RESUMEN
Recent developments in micro-scale additive manufacturing (AM) have opened new possibilities in state-of-the-art areas, including microelectromechanical systems (MEMS) with intrinsically soft and compliant components. While fabrication with soft materials further complicates micro-scale AM, a soft photocurable polydimethylsiloxane (PDMS) resin, IP-PDMS, has recently entered the market of two-photon polymerization (2PP) AM. To facilitate the development of microdevices with soft components through the application of 2PP technique and IP-PDMS material, this research paper presents a comprehensive material characterization of IP-PDMS. The significance of this study lies in the scarcity of existing research on this material and the thorough investigation of its properties, many of which are reported here for the first time. Particularly, for uncured IP-PDMS resin, this work evaluates a surface tension of 26.7 ± 4.2 mN/m, a contact angle with glass of 11.5 ± 0.6°, spin-coating behavior, a transmittance of more than 90% above 440 nm wavelength, and FTIR with all the properties reported for the first time. For cured IP-PDMS, novel characterizations include a small mechanical creep, a velocity-dependent friction coefficient with glass, a typical dielectric permittivity value of 2.63 ± 0.02, a high dielectric/breakdown strength for 3D-printed elastomers of up to 73.3 ± 13.3 V/µm and typical values for a spin coated elastomer of 85.7 ± 12.4 V/µm, while the measured contact angle with water of 103.7 ± 0.5°, Young's modulus of 5.96 ± 0.2 MPa, and viscoelastic DMA mechanical characterization are compared with the previously reported values. Friction, permittivity, contact angle with water, and some of the breakdown strength measurements were performed with spin-coated cured IP-PDMS samples. Based on the performed characterization, IP-PDMS shows itself to be a promising material for micro-scale soft MEMS, including microfluidics, storage devices, and micro-scale smart material technologies.
RESUMEN
Dielectric elastomer actuator (DEA) is a smart material that holds promise for soft robotics due to the material's intrinsic softness, high energy density, fast response, and reversible electromechanical characteristics. Like for most soft robotics materials, additive manufacturing (AM) can significantly benefit DEAs and is mainly applied to the unimorph DEA (UDEA) configuration. While major aspects of UDEA modeling are known, 3D printed UDEAs are subject to specific material and geometrical limitations due to the AM process and require a more thorough analysis of their design and performance. Furthermore, a figure of merit (FOM) is an analytical tool that is frequently used for planar DEA design optimization and material selection but is not yet derived for UDEA. Thus, the objective of the paper is modeling of 3D printed UDEAs, analyzing the effects of their design features on the actuation performance, and deriving FOMs for UDEAs. As a result, the derived analytical model demonstrates dependence of actuation performance on various design parameters typical for 3D printed DEAs, provides a new optimum thickness to Young's modulus ratio of UDEA layers when designing a 3D printed DEA with fixed dielectric elastomer layer thickness, and serves as a base for UDEAs' FOMs. The FOMs have various degrees of complexity depending on considered UDEA design features. The model was numerically verified and experimentally validated through the actuation of a 3D printed UDEA. The fabricated and tested UDEA design was optimized geometrically by controlling the thickness of each layer and from the material perspective by mixing commercially available silicones in non-standard ratios for the passive and dielectric layers. Finally, the prepared non-standard mix ratios of the silicones were characterized for their viscosity dynamics during curing at various conditions to investigate the silicones' manufacturability through AM.