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Dent Mater J ; 2021 Oct 01.
Artigo em Inglês | MEDLINE | ID: mdl-34602588


This study aimed to evaluate the pulpal responses of monkey's pulp after direct pulp capping (DPC) with the novel mineral trioxide aggregate containing phosphorylated pullulan-based material (MTAPPL). Seventy-two teeth were randomly divided into four groups: MTAPPL; Nex-Cem MTA (NX); TheraCal LC (TH); and Dycal (DY). Histopathological changes in the pulps were observed at days 3, 7 and 70. On day 3, mild inflammatory responses were observed in the MTAPPL, no to moderate inflammatory responses in the TH, whereas moderate inflammatory responses in the NX and DY. No mineralized tissue formation (MTF) was observed in all groups. On day 7, no or mild inflammatory responses were observed in all groups. Initial MTF was observed except for DY. No inflammation with complete MTF including presence of odontoblast-like cells was observed in the MTAPPL, NX and TH groups at day 70. These findings indicate that MTAPPL could be an efficient DPC material.

Dent Mater ; 33(8): 895-903, 2017 08.
Artigo em Inglês | MEDLINE | ID: mdl-28552335


OBJECTIVES: To evaluate the influence of different air-blowing durations on the micro-tensile bond strength (µTBS) of five current one-step adhesive systems to dentin. METHODS: One hundred and five caries-free human molars and five current one-step adhesive systems were used: ABU (All Bond Universal, Bisco, Inc.), CUB (CLEARFIL™ Universal Bond, Kuraray), GPB (G-Premio BOND, GC), OBA (OptiBond All-in-one, Kerr) and SBU (Scotchbond Universal, 3M ESPE). The adhesives were applied to 600 SiC paper-flat dentin surfaces according to each manufacturer's instructions and were air-dried with standard, oil-free air pressure of 0.25MPa for either 0s, 5s, 15s or 30s before light-curing. Bond strength to dentin was determined by using µTBS test after 24h of water storage. The fracture pattern on the dentin surface was analyzed by SEM. The resin-dentin interface of untested specimens was visualized by panoramic SEM image. Data from µTBS were analyzed using two-way ANOVA (adhesive vs. air-blowing time), and Games-Howell (a=0.05). RESULTS: Two-way ANOVA revealed a significant effect of materials (p=0.000) and air-blowing time (p=0.000) on bond strength to dentin. The interaction between factors was also significantly different (p=0.000). Maximum bond strength for each system were recorded, OBA/15s (76.34±19.15MPa), SBU/15s (75.18±12.83MPa), CUB/15s (68.23±16.36MPa), GPB/30s (55.82±12.99MPa) and ABU/15s (44.75±8.95MPa). The maximum bond strength of OBA and SUB were significantly higher than that of GPB and ABU (p<0.05). SIGNIFICANCE: The bond strength of the current one-step adhesive systems is material-dependent (p=0.000), and was influenced by air-blowing duration (p=0.000). For the current one-step adhesive systems, higher bond strengths could be achieved with prolonged air-blowing duration between 15-30s.

Luzes de Cura Dentária , Colagem Dentária , Dentina , Adesivos , Resinas Compostas , Cimentos Dentários , Adesivos Dentinários , Humanos , Teste de Materiais , Cimentos de Resina , Resistência à Tração
Dent Mater J ; 35(3): 386-91, 2016.
Artigo em Inglês | MEDLINE | ID: mdl-27251993


The purpose of this study was to compare the micro-tensile bond strength (µTBS) of three resin core composites to dentin and to examine the bonded interface of the composites. One experimental TDK-03(TD) and, two commercial, DC core Automix One (DC) and Unifil core EM(UN) were used. Flat dentin surfaces of human molars were exposed using #600 SiC paper and bonded with the respective adhesive of each system. After bonding, the composites were built up on the surfaces and cured under two conditions: "light condition" or "dark condition". µTBSs (MPa) in the light condition were: TD; 60.02±17.08, DC; 38.21±13.70, and UN; 29.50±9.71; in the dark condition: TD; 54.62±17.11, DC; 8.40±4.81, and UN; 9.47±6.56. Dark curing negatively affected the bond strength of the two commercial resin-core materials. The experimental material was not affected by the curing conditions.

Colagem Dentária , Cimentos Dentários , Adesivos Dentinários , Resinas Compostas , Dentina , Humanos , Teste de Materiais , Cimentos de Resina , Resistência à Tração , Tato
Dent Mater J ; 34(1): 61-9, 2015.
Artigo em Inglês | MEDLINE | ID: mdl-25748460


The purpose of this study was to evaluate the microtensile bond strength (µTBS) of a newly developed resin cement, ECD-89 (ECD, Tokuyama Dental, Tokyo, Japan) to dentin and to observe the interfacial micromorphology by comparing with two commercial resin cements, Multilink Automix (MA, Ivoclar Vivadent AG, Schaan, Liechtenstein) and Panavia F2.0 (PF, Kuraray Noritake Dental, Tokyo, Japan). Flat dentin surfaces of human third molars were exposed using #600 SiC. After application of primer and cement to the dentin surface, each cement was applied and cured with light (light condition) or without light (dark condition). The teeth were sectioned to obtain beams (1 mm×1 mm) after 24 h of water storage. The mean bond strengths and SDs (MPa) were: ECD: 68.6±14.9, MA: 39.2±18.9, PF: 39.4±18.5 and ECD: 54.5±22.4, MA: 36.7±15.6, PF: 13.4±4.46 when cured in light and dark condition, respectively. In both conditions, ECD-89 showed statistically higher µTBS than the others.

Adesivos Dentinários/química , Cimentos de Resina/química , Humanos , Técnicas In Vitro , Teste de Materiais , Dente Serotino , Compostos de Organossilício/química , Propriedades de Superfície , Resistência à Tração