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1.
J Magn Reson ; 265: 83-9, 2016 Apr.
Artículo en Inglés | MEDLINE | ID: mdl-26874333

RESUMEN

In recent years, permanent magnet-based NMR spectrometers have resurfaced as low-cost portable alternatives to superconducting instruments. While the development of these devices as well as clever shimming methods have yielded impressive advancements, scaling the size of these magnets to miniature lengths remains a problem to be addressed. Here we present the results of a study of a discrete shimming scheme for NMR Mandhalas constructed from a set of individual magnet blocks. While our calculations predict a modest reduction in field deviation by a factor of 9.3 in the case of the shimmed ideal Mandhala, a factor of 28 is obtained in the case of the shimmed imperfect Mandhala. This indicates that imperfections of magnet blocks can lead to improved field homogeneity. We also present a new algorithm to improve the homogeneity of a permanent magnet assembly. Strategies for future magnet construction can improve the agreement between simulation and practical implementation by using data from real magnets in these assemblies as the input to such an algorithm to optimize the homogeneity of a given design.

2.
Rev Sci Instrum ; 81(12): 124904, 2010 Dec.
Artículo en Inglés | MEDLINE | ID: mdl-21198044

RESUMEN

This article describes a technique to measure the temperature of a resistively heated ferromagnetic wire. The wire's temperature rapidly increases, a scenario in which a thermocouple or thermistor's thermal inertia prevents it from keeping up with the rapid temperature variation. The temperature is derived from electrical measurands (voltage and current) and time, as well as thermophysical data such as heat losses and emissivity, and is based on a dynamical thermal-electrical energy conservation principle. We go on to use our technique for the quantitative determination of the Curie point as well as the magnetic susceptibility at elevated temperatures. The results are in good agreement with accepted values.

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