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Construction of Multifunctional 3-Amino-2-carbamimidoylacrylamides and Their Crystalline Channel-Type Inclusion Complexes.
Wang, Jinjin; Liu, Jiyong; Ding, Hualong; Wang, Jing; Lu, Ping; Wang, Yanguang.
Affiliation
  • Wang J; Department of Chemistry, Zhejiang University, Hangzhou 310027, P. R. China.
  • Liu J; Department of Chemistry, Zhejiang University, Hangzhou 310027, P. R. China.
  • Ding H; Department of Chemistry, Zhejiang University, Hangzhou 310027, P. R. China.
  • Wang J; Department of Chemistry, Zhejiang University, Hangzhou 310027, P. R. China.
  • Lu P; Department of Chemistry, Zhejiang University, Hangzhou 310027, P. R. China.
  • Wang Y; Department of Chemistry, Zhejiang University, Hangzhou 310027, P. R. China.
J Org Chem ; 80(11): 5842-50, 2015 Jun 05.
Article in En | MEDLINE | ID: mdl-25974094
ABSTRACT
3-Amino-2-carbamimidoylacrylamides were efficiently prepared via a copper(I)-catalyzed three-component reaction of sulfonylazides, propriolamides, and amidines. The synthesized compounds provided three kinds of crystalline structures based on the position of halogen. Two of them presented channel-type inclusion complexes with ethyl acetate through intermolecular hydrogen bonding, intermolecular C-H···π and π-π interactions, and van der Waals forces.
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Full text: 1 Collection: 01-internacional Database: MEDLINE Language: En Journal: J Org Chem Year: 2015 Document type: Article
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Full text: 1 Collection: 01-internacional Database: MEDLINE Language: En Journal: J Org Chem Year: 2015 Document type: Article