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1.
3D Print Addit Manuf ; 11(3): e1087-e1099, 2024 Jun.
Article de Anglais | MEDLINE | ID: mdl-39359574

RÉSUMÉ

Additive manufacturing/three-dimensional printing (AM/3DP) processes promise a flexible production modality to fabricate a complex build directly from its digital design file with minimal postprocessing. However, some critical shortcomings of AM/3DP processes related to the build quality and process repeatability are frequently experienced and reported in the literature. In this study, an in situ real-time nondestructive monitoring framework based on the dispersive properties of phononic crystal artifacts (PCAs) to address such quality challenges is described. Similar to a witness coupon, a PCA is printed alongside a build while it is interrogated and monitored with ultrasound. A PCA is substantially smaller than the actual build. Due to its periodic internal structures, a PCA creates pass and stop bands in its spectral response, which are sensitive to the variations in its process and material parameters. These periodic structures, representing the geometric complexities of an actual build, are designed for a specific monitoring objective(s) in AM/3DP. As a model application, in this demonstration study, the effect of the laser scanning speed of a slective laser melting (SLM) printer on the spectral properties of metal PCAs (mPCAs) is ultrasonically evaluated offline. The dependency of the pressure and shear wave speeds, the apparent Young's and shear moduli, and Poisson's ratio on the scanning speed are quantified, and it is found that they are highly sensitive to the laser scanning speed of an SLM printer. The sensitivity of the peaks of the pressure and shear spectral waveforms acquired for the identical mPCA designs printed on the same build plate with the same process parameters is also quantified. For powder-based AM/3DP technologies, where scanning speed is among the crucial process parameters such as laser power and bed temperature, the reported correlations between scanning speeds and the mechanical and spectral features of the mPCAs are expected to be instrumental in developing in situ real-time monitoring systems.

2.
BMC Oral Health ; 24(1): 1205, 2024 Oct 10.
Article de Anglais | MEDLINE | ID: mdl-39390416

RÉSUMÉ

OBJECTIVE: A hybrid manufacturing technique that combines selective laser melting (SLM) and computer numerical control (CNC) has been developed for the fabrication of implant-platform/framework interfaces (PFIs) for mandibular and maxillary full-arch implant-supported titanium frameworks. The aim of this study was to compare the discrepancies in specimens fabricated using the hybrid technique (termed SLM/m hereafter) with those in specimens fabricated by conventional CNC milling. MATERIALS AND METHODS: Based on a mandibular four-PFI CAD model and a maxillary six-PFI CAD model, four groups of titanium frameworks (eight per group, totaling 32) were fabricated according to the fabrication technique (SLM/m or milling) and number of PFIs (four or six). The frameworks were scanned by a structured light scanner and aligned with the CAD model in Geomagic Control X. Discrepancy was defined as the difference between the PFIs of the scanned framework and those of the CAD model. Discrepancies were measured and evaluated by multilevel analysis using a mixed-effects model (α = 0.05), followed by independent samples t-tests (α = 0.0125). Furthermore, the manufacturing times and raw-material costs were recorded and compared. RESULTS: The maximum discrepancy values for the four-PFI and six-PFI hybrid frameworks were 52.2 and 64.3 µm, respectively. Multilevel analysis revealed that the fabrication technique and the number of PFIs had no significant effect on the discrepancy value. However, a significant interaction between the two factors was observed (P = 0.020). The discrepancies for the four-PFI hybrid frameworks were significantly lower than those for the four-PFI milled frameworks (P = 0.001). No significant difference in discrepancies between the six-PFI hybrid frameworks and six-PFI milled frameworks was observed (P = 0.697). Furthermore, the hybrid frameworks required only 11% of the raw materials and 25% of the milling time required for the conventionally milled frameworks. CONCLUSION: SLM/m hybrid frameworks are viable, accurate alternatives to CNC-milled frameworks, with the added benefit of substantial cost reduction.


Sujet(s)
Conception assistée par ordinateur , Prothèse dentaire implanto-portée , Titane , Titane/composition chimique , Humains , Lasers , Mandibule , Conception de prothèse dentaire/méthodes
3.
Materials (Basel) ; 17(17)2024 Aug 28.
Article de Anglais | MEDLINE | ID: mdl-39274635

RÉSUMÉ

Metals manufactured by selective laser melting (SLM) with different directions exhibit different mechanical properties. This study conducted dynamic and static mechanical tests using a universal testing machine and split-Hopkinson bar (SHPB). The mechanical properties of 18Ni300 with 0° and 90° build directions manufactured by SLM were compared, and the micro-structure properties of the two build directions were analysed by metallographic tests. The Johnson-Cook (J-C) constitutive model was fitted according to the experimental results, and the obtained constitutive parameters were verified by numerical simulations. The results revealed that the constitutive model could predict the mechanical properties of 18Ni300 in a dynamic state. The build direction had little influence on the mechanical properties in a static state, but there was a significant difference in the dynamic state. The difference in the dynamic compressive yield strength of the 18Ni300 material manufactured by SLM with two build directions was 9.8%. The SLM process can be improved to produce 18Ni300 with uniform mechanical properties by studying the reasons for this difference.

4.
Materials (Basel) ; 17(17)2024 Aug 30.
Article de Anglais | MEDLINE | ID: mdl-39274705

RÉSUMÉ

Laser-based powder bed fusion of metals (PBF-LB/M) is a widely used additive manufacturing process characterized by a high degree of design freedom. As a result, near fully dense complex components can be produced in near-net shape by PBF-LB/M. Recently, the PBF-LB/M process was found to be a promising candidate to overcome challenges related to conventional machining of the Fe64Ni36 Invar alloy being well known for a low coefficient of thermal expansion (CTE). In this context, a correlation between process-induced porosity and the CTE was presumed in several studies. Therefore, the present study investigates whether the unique thermal properties of the PBF-LB/M-processed Fe64Ni36 Invar alloy can be tailored by the selective integration of defects. For this purpose, a full-factorial experimental design, representing by far the largest processing window in the literature, was considered, correlating the thermal expansion properties with porosity and hardness. Furthermore, the microstructure and mechanical properties were investigated by scanning electron microscopy and quasi-static tensile tests. Results by means of statistical analysis reveal that a systematic correlation between porosity and CTE properties could not be determined. However, by using specific process parameter combinations, the microstructure changed from a fine-grained fan-like structure to a coarse columnar structure.

5.
Materials (Basel) ; 17(17)2024 Aug 31.
Article de Anglais | MEDLINE | ID: mdl-39274721

RÉSUMÉ

Organic phase change material is an ideal solution to solve the heat dissipation problem of electronic devices. However, its low thermal conductivity limits its application. To solve this problem, a new porous aluminum skeleton/paraffin composite phase change material (AS-PCM) was prepared. The effects of porosity and porous aluminum skeletons on temperature control performance were explored. The experimental results show that the addition of AS significantly improves the thermal conductivity of organic PCM, and the thermal conductivity of AS-PCM is 32.3-59.6 times higher than that of pure paraffin. In addition, the temperature difference in AS-PCM with 75% porosity is 1-2 °C lower than that of AS-PCM with 85%, and 5-8 °C lower than that of AS-PCM with 95% porosity. The skeleton structure has an impact on the temperature control performance. The Mcc porous aluminum skeleton/paraffin composite phase change material (MAS-PCM) yields the best thermal performance compared with the Fcc porous aluminum skeleton/paraffin composite phase change material (FAS-PCM). The temperature control time of the MAS-PCM heat sink is increased by 5.3-50.8% relative to the FAS-PCM heat sink. The research results provide a novel approach for improving the thermal conductivity of PCMs.

6.
Materials (Basel) ; 17(17)2024 Sep 09.
Article de Anglais | MEDLINE | ID: mdl-39274822

RÉSUMÉ

Topology optimization enables the design of advanced architected materials with tailored mechanical properties and optimal material distribution. This method can result in the production of parts with uniform mechanical properties, reducing anisotropy effects and addressing a critical challenge in metal additive manufacturing (AM). The current study aims to examine the micro-tensile response of Inconel 718 architected materials utilizing the Selective Laser Melting Technique. In this context, three novel architected materials, i.e., Octet, Schwarz Diamond (SD), and hybrid Schwarz Diamond and Face Centered Cubic (FCC), were tested in three different relative densities. The specimens were then subjected to uniaxial quasi-static tensile tests to determine their key mechanical properties, including elastic modulus, yield strength, and ultimate tensile strength (UTS), as well as the scaling laws describing the tensile response of each architected material. In situ Scanning Electron Microscopy (SEM) has been performed to observe the structure and grain morphology of the 3D printed specimens along with the phase transitions (elastic, plastic), the crack propagation, and the overall failure mechanisms. The results highlight the effect of the lattice type and the relative density on the mechanical properties of architected materials. Topologically optimized structures presented a 70-80% reduction in overall strength, while the SD and SD&FCC structures presented higher stretching dominated behavior, which was also verified by the n-value range (1-2) extracted from the identification of the scaling laws.

7.
Sensors (Basel) ; 24(17)2024 Sep 09.
Article de Anglais | MEDLINE | ID: mdl-39275770

RÉSUMÉ

Additive manufacturing (AM) excels in engineering intricate shapes, pioneering functional components, and lightweight structures. Nevertheless, components fabricated through AM often manifest elevated residual stresses and a myriad of thermally induced micro-instabilities, including cracking, incomplete fusion, crazing, porosity, spheroidization, and inclusions. In response, this study proposed a sophisticated multi-sensing inspection system specifically tailored for the inspection of thermally induced micro-instabilities at the micro-nano scale. Simulation results substantiate that the modulation transfer function (MTF) values for each field of view in both visible and infrared optical channels surpass the benchmark of 0.3, ensuring imaging fidelity conducive to meticulous examination. Furthermore, the innovative system can discern and accurately capture data pertaining to thermally induced micro-instabilities across visible and infrared spectra, seamlessly integrating this information into a backend image processing system within operational parameters of a 380-450 mm distance and a 20-70 °C temperature range. Notably, the system's design is harmoniously aligned with the requisites of processing and assembly, heralding a significant advancement in bolstering the inspection effect of thermally induced micro-instabilities for the AM component.

8.
Materials (Basel) ; 17(18)2024 Sep 19.
Article de Anglais | MEDLINE | ID: mdl-39336345

RÉSUMÉ

Additive manufacturing from metal powders using selective laser melting technology is gaining increasing interest in various industries. The purpose of this study was to determine the effect of changes in process parameter values on the relative density, microstructure and mechanical properties of Ti-6Al-4V and Ti-6Al-7Nb alloy samples. The experiment was conducted in response to a noticeable gap in the research on the manufacturability of the Ti-6Al-7Nb alloy in SLM technology. This topic is significant given the growing interest in this alloy for biomedical applications. The results of this study indicate that by properly selecting the volumetric energy density (VED), the relative density of the material produced and the surface roughness of the components can be effectively influenced. Microstructural analyses revealed similar patterns in both alloys manufactured under similar conditions, characterized by columnar ß phase grains with needle-like α' phases. Increasing the VED increased the tensile strength of the fabricated Ti-6Al-4V alloy components, while the opposite effect was observed for components fabricated from Ti-6Al-7Nb alloy. At the same time, Ti-6Al-7Nb alloy parts featured higher elongation values, which is desirable from the perspective of biomedical applications.

9.
Article de Anglais | MEDLINE | ID: mdl-39300896

RÉSUMÉ

PURPOSE: The objective of this study was to assess the surface micro-roughness and abutment adaptation of selective laser melting (SLM) implant abutments in comparison to cast and machined implant abutments. METHODS: Forty abutment specimens were divided equally into four groups according to the fabrication technique as follows (n = 10), Machined Ti alloy abutments (Control), Cast CoCr abutments, SLM-CoCr abutments, and SLM-Ti alloy abutments. Forty internal connection implants (Ø 4.0 ×10 mm, Superline™, Dentium Co., Seoul, Korea) were mounted in clear acrylic resin. Fabricated abutments were assessed for surface micro-roughness using a 3D optical noncontact surface microscope. Vertical and horizontal adaptation of the abutment with implant interface was assessed by using Bruker micro-CT. Data was assessed using analysis of variance and Tukey post hoc comparison tests for all the variables except vertical misfit was assessed using Kruskal-Wallis test. Pearson correlation was used to assess dependence between independent variable (surface roughness) and dependent variables (Horizontal misfit and vertical misfit). RESULTS: SLM-Ti abutments showed significantly rougher surface (p < 0.05) among the study groups. While SLM-CoCr abutments were smoother than Cast abutments with mean Ra of 1.30 ± 0.11 and 1.58 ± 0.17 µm, respectively (p < 0.05). For abutment adaptation, SLM-Ti abutments showed the highest horizontal misfit among the groups (p < 0.05). While, SLM-CoCr abutments (29.24 ± 11.11 µm) showed comparable (p > 0.05) horizontal misfit results with Cast (26.08 ± 3.93 µm) and machined (26.45 ± 7.33 µm) abutments. Comparable (p > 0.05) vertical misfit values between Cast CoCr (487.01 ± 40.34 µm), SLM-CoCr (358.38 ± 114.93 µm) and SLM-Ti (299.85 ± 172.88 µm) abutments were observed. A positive correlation was found between the surface roughness of the mating surfaces and abutment adaptation. CONCLUSION: SLM CoCr abutments exhibited low roughness and comparable abutment adaptation (vertically and horizontally) than cast (control) abutments. Therefore, SLM CoCr abutments should be clinically investigated as potential implant abutments for clinical use.

10.
Biomimetics (Basel) ; 9(8)2024 Jul 29.
Article de Anglais | MEDLINE | ID: mdl-39194440

RÉSUMÉ

The interaction between oral bacteria and dental implant surfaces is a critical factor in the success and longevity of dental implants. With advancements in additive manufacturing technologies, selective laser melting (SLM) has emerged as a prominent method for producing titanium implants with highly controlled microstructures and porosities. These 3D printed titanium surfaces offer significant benefits, such as enhanced osseointegration and improved mechanical properties. However, the same surface features that promote bone cell attachment and proliferation may also provide favorable conditions for bacterial adhesion and biofilm formation. Understanding the dynamics of these interactions is essential for developing implant surfaces that can effectively resist bacterial colonization while promoting tissue integration. This narrative review explores the complex interplay between oral bacteria and SLM-produced titanium porous surfaces, examining current research findings and potential strategies for optimizing implant design to mitigate the risks of infection and ensure successful clinical outcomes.

11.
J Prosthodont ; 2024 Aug 08.
Article de Anglais | MEDLINE | ID: mdl-39118292

RÉSUMÉ

PURPOSE: To evaluate the seating accuracy of removable partial denture (RPD) frameworks fabricated by two digital workflows involving selective laser melting (SLM) in comparison to the conventional workflow. MATERIALS AND METHODS: A Kennedy class III modification 1 partially edentulous mandibular arch was used as a master model. Three RPD framework groups were included: (1) a conventional workflow group with conventional impression and casting (CC), (2) a partial digital workflow group with conventional impression and digital fabrication (CD), and (3) a complete digital workflow group with digital impression and digital fabrication (DD). A total of 10 frameworks were produced for each group. The marginal gaps at the occlusal rests, retention arms, and reciprocating arms were measured by a traveling microscope. The data were analyzed with the one-way analysis of variance test. RESULTS: At the framework level, the most superior fit was observed for the CD group (79.5 µm) followed by DD (85.3 µm) and CC (114.2 µm) groups. The CD and DD groups were significantly superior to CC (p < 0.001). This fit pattern was consistent for the retention and reciprocating arms, while the occlusal rest fit was similar among all the groups. CONCLUSIONS: The SLM frameworks had a promising seating accuracy in comparison to conventional frameworks. The type of impression, conventional or digital, did not affect the accuracy of SLM frameworks. The differences observed in the present study are likely to be of minimal clinical significance.

12.
Sci Rep ; 14(1): 18225, 2024 Aug 06.
Article de Anglais | MEDLINE | ID: mdl-39107387

RÉSUMÉ

Parts are often warped and deformed when they are molded using selective laser melting (SLM) technology. Thus, it is necessary to study the addition support modes of parts molded using SLM. Consequently, we designed dendritic, E-stage and conical supports, having different structural parameters and different partitions using Magics, and then, we analyzed their performances using the finite element software Abaqus. The structural parameters of the supports were optimized and finally tested using SLM molding technology. The maximum stress concentration was found for dendritic supports, followed by E-stage supports, and then conical supports. The stress concentration and deformation level of Scheme 2 were less than those of Scheme 1. The stress intensity and deformation levels for two partitions were less than those for three partitions. For parts molded by SLM, the deformation was maximum for conical supports, followed by dendritic supports, and then E-stage supports. When gradient supports of similar volumes were added, additional partitions did not effectively improve the molding quality. When supports of similar volumes were added, adding gradient supports did not effectively improve the molding quality. The results provide a basis for the application of SLM in molding high-precision parts.

13.
BMC Oral Health ; 24(1): 910, 2024 Aug 07.
Article de Anglais | MEDLINE | ID: mdl-39112988

RÉSUMÉ

BACKGROUND: There is insufficient evidence recommending a framework material and a CAD/CAM manufacturing technique for mandibular implant-supported prostheses. The study objective was to evaluate the clinical application of different materials and construction techniques used for mandibular All-on-4 prosthesis on circumferential peri-implant bony changes after 5 years. METHODS: Thirty-six male patients with all-on-4 mandibular implant-supported prostheses were recalled and divided into three groups. Group PK (patients with frameworks milled from PEEK blocks), Group PSM (patients with frameworks milled from soft metal blocks), and Group SLM (patients with frameworks constructed with additive manufacturing; selective laser melting). The circumferential bone level on all implant faces was assessed with a CBCT. Two-way repeated measures ANOVA was used to compare vertical bone loss (VBL) and horizontal bone loss (HBL) between different groups, implant positions, and observation times followed by Tukey's multiple comparisons. RESULTS: For all observation times, there was a significant difference in VBL between groups for both anterior and posterior implants (P < .001). For anterior implants, group PSM showed the lowest VBL while group PK showed the highest for anterior and posterior implants. For all groups, HBL significantly increased after 5 years for both anterior and posterior implants (P < .001). For anterior implants, group PSM showed the highest HBL. For posterior implants, group PK and SLM showed the highest. CONCLUSION: Within the study's limitations, mandibular implant-supported fixed frameworks fabricated with either milling from PEEK or soft metal blocks, or additive manufacturing (laser melting technology) exhibited significant vertical and horizontal bone height changes after 5 years. CLINICAL TRIAL REGISTRY NUMBER: (NCT06071689) (11/10/2023).


Sujet(s)
Résorption alvéolaire , Conception assistée par ordinateur , Prothèse dentaire implanto-portée , Mandibule , Humains , Mâle , Adulte d'âge moyen , Mandibule/imagerie diagnostique , Mandibule/chirurgie , Résorption alvéolaire/imagerie diagnostique , Tomodensitométrie à faisceau conique/méthodes , Conception de prothèse dentaire , Sujet âgé , Benzophénones , Adulte , Implants dentaires , Polymères
14.
Sensors (Basel) ; 24(15)2024 Jul 31.
Article de Anglais | MEDLINE | ID: mdl-39124003

RÉSUMÉ

This study investigates the methods for controlling porosity in thermal pipes manufactured using selective laser melting (SLM) technology. Experiments conducted include water permeability tests and surface roughness measurements, which are complemented by SEM image ML-based analysis for pore recognition. The results elucidate the impact of SLM printing parameters on water permeability. Specifically, an increase in hatch and point distances leads to a linear rise in permeability, while higher laser power diminishes permeability. Using machine learning (ML) techniques, precise pore identification on SEM images depicting surface microstructures of the samples is achieved. The average percentage of the surface area containing detected pores for microstructure samples printed with laser parameters (laser power (W) _ hatch distance (µm) _ point distance (µm)) 175_ 80_80 was found to be 5.2%, while for 225_120_120, it was 4.2%, and for 275_160_160, it was 3.8%. Pore recognition was conducted using the Haar feature-based method, and the optimal patch size was determined to be 36 pixels on monochrome images of microstructures with a magnification of 33×, which were acquired using a Leica S9 D microscope.

15.
Materials (Basel) ; 17(15)2024 Jul 26.
Article de Anglais | MEDLINE | ID: mdl-39124355

RÉSUMÉ

This paper presents novel configurations for additively manufactured lattice structures, including helical and elliptic designs, in addition to the pyramid base model. Functionally graded versions of the pyramid and elliptic lattice structures are developed by considering desirable relative densities in each layer. The lattice structures were manufactured using Ti-6Al-4V powder in a three-dimensional selective laser melting printer. The averaged porosities are 0.86, 0.91, 0.916, 0.93 and 0.74 for pyramid, functionally graded pyramid, elliptic, functionally graded elliptic and helical, respectively. The mechanical behavior of the lattice structures was characterized through compression tests using a universal testing machine and computationally analyzed using finite element code. The results indicate that the elliptic and functionally graded elliptic lattices have elastic moduli of 0.76 and 0.67 GPa, while the yield strengths are 41.32 and 32.24 MPa, respectively, in comparison to cancellous bone. Moreover, pyramid, functionally graded pyramid, and helical lattices show relatively lower elastic moduli of 0.57, 0.65 and 0.41 GPa and higher yield strengths of 54.1, 52.15 and 61.02 MPa, respectively. This could be an indication that they are fit for cortical bones. All samples have low elastic moduli coupled with high yield strengths. This could reduce or eliminate stress shielding, making them suitable for some load-bearing bio-inspired applications. A comparative study utilizing experimental and numerical models was conducted to evaluate the performance of the proposed designs.

16.
Materials (Basel) ; 17(15)2024 Jul 30.
Article de Anglais | MEDLINE | ID: mdl-39124419

RÉSUMÉ

Nowadays, H13 hot work steel is a commonly used hot work die material in the industry; however, its creep behavior for additively manufactured H13 steel parts has not been widely investigated. This research paper examines the impact of volumetric energy density (VED), a critical parameter in additive manufacturing (AM), and the effect of post heat-treatment nitrification on the creep behavior of H13 hot work tool steel, which is constructed through selective laser melting (SLM), which is a powder bed fusion process according to ISO/ASTM 52900:2021. The study utilizes nanoindentation tests to investigate the creep response and the associated parameters such as the steady-state creep strain rate. Measurements and observations taken during the holding phase offer a valuable understanding of the behavior of the studied material. The findings of this study highlight a substantial influence of both VED and nitrification on several factors including hardness, modulus of elasticity, indentation depth, and creep displacement. Interestingly, the creep strain rate appears to be largely unaltered by these parameters. The study concludes with the observation that the creep stress exponent (n) shows a decreasing trend with an increase in VED and the application of nitrification treatment.

17.
Materials (Basel) ; 17(15)2024 Aug 03.
Article de Anglais | MEDLINE | ID: mdl-39124514

RÉSUMÉ

Magnesium alloys, renowned for their lightweight yet high-strength characteristics, with exceptional mechanical properties, are highly coveted for numerous applications. The emergence of magnesium alloy additive manufacturing (Mg AM) has further propelled their popularity, offering advantages such as unparalleled precision, swift production rates, enhanced design freedom, and optimized material utilization. This technology holds immense potential in fabricating intricate geometries, complex internal structures, and performance-tailored microstructures, enabling groundbreaking applications. In this paper, we delve into the core processes and pivotal influencing factors of the current techniques employed in Mg AM, including selective laser melting (SLM), electron beam melting (EBM), wire arc additive manufacturing (WAAM), binder jetting (BJ), friction stir additive manufacturing (FSAM), and indirect additive manufacturing (I-AM). Laser powder bed fusion (LPBF) excels in precision but is limited by a low deposition rate and chamber size; WAAM offers cost-effectiveness, high efficiency, and scalability for large components; BJ enables precise material deposition for customized parts with environmental benefits; FSAM achieves fine grain sizes, low defect rates, and potential for precision products; and I-AM boasts a high build rate and industrial adaptability but is less studied recently. This paper attempts to explore the possibilities and challenges for future research in AM. Among them, two issues are how to mix different AM applications and how to use the integration of Internet technologies, machine learning, and process modeling with AM, which are innovative breakthroughs in AM.

18.
Materials (Basel) ; 17(14)2024 Jul 15.
Article de Anglais | MEDLINE | ID: mdl-39063786

RÉSUMÉ

The oxidation behaviour of iron-based 316L stainless steel was investigated in the temperature range of 700 to 1000 °C. The test specimens in the shape of plates were produced by selective laser melting. After fabrication, the samples were sandblasted and then annealed in air for different periods of time (0.5, 2, 8, 32 h). Under the influence of temperature and time, stainless steels tend to form an oxide layer. Scanning electron microscopy, energy dispersive analysis, and X-ray diffraction were employed to analyse the composition of this layer. Notably, a thin oxide layer primarily composed of (Fe-Cr) formed on the surface due to temperature effects. In addition, with increasing temperature (up to 1000 °C), the oxide of the main alloying elements, specifically Mn2(Fe-Cr)O4, appeared alongside the Fe-Cr oxide. Furthermore, the samples were subjected to conversion X-ray (CXMS) and conversion electron (CEMS) Mössbauer spectroscopy. CXMS revealed a singlet with a decreasing Mössbauer effect based on the surface metal oxide thickness. CEMS revealed the presence of Fe3+ in the surface layer (0.3 µm). Moreover, an interesting phenomenon occurred at higher temperature levels due to the inhomogeneously thick surface metal oxide layer and the tangential direction of the Mössbauer radiation towards the electron detector.

19.
Materials (Basel) ; 17(14)2024 Jul 18.
Article de Anglais | MEDLINE | ID: mdl-39063860

RÉSUMÉ

The detection of defects in aluminium alloys using eddy current testing (ECT) can be restricted by higher electrical conductivity. Considering the occurrence of discontinuities during the selective laser melting (SLM) process, checking the ability of the ECT method for the mentioned purpose could bring simple and fast material identification. The research described here is focused on the application of three ECT probes with different frequency ranges (0.3-100 kHz overall) for the identification of artificial defects in SLM aluminium alloy AlSi10Mg. Standard penetration depth for the mentioned frequency range and identification abilities of used probes expressed through lift-off diagrams precede the main part of the research. Experimental specimens were designed in four groups to check the signal sensitivity to variations in the size and depth of cavities. The signal behavior was evaluated according to notch-type and hole-type artificial defects' presence on the surface of the material and spherical cavities in subsurface layers, filled and unfilled by unmolten powder. The maximal penetration depth of the identified defect, the smallest detectable notch-type and hole-type artificial defect, the main characteristics of signal curves based on defect properties and circumstances for distinguishing between the application of measurement regime were stated. These conclusions represent baselines for the creation of ECT methodology for the defectoscopy of evaluated material.

20.
Micromachines (Basel) ; 15(7)2024 Jul 07.
Article de Anglais | MEDLINE | ID: mdl-39064400

RÉSUMÉ

This paper address the performance optimization of the battery heat sink module by analyzing the lattice structure of the battery heat sink module through in-depth modeling and simulation, and combining the laser powder bed fusion (LPBF)-forming technology with mechanical and corrosion resistance experiments for a comprehensive study. It is found that the introduction of the lattice skeleton significantly improves the thermal conductivity of the phase change material (PCM), realizing the efficient distribution and fast transfer of heat in the system. At the same time, the lattice skeleton makes the heat distribution in the heat exchanger more uniform, improves the utilization rate of the PCM, and helps to maintain the stability of the cell temperature. In addition, the melting of PCM in the lattice heat exchanger is more uniform, thus maximizing its latent heat capacity. In summary, by optimizing the lattice structure and introducing the lattice skeleton, this study successfully improves the performance of the battery heat dissipation system, which provides a strong guarantee for the high efficiency and stable operation of the battery, and provides new ideas and references for the development of the battery heat dissipation technology.

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