The structural integrity of mechanical components is assessed by FBG sensors in many industrial fields. The FBG sensor has a relevant application at very high or low temperatures. To avoid the variability of the reflected spectrum and the mechanical properties degradation of the FBG sensor, metal coatings have been used to guarantee the grating's integrity in extreme temperature environments. Particularly, at high temperatures, Ni could be a suitable selection as a coating to improve the features of FBG sensors. Furthermore, it was demonstrated that Ni coating and high-temperature treatments can recover a broken, seemingly unusable sensor. In this work, two main objectives were pursued: first, the determination of the best operative parameters to achieve the most compact, adherent, and homogeneous coating; second, the correlation between the obtained morphology and structure and the FBG spectrum modification, once Ni was deposited on the FBG sensor. The Ni coating was deposited from aqueous solutions. By performing heat treatments of the Ni-coated FBG sensor, it was investigated how the wavelength (WL) varied as a function of temperature and how that variation was caused by the structural or dimensional change of the Ni coating.
FBG sensors are used in many scientific and industrial fields for assessing the structural integrity of mechanical components and in very high (above 600 °C) or very low (cryogenic) temperature applications. The main concerns with the use of such sensors in applications involving extreme temperatures are related partly to the instability of the reflected spectrum, which tends to dissolve into the noise floor, and partly to the degradation of the mechanical properties of the optical fiber, which tends to worsen the inherent brittleness. All of this raises the need for a robust nickel protective coating to ensure the grating's integrity in high-temperature environments. In addition, the inherent brittleness of fiber-optic gratings leaves one to wonder whether it is possible to recover a broken, seemingly unusable sensor. In this way, a single-peak commercial FBG was intentionally broken in the middle of the grating length and re-spliced, inducing a strongly asymmetric chirped-like spectrum; then, a nickel coating was electrodeposited on its surface. The most important outcome achieved by this work is the regeneration of a highly distorted reflected spectrum through three thermal cycles performed from room temperature up to 500, 750, and 800 °C, respectively. After reaching a temperature of at least 700 °C, the spectrum, which has been drastically altered by splicing, becomes stable and restores its single peak shape. A further stabilization cycle carried out at 800 °C for 80 min led to an estimation of the stabilizing time of the new single-peak reflected spectrum.
Use of fiber Bragg gratings (FBGs) to monitor high temperature (HT) applications is of great interest to the research community. Standard commercial FBGs can operate up to 600 ∘ C. For applications beyond that value, specific processing of the FBGs must be adopted to allow the grating not to deteriorate. The most common technique used to process FBGs for HT applications is the regeneration procedure (RP), which typically extends their use up to 1000 ∘ C. RP involves a long-term annealing of the FBGs, to be done at a temperature ranging from 550 to 950 ∘ C. As at that temperature, the original coating of the FBGs would burn out, they shall stay uncoated, and their brittleness is a serious concern to deal with. Depositing a metal coating on the FBGs prior to process them for RP offers an effective solution to provide them with the necessary mechanical strengthening. In this paper, a procedure to provide the FBG with a bimetallic coating made by copper and nickel electrodeposition (ED) is proposed, discussing issues related to the coating morphology, adherence to the fiber, and effects on the grating spectral response. To define the processing parameters of the proposed procedure, production tests were performed on dummy samples which were used for destructive SEM-EDS analysis. As a critical step, the proposed procedure was shown to necessitate a heat treatment after the nickel ED, to remove the absorbed hydrogen. The spectral response of the FBG samples was monitored along the various steps of the proposed procedure and, as a final proof test for adherence stability of the bimetallic coating, along a heating/cooling cycle from room temperature to 1010 ∘ C. The results suggest that, given the emergence of Kirkendall voids at the copper-nickel interface, occurring at the highest temperatures (700-1010 ∘ C), the bimetallic layer could be employed as FBG coating up to 700 ∘ C.
