is made of foldable polyoxymethylene (acetal) thick platelets with the bottom portion consisting of a cavity track to drag the SPEs in position and the top portion having predrilled T-like holes to arrange the Ag/AgCl reference electrode and stainless steel inlet & outlet. An "O ring" is suitably fixed on the top of the working electrode to form a thin-layer space where the electrochemical reaction can take place. Hydrodynamic characterization was validated by using a benchmark hexacyanoferrate redox couple. The results of practical analysis of glucose in human plasma clearly demonstrate the characteristics and applicability of the proposed wall-jet electrochemical cell in FIA.


Asunto(s)
Glucemia/análisis , Resinas Sintéticas/química , Plata/química , Electroquímica , Electrodos , Análisis de Inyección de Flujo/instrumentación , Análisis de Inyección de Flujo/métodos , Humanos , Microscopía Electrónica de Rastreo/instrumentación , Microscopía Electrónica de Rastreo/métodos , Oxidación-Reducción , Sensibilidad y Especificidad , Factores de Tiempo
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