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Molecules ; 14(12): 4973-86, 2009 Dec 01.
Artículo en Inglés | MEDLINE | ID: mdl-20032871

RESUMEN

Commercial dehydroacetic acid was converted into 4-hydroxy-6-methylpyridin-2(1H)-one (3), which was then condensed with several aliphatic aldehydes to produce seven new title compounds in variable yields (35-92%). Reaction of 3 with alpha,beta-unsaturated aldehydes resulted in the formation of condensed pyran derivatives 4g' and 4h'. A mechanism is proposed to explain the formation of such compounds. The effects of all methylpyridin-2(1H)-one derivatives on the development of the dicotyledonous species Ipomoea grandifolia and Cucumis sativus and the monocotyledonous species Sorghum bicolor were evaluated. At the dose of 6.7 x 10(-8) mol a.i./g substrate the compounds showed some phytotoxic selectivity, being more active against the dicotyledonous species. These compounds can be used as lead structures for the development of more active phytotoxic products.


Asunto(s)
Piridonas/síntesis química , Piridonas/farmacología , Sorghum/efectos de los fármacos , Cristalografía por Rayos X , Espectroscopía de Resonancia Magnética , Modelos Moleculares , Piridonas/química , Espectrometría de Masa por Ionización de Electrospray , Espectrofotometría Infrarroja
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