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Materials (Basel) ; 14(2)2021 Jan 09.
Artigo em Inglês | MEDLINE | ID: mdl-33435447


A graphene oxide aerogel (GOA) was formed inside a melamine sponge (MS) framework. After reduction with hydrazine at 60 °C, the electrical conductive nitrogen-enriched rGOA-MS composite material with a specific density of 20.1 mg/cm3 was used to fabricate an electrode, which proved to be a promising electrocatalyst for the oxygen reduction reaction. The rGOA-MS composite material was characterized by elemental analysis, scanning electron microscopy, X-ray photoelectron spectroscopy, and Raman spectroscopy. It was found that nitrogen in the material is presented by different types with the maximum concentration of pyrrole-like nitrogen. By using Raman scattering it was established that the rGOA component of the material is graphene-like carbon with an average size of the sp2-domains of 5.7 nm. This explains a quite high conductivity of the composite obtained.

ACS Appl Mater Interfaces ; 11(35): 32517-32522, 2019 Sep 04.
Artigo em Inglês | MEDLINE | ID: mdl-31408314


Polytetrafluoroethylene-based aerogel was synthesized for the first time. Graphene oxide was used as a binder. After reduction with hydrazine and annealing at 370 °C, the aerogel with a density of 29 ± 2 mg/cm3 became superhydrophobic. The aerogel was characterized by IR spectroscopy, scanning electron microscopy, and X-ray photoelectron spectroscopy. The sorption capacity of the aerogel for seven solvents and its sorption recyclability for hexane were measured.