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Four process-related potential new impurities in ticagrelor: Identification, isolation, characterization using HPLC, LC/ESI-MS(n), NMR and their synthesis.
Kumar, Neeraj; Devineni, Subba Rao; Gajjala, Prasad Reddy; Gupta, Dharmendra Kumar; Bhat, Sandesh; Kumar, Rajesh; Dubey, Shailendra Kumar; Kumar, Pramod.
Affiliation
  • Kumar N; Microlabs Ltd., Chemical Research Department, API R&D Centre, Bommasandra-Jigani Link Road, KIADB INDL Area, Bommasandra, Bangalore 560105, Karnataka, India.
  • Devineni SR; Microlabs Ltd., Chemical Research Department, API R&D Centre, Bommasandra-Jigani Link Road, KIADB INDL Area, Bommasandra, Bangalore 560105, Karnataka, India.
  • Gajjala PR; Microlabs Ltd., Chemical Research Department, API R&D Centre, Bommasandra-Jigani Link Road, KIADB INDL Area, Bommasandra, Bangalore 560105, Karnataka, India.
  • Gupta DK; Microlabs Ltd., Chemical Research Department, API R&D Centre, Bommasandra-Jigani Link Road, KIADB INDL Area, Bommasandra, Bangalore 560105, Karnataka, India.
  • Bhat S; Microlabs Ltd., Chemical Research Department, API R&D Centre, Bommasandra-Jigani Link Road, KIADB INDL Area, Bommasandra, Bangalore 560105, Karnataka, India.
  • Kumar R; Microlabs Ltd., Analytical Research Department, API R&D Centre, Bommasandra-Jigani Link Road, KIADB INDL Area, Bommasandra, Bangalore 560105, Karnataka, India.
  • Dubey SK; Microlabs Ltd., Chemical Research Department, API R&D Centre, Bommasandra-Jigani Link Road, KIADB INDL Area, Bommasandra, Bangalore 560105, Karnataka, India.
  • Kumar P; Microlabs Ltd., Chemical Research Department, API R&D Centre, Bommasandra-Jigani Link Road, KIADB INDL Area, Bommasandra, Bangalore 560105, Karnataka, India. Electronic address: pramodkumar@microlabs.in.
J Pharm Biomed Anal ; 120: 248-60, 2016 Feb 20.
Article in En | MEDLINE | ID: mdl-26760243
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Full text: 1 Collection: 01-internacional Database: MEDLINE Main subject: Magnetic Resonance Spectroscopy / Adenosine / Drug Contamination / Spectrometry, Mass, Electrospray Ionization / Tandem Mass Spectrometry Type of study: Diagnostic_studies Language: En Journal: J Pharm Biomed Anal Year: 2016 Document type: Article Affiliation country: Country of publication:
Fulltext
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Full text: 1 Collection: 01-internacional Database: MEDLINE Main subject: Magnetic Resonance Spectroscopy / Adenosine / Drug Contamination / Spectrometry, Mass, Electrospray Ionization / Tandem Mass Spectrometry Type of study: Diagnostic_studies Language: En Journal: J Pharm Biomed Anal Year: 2016 Document type: Article Affiliation country: Country of publication: