RESUMEN
The results of an international comparison of activity measurements of a solution of 231Pa are reported and analysed. Prior to this, no known standardisation of 231Pa by activity measurement had been carried out. The comparison was run in 2017-2018 involving eight laboratories, and returned results with no identifiable inconsistencies between methods or laboratories. The results, including one mass determination, gave a231Pa activity concentration of 41.461(48) kBq g-1 and a231Pa atom concentration of 61.48(23)â¯×â¯1015 atoms g-1, from which a half-life value of 32â¯570(130) years was derived.
RESUMEN
The results of the three years European Metrology Research Programme's (EMRP) joint research project 'Metrology for processing materials with high natural radioactivity' (MetroNORM) are presented. In this project, metrologically sound novel instruments and procedures for laboratory and in-situ NORM activity measurements have been developed. Additionally, standard reference materials and sources for traceable calibration and improved decay data of natural radionuclides have been established.
RESUMEN
New measurements of photon emission intensities in the decay of U-235 were performed. Source was prepared by deposition of a U-235 solution on glass plate. Standardization was carried out by defined solid angle alpha counting, giving the reference activity with 0.7% relative combined uncertainty. Gamma spectrometry was performed with accurately calibrated high-purity germanium detectors. Corrections for source geometry and coincidence summing effects were applied. The reference line (185.72keV) intensity was obtained with 1.3% relative standard uncertainty.