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K2S2O8-HFIP synergistically promoted para-selective sp3 C-H bond diarylation of glycine esters.
Xu, Qingfeng; Li, Bang; Ma, Yujie; Sun, Fei; Gao, Yanan; Ye, Na.
Affiliation
  • Xu Q; Jiangsu Key Laboratory of Neuropsychiatric Diseases and College of Pharmaceutical Sciences, Soochow University, Suzhou, Jiangsu 215123, China. yena@suda.edu.cn.
  • Li B; Jiangsu Key Laboratory of Neuropsychiatric Diseases and College of Pharmaceutical Sciences, Soochow University, Suzhou, Jiangsu 215123, China. yena@suda.edu.cn.
  • Ma Y; Jiangsu Key Laboratory of Neuropsychiatric Diseases and College of Pharmaceutical Sciences, Soochow University, Suzhou, Jiangsu 215123, China. yena@suda.edu.cn.
  • Sun F; Jiangsu Key Laboratory of Neuropsychiatric Diseases and College of Pharmaceutical Sciences, Soochow University, Suzhou, Jiangsu 215123, China. yena@suda.edu.cn.
  • Gao Y; Jiangsu Key Laboratory of Neuropsychiatric Diseases and College of Pharmaceutical Sciences, Soochow University, Suzhou, Jiangsu 215123, China. yena@suda.edu.cn.
  • Ye N; Jiangsu Key Laboratory of Neuropsychiatric Diseases and College of Pharmaceutical Sciences, Soochow University, Suzhou, Jiangsu 215123, China. yena@suda.edu.cn.
Org Biomol Chem ; 18(4): 666-670, 2020 01 28.
Article in En | MEDLINE | ID: mdl-31894805
ABSTRACT
A metal-free K2S2O8-HFIP synergistically promoted double Friedel-Crafts alkylation between a glycine derivative and N-substituted aniline was developed to efficiently synthesize diarylmethane derivatives with high para-selectivity. The reaction proceeded smoothly in the absence of any metal and ligand, and exhibited a good tolerance of functional groups.
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Full text: 1 Collection: 01-internacional Database: MEDLINE Main subject: Sulfates / Potassium Compounds / Propanols / Esters / Glycine Language: En Journal: Org Biomol Chem Journal subject: BIOQUIMICA / QUIMICA Year: 2020 Document type: Article Affiliation country: China
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Full text: 1 Collection: 01-internacional Database: MEDLINE Main subject: Sulfates / Potassium Compounds / Propanols / Esters / Glycine Language: En Journal: Org Biomol Chem Journal subject: BIOQUIMICA / QUIMICA Year: 2020 Document type: Article Affiliation country: China