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1.
Chemistry ; 14(29): 8972-9, 2008.
Artigo em Inglês | MEDLINE | ID: mdl-18696525

RESUMO

We report a series of [2]borametallocenophanes of Ti, Zr, and Hf with various ligand systems. The ligands have been synthesized in high yields starting from 1,2-dibromo-1,2-bis(dimethylamino)diborane(4) upon reaction with Na[C5H5] and Li[C13H9], respectively. All compounds were fully characterized by multinuclear NMR spectroscopy and, for selected examples, by X-ray analysis.

2.
Inorg Chem ; 45(14): 5275-7, 2006 Jul 10.
Artigo em Inglês | MEDLINE | ID: mdl-16813387

RESUMO

In the present paper, we describe the first structural characterization of cymantrenyl(dihalo)borane and report on its use for the synthesis of novel cymantrenylboryl complexes.

3.
Chem Commun (Camb) ; (18): 2344-5, 2003 Sep 21.
Artigo em Inglês | MEDLINE | ID: mdl-14518906

RESUMO

Di(p-tolyl)diazomethane reacts with the tripyrrinate TrpyPdOAc(F) 1 after activation with NaBAr(F) to yield the first stable Pd(II) complex 2 of a non-Arduengo type carbene ligand, which could be characterised by X-ray crystallography.

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