Strong yet flexible ceramic aerogel.

Ceramic aerogels are highly efficient, lightweight, and chemically stable thermal insulation materials but their application is hindered by their brittleness and low strength. Flexible nanostructure-assembled compressible aerogels have been developed to overcome the brittleness but they still show low strength, leading to insufficient load-bearing capacity. Here we designed and fabricated a laminated SiC-SiOx nanowire aerogel that exhibits reversible compressibility, recoverable buckling deformation, ductile tensile deformation, and simultaneous high strength of up to an order of magnitude larger than other ceramic aerogels. The aerogel also shows good thermal stability ranging from -196 °C in liquid nitrogen to above 1200 °C in butane blow torch, and good thermal insulation performance with a thermal conductivity of 39.3 ± 0.4 mW m-1 K-1. These integrated properties make the aerogel a promising candidate for mechanically robust and highly efficient flexible thermal insulation materials.

Dynamic range expansion of spatial light modulators based on a module-nπ method.

It is known that the cumbersome 2π correction is needed in the traditional module-2π method (i.e., the phase wrapping method) due to the 2π deviation of the phase modulation depth of spatial light modulators (SLMs). To avoid the cumbersome 2π correction in the module-2π method, this paper proposes a module-n π method, and it can directly utilize any full-field phase modulation depth. First, for a Gaussian phase with a phase depth of 30 rad, wrapped by the module-3.6π, it is reconstructed with the root-mean-square (RMS) values of its phase response are 0.1006λ (for the Twyman-Green interferometer) and 0.1101λ (for the Shack-Hartmann wavefront sensor method), respectively, which proves that the monitoring accuracy is relatively consistent. Subsequently, some comparative experiments based on the traditional module-2π are performed. The experimental results show that the RMS values of its phase response are 0.8886λ (for a modulation depth of 11.3 rad) and 0.2261λ (for a modulation depth of 6.28 rad), respectively. All the results have proved that the SLM with a phase modulation depth exceeding 2π (e.g., 11.3 rad) has more prominent advantages. More specifically, increasing the SLM's phase modulation depth can effectively reduce the fringe orders of the wrapped patterns generated by the module-n π method. With the further reduction of the fringe orders, the influence of the fly-back zone error on the wavefront phase modulation is reduced, that is, the modulation accuracy is improved (the RMS values are reduced from 0.2261λ to 0.1006λ). Different from the traditional module-2π method, there is no need to consider the problems of the SLMs' over modulation or the insufficient modulation in the module-n π method. Furthermore, it avoids the cumbersome 2π correction process, which will make the use of the SLM more convenient.

Phase response measurement of spatial light modulators based on a Shack-Hartmann wavefront sensor.

It is known that the phase response of spatial light modulators (SLMs) measured by double-beam interferometers is sensitive to mechanical and environmental disturbances. This paper proposes a Shack-Hartmann wavefront sensor (SHWS) method to measure the phase response characteristics of the SLM. The results show that the phase modulation depth measured by the proposed method is 1.7581λ, and 1.7993λ by the Twyman-Green interferometer method. The difference in the phase modulation depth between the two methods is only 0.0412λ, and its relative error rate is 2.29%. It proves that the phase modulation accuracy obtained by the SHWS with lenslets of 73*73 used in this paper is equivalent to that of the Twyman-Green interferometer. Compared with the interferometer method, the SHWS method is simple, compact, and robust, has good real-time performance, and is relatively vibration insensitive. In the future, the SHWS method will play a more important role in the detection of the SLM's phase response.

Highly Stretchable, Crack-Insensitive and Compressible Ceramic Aerogel.

Ceramic aerogels are attractive candidates for high-temperature thermal insulation, catalysis support, and ultrafiltration materials, but their practical applications are usually limited by brittleness. Recently, reversible compressibility has been realized in flexible nanostructures-based ceramic aerogels. However, these modified aerogels still show fast and brittle fracture under tension. Herein, we demonstrate achieving reversible stretch and crack insensitivity in a highly compressible ceramic aerogel through engineering its microstructure by using curly SiC-SiOx bicrystal nanowire as the building blocks. The aerogel exhibits large-strain reversible stretch (20%) and good resistance to high-speed tensile fatigue test. Even for a prenotched sample, a reversible stretch at 10% strain is achieved, indicating good crack resistance. The aerogel also displays reversible compressibility up to 80% strain, ultralow thermal conductivity of 28.4 mW m-1 K-1, and excellent thermal stability even at temperatures as high as 1200 °C in butane blow torch or as low as -196 °C in liquid nitrogen. Our findings show that the attractive tensile properties arise from the deformation, interaction, and reorientation of the curly nanowires which could reduce stress concentration and suppress crack initiation and growth during tension. This study not only expands the applicability of ceramic aerogels to conditions involving complex dynamic stress under extreme temperature conditions but also benefits the design of other highly stretchable and crack-resistant porous ceramic materials for various applications.

Radiation Effects in the Crystalline-Amorphous SiOC Polymer-Derived Ceramics: Insights from Experiments and Molecular Dynamics Simulation.

Radiation-tolerant materials are in great demand for safe operation and advancement of nuclear and aerospace systems. Nanostructuring is a key strategy to improve the radiation tolerance of materials. SiOC polymer-derived ceramics (PDCs) are unique synthetic nanocomposites consisting of ß-SiC nanocrystals and turbostratic graphite distributed in amorphous SiOC matrix, which are "all-rounder" materials for many advanced structural and functional applications. Radiation effects in the crystalline-amorphous system have been investigated in detail by experiments and molecular dynamics (MD) simulations. The results indicate that the amorphous SiOC structure retains amorphous accompanied by redistribution of the Si-containing tetrahedra. The graphite is shown to amorphize more easily than ß-SiC nanocrystals under the same irradiation condition. The sample richer in oxygen, namely, containing more amorphous SiOC, shows less disordering of graphite, resulting from greater mitigation of radiation damage by the amorphous phase as efficient sinks. This study provides details of the microstructure evolution of SiOC PDCs under ion irradiation, as well as insights for the design and development of advanced ion damage-resistant materials.

Design and Fabrication of a MEMS Electromagnetic Swing-Type Actuator for Optical Switch.

A microelectromechanical systems system (MEMS) electromagnetic swing-type actuator is proposed for an optical fiber switch in this paper. The actuator has a compact size of 5.1 × 5.1 × 5.3 mm3, consisting of two stators, a swing disc (rotator), a rotating shaft, and protective covers. Multi-winding stators and a multipole rotator were adopted to increase the output torque of the actuator. The actuator's working principle and magnetic circuit were analyzed. The calculation results show that the actuator's output torque is decisive to the air gap's magnetic flux density between the stators and the swing disc. NiFe alloy magnetic cores were embedded into each winding center to increase the magnetic flux density. A special manufacturing process was developed for fabricating the stator windings on the ferrite substrate. Six copper windings and NiFe magnetic cores were electroplated onto the ferrite substrates. The corresponding six magnetic poles were configured to the SmCo permanent magnet on the swing disc. A magnetizing device with a particular size was designed and fabricated to magnetize the permanent magnet of the swing disc. The actuator prototype was fabricated, and the performance was tested. The results show that the actuator has a large output torque (40 µNm), fast response (5 ms), and a large swing angle (22°).

3D Printing of Highly Sensitive and Large-Measurement-Range Flexible Pressure Sensors with a Positive Piezoresistive Effect.

Piezoresistive composite-based flexible pressure sensors often suffer from a trade-off between the sensitivity and measurement range. Moreover, the sensitivity or measurement range is theoretically limited owing to the negative piezoresistive coefficient, resulting in resistance variation below 100%. Here, flexible pressure sensors were fabricated using the three-dimensional (3D) printing technique to improve both the sensitivity and sensing range through the positive piezoresistive effect. With the addition of carbon nanotubes (CNTs) and fumed silica nanoparticles (SiNPs) as a conductive filler and rheology modifier, respectively, the viscoelastic silicone rubber solution converted to a printable gel ink. Soft and porous composites (SPCs) were then directly printed in air at room temperature. The sensitivity and sensing range of the SPC-based pressure sensor can be simultaneously tuned by adjusting the conducting CNT and insulating SiNP contents. By optimizing the density of the CNT conductive network in the matrix, positive piezoresistive sensitivity (+0.096 kPa-1) and a large linear sensing range (0-175 kPa) were obtained. To demonstrate potential applications, the completely soft SPC-based sensor was successfully used in grasp sensing and gait monitoring systems. The 3D printed sensors were also assembled as a smart artificial sensory array to map the pressure distribution.

Phase curvature compensation in digital holographic microscopy based on phase gradient fitting and optimization.

We propose a numerical method for phase curvature compensation in digital holographic microscopy, in which the phase curvature is compensated for by subtracting a numerical phase mask from the distorted phase. The parameters of the phase mask are obtained based on phase gradient fitting and optimization, in which the initial mask parameters are obtained by fitting the phase gradient, and then more accurate mask parameters are determined using a spectrum energy search. The compensation can be executed in a hologram without extra devices or any prior knowledge of the setup and specimen. A computer simulation and experimental results demonstrated the feasibility of the proposed method.

Hybrid method for speckle noise reduction in digital holography.

In digital holography, the inherited speckle noise degrades imaging quality due to the coherent laser source. To overcome this problem, a hybrid method for speckle noise reduction is presented by combining a novel angular diversity approach with the block-matching and 3D filtering (BM3D) algorithm. A serial of holograms is first captured by the proposed recording approach, and then the image with high signal-to-noise ratio is obtained by averaging multiple reconstructed intensity images. Finally, the residual noise in the averaged image is further eliminated by the BM3D filtering algorithm. The speckle noise is significantly suppressed, and a nearly speckle-free image can be obtained. Experimental results demonstrate the effectiveness of the proposed method.

Recent Progress on Electromagnetic Field Measurement Based on Optical Sensors.

Electromagnetic field sensors are widely used in various areas. In recent years, great progress has been made in the optical sensing technique for electromagnetic field measurement, and varieties of corresponding sensors have been proposed. Types of magnetic field optical sensors were presented, including probes-based Faraday effect, magnetostrictive materials, and magnetic fluid. The sensing system-based Faraday effect is complex, and the sensors are mostly used in intensive magnetic field measurement. Magnetic field optical sensors based on magnetic fluid have high sensitivity compared to that based on magnetostrictive materials. Three types of electric field optical sensors are presented, including the sensor probes based on electric-optic crystal, piezoelectric materials, and electrostatic attraction. The majority of sensors are developed using the sensing scheme of combining the LiNbO3 crystal and optical fiber interferometer due to the good electro-optic properties of the crystal. The piezoelectric materials-based electric field sensors have simple structure and easy fabrication, but it is not suitable for weak electric field measurement. The sensing principle based on electrostatic attraction is less commonly-used sensing methods. This review aims at presenting the advances in optical sensing technology for electromagnetic field measurement, analyzing the principles of different types of sensors and discussing each advantage and disadvantage, as well as the future outlook on the performance improvement of sensors.

Coaxial Printing of Silicone Elastomer Composite Fibers for Stretchable and Wearable Piezoresistive Sensors.

Despite the tremendous efforts dedicated to developing various wearable piezoresistive sensors with sufficient stretchability and high sensitivity, challenges remain pertaining to fabrication scalability, cost, and efficiency. In this study, a facile, scalable, and low-cost coaxial printing strategy is employed to fabricate stretchable and flexible fibers with a core-sheath structure for wearable strain sensors. The highly viscous silica-modified silicone elastomer solution is used to print the insulating sheath layer, and the silicone elastomer solutions containing multi-walled carbon nanotubes (CNTs) are used as the core inks to print the conductive inner layer. With the addition of silica powders as viscosifiers, silica-filled silicone ink (sheath ink) converts to printable ink. The dimensions of the printed coaxial fibers can be flexibly controlled via adjusting the extrusion pressure of the inks. In addition, the electro-mechanical responses of the fiber-shaped strain sensors are investigated. The printed stretchable and wearable fiber-like CNT-based strain sensor exhibits outstanding sensitivities with gauge factors (GFs) of 1.4 to 2.5 × 106, a large stretchability of 150%, and excellent waterproof performance. Furthermore, the sensor can detect a strain of 0.1% and showed stable responses for over 15,000 cycles (high durability). The printed fiber-shaped sensor demonstrated capabilities of detecting and differentiating human joint movements and monitoring balloon inflation. These results obtained demonstrate that the one-step printed fiber-like strain sensors have potential applications in wearable devices, soft robotics, and electronic skins.

Highly Stretchable Core-Sheath Fibers via Wet-Spinning for Wearable Strain Sensors.

Lightweight, stretchable, and wearable strain sensors have recently been widely studied for the development of health monitoring systems, human-machine interfaces, and wearable devices. Herein, highly stretchable polymer elastomer-wrapped carbon nanocomposite piezoresistive core-sheath fibers are successfully prepared using a facile and scalable one-step coaxial wet-spinning assembly approach. The carbon nanotube-polymeric composite core of the stretchable fiber is surrounded by an insulating sheath, similar to conventional cables, and shows excellent electrical conductivity with a low percolation threshold (0.74 vol %). The core-sheath elastic fibers are used as wearable strain sensors, exhibiting ultra-high stretchability (above 300%), excellent stability (>10 000 cycles), fast response, low hysteresis, and good washability. Furthermore, the piezoresistive core-sheath fiber possesses bending-insensitiveness and negligible torsion-sensitive properties, and the strain sensing performance of piezoresistive fibers maintains a high degree of stability under harsh conditions. On the basis of this high level of performance, the fiber-shaped strain sensor can accurately detect both subtle and large-scale human movements by embedding it in gloves and garments or by directly attaching it to the skin. The current results indicate that the proposed stretchable strain sensor has many potential applications in health monitoring, human-machine interfaces, soft robotics, and wearable electronics.

Graphene-Based Polymer Bilayers with Superior Light-Driven Properties for Remote Construction of 3D Structures.

3D structure assembly in advanced functional materials is important for many areas of technology. Here, a new strategy exploits IR light-driven bilayer polymeric composites for autonomic origami assembly of 3D structures. The bilayer sheet comprises a passive layer of poly(dimethylsiloxane) (PDMS) and an active layer comprising reduced graphene oxides (RGOs), thermally expanding microspheres (TEMs), and PDMS. The corresponding fabrication method is versatile and simple. Owing to the large volume expansion of the TEMs, the two layers exhibit large differences in their coefficients of thermal expansion. The RGO-TEM-PDMS/PDMS bilayers can deflect toward the PDMS side upon IR irradiation via the cooperative effect of the photothermal effect of the RGOs and the expansion of the TEMs, and exhibit excellent light-driven, a large bending deformation, and rapid responsive properties. The proposed RGO-TEM-PDMS/PDMS composites with excellent light-driven bending properties are demonstrated as active hinges for building 3D geometries such as bidirectionally folded columns, boxes, pyramids, and cars. The folding angle (ranging from 0° to 180°) is well-controlled by tuning the active hinge length. Furthermore, the folded 3D architectures can permanently preserve the deformed shape without energy supply. The presented approach has potential in biomedical devices, aerospace applications, microfluidic devices, and 4D printing.

Digital holographic metrology based on multi-angle interferometry.

We propose a multi-angle interferometry method for digital holographic metrology. In an application of three-dimensional (3D) reconstruction, the hologram corresponding to a different illumination angle is recorded as the illumination angle with a single wavelength tilted at regular intervals by an electronically controlled rotating stage. A Fourier-transform-based axial depth scanning algorithm formed by the reconstructed phase is used to obtain the height point by point over the whole field of view. Hence, the 3D reconstruction can be obtained effectively; even the object has large depth discontinuities resulting from the difficulty of the phase unwrapping. Due to a monochrome source only being used, the method is available for objects with wavelength-dependent reflectivity and those that are free of chromatic aberration caused by the different wavelengths.

Multi-frequency fringe projection profilometry based on wavelet transform.

Based on wavelet transforms (WTs), an alternative multi-frequency fringe projection profilometry is described. Fringe patterns with multiple frequencies are projected onto an object and the reflected patterns are recorded digitally. Phase information for every pattern is calculated by identifying the ridge that appears in WT results. Distinct from the phase unwrapping process, a peak searching algorithm is applied to obtain object height from the phases of the different frequency for a single point on the object. Thus, objects with large discontinuities can be profiled. In comparing methods, the height profiles obtained from the WTs have lower noise and higher measurement accuracy. Although measuring times are similar, the proposed method offers greater reliability.

Multi-frequency color-marked fringe projection profilometry for fast 3D shape measurement of complex objects.

We propose a novel multi-frequency color-marked fringe projection profilometry approach to measure the 3D shape of objects with depth discontinuities. A digital micromirror device projector is used to project a color map consisting of a series of different-frequency color-marked fringe patterns onto the target object. We use a chromaticity curve to calculate the color change caused by the height of the object. The related algorithm to measure the height is also described in this paper. To improve the measurement accuracy, a chromaticity curve correction method is presented. This correction method greatly reduces the influence of color fluctuations and measurement error on the chromaticity curve and the calculation of the object height. The simulation and experimental results validate the utility of our method. Our method avoids the conventional phase shifting and unwrapping process, as well as the independent calculation of the object height required by existing techniques. Thus, it can be used to measure complex and dynamic objects with depth discontinuities. These advantages are particularly promising for industrial applications.

The application of multi-frequency fringe projection profilometry on the measurement of biological tissues.

A volume of research has been performed on the optical surface profilometry in the field of biomedicine and the optical system with the phase-measuring method becomes the main emphasis of the research. In this research, a brand new fringe projection profilometry with multiple frequencies is described for measuring the biological tissue. A pork liver, as an object, is regarded as a human organ and a DMD projector is used to generate the multi-frequency fringe patterns. The wrapped phase maps are obtained by means of the five-step phase shifting method and calculated via a peak searching algorithm in which the process of measuring the point on the surface of the object is independent so that the step of unwrapping the phase can be avoided. The final results given are acceptable which confirm this method and suggest its enormous potential for the biomedical measurements.

Recovery of absolute height from wrapped phase maps for fringe projection profilometry.

A novel multi-frequency fringe projection profilometry is presented in this paper. Fringe patterns with multiple frequencies are projected onto an object by a digital micro-mirror device projector. The approach involves an improved Fourier transform profilometry method with an additional π phase shifting stage and hence the acquisition of two source images. A peak searching algorithm is then employed to obtain the real height profile of the object together with a mathematical proof of this algorithm. In our method, the height of each point on the object is measured independently and the phase unwrapping procedure is avoided, enabling the measurement of objects with large depth discontinuities, where the phase unwrapping is difficult. The measurement result is given to validate the method in the paper. Our technique has great potential in industrial applications where the measurement of objects with complex shape and large discontinuities is needed.

Extreme strain rate and temperature dependence of the mechanical properties of nano silicon nitride thin layers in a basal plane under tension: a molecular dynamics study.

Molecular dynamics simulations are performed to clarify the extreme strain rate and temperature dependence of the mechanical behaviors of nano silicon nitride thin layers in a basal plane under tension. It is found that fracture stresses show almost no change with increasing strain rate. However, fracture strains decrease gradually due to the appearance of additional N(2c)-Si bond breaking defects in the deformation process. With increasing loading temperature, there is a noticeable drop in fracture stress and fracture strain. In the low temperature range, roughness phases can be observed owing to a combination of factors such as configuration evolution and energy change.

Investigation of the nanomechanical properties of ß-Si3N4 nanowires under three-point bending via molecular dynamics simulation.

The nanowire with an aspect ratio of 3 : 1 possesses a higher bending stress of 15.85 GPa. It can be observed that the initial Si-Si bond and N atom defects with a coordination number of 2, subsequently evolving to 0 and 1, with Si evolving from 5 to 6 and 7, are mainly responsible for the final fracture.