Preparation of enantiopure methionine, arginine, tryptophan, and proline benzyl esters in green ethers by Fischer-Speier reaction.

Bolchi, Cristiano; Bavo, Francesco; Regazzoni, Luca; Pallavicini, Marco

Bolchi, Cristiano; Bavo, Francesco; Regazzoni, Luca; Pallavicini, Marco.

Affiliation

Bolchi C; Dipartimento di Scienze Farmaceutiche, Sezione "Pietro Pratesi", Università degli Studi di Milano, via Mangiagalli 25, 20133, Milan, Italy. cristiano.bolchi@unimi.it.
Bavo F; Dipartimento di Scienze Farmaceutiche, Sezione "Pietro Pratesi", Università degli Studi di Milano, via Mangiagalli 25, 20133, Milan, Italy.
Regazzoni L; Dipartimento di Scienze Farmaceutiche, Sezione "Pietro Pratesi", Università degli Studi di Milano, via Mangiagalli 25, 20133, Milan, Italy.
Pallavicini M; Dipartimento di Scienze Farmaceutiche, Sezione "Pietro Pratesi", Università degli Studi di Milano, via Mangiagalli 25, 20133, Milan, Italy.

Amino Acids ; 50(9): 1261-1268, 2018 Sep.

Article in En | MEDLINE | ID: mdl-29876689

Subject(s)

Arginine/chemistry; Benzyl Compounds/chemistry; Esters/chemistry; Ethers/chemistry; Methionine/chemistry; Proline/analogs & derivatives; Proline/chemistry; Tryptophan/chemistry; Chromatography, High Pressure Liquid; Esterification; Hazardous Substances; Magnetic Resonance Imaging; Solubility; Solvents/adverse effects

Key words

Amino acid benzyl ester; CPME; Chiral HPLC; Me-THF; Mosher's acid; Racemization; TAME; Water azeotrope

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Full text: 1 Collection: 01-internacional Database: MEDLINE Main subject: Arginine / Tryptophan / Benzyl Compounds / Proline / Esters / Ethers / Methionine Type of study: Risk_factors_studies Language: En Journal: Amino Acids Journal subject: BIOQUIMICA Year: 2018 Document type: Article Affiliation country: Italy Country of publication: Austria

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