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Unusual (+/-)-electrospray ionization induced fragmentation: Structural elucidation of an in-process synthetic intermediate of doravirine (MK-1439) using liquid chromatography/high-resolution tandem mass spectrometry and two-dimensional nuclear magnetic resonance.
Sheng, Huaming; Lexa, Katrina W; Zhang, Li-Kang; Yang, Rong-Sheng; Wright, Timothy J; Sherry, Benjamin D; Helmy, Roy; Martin, Gary E.
Affiliation
  • Sheng H; Analytical Research & Development, Merck Research Laboratories, Rahway, NJ, 07065, USA.
  • Lexa KW; Process Research & Development, Merck Research Laboratories, Rahway, NJ, 07065, USA.
  • Zhang LK; Analytical Research & Development, Merck Research Laboratories, Rahway, NJ, 07065, USA.
  • Yang RS; Analytical Research & Development, Merck Research Laboratories, Rahway, NJ, 07065, USA.
  • Wright TJ; Chemical Engineering Research & Development, Merck Research Laboratories, Rahway, NJ, 07065, USA.
  • Sherry BD; Process Research & Development, Merck Research Laboratories, Rahway, NJ, 07065, USA.
  • Helmy R; Analytical Sciences, Merck Research Laboratories, Rahway, NJ, 07065, USA.
  • Martin GE; Analytical Research & Development, Merck Research Laboratories, Rahway, NJ, 07065, USA.
Rapid Commun Mass Spectrom ; 31(8): 719-727, 2017 Apr 30.
Article in En | MEDLINE | ID: mdl-28171682

Full text: 1 Collection: 01-internacional Database: MEDLINE Language: En Journal: Rapid Commun Mass Spectrom Year: 2017 Document type: Article Affiliation country: United States Country of publication: United kingdom

Full text: 1 Collection: 01-internacional Database: MEDLINE Language: En Journal: Rapid Commun Mass Spectrom Year: 2017 Document type: Article Affiliation country: United States Country of publication: United kingdom