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20 µs-resolved high-throughput X-ray photon correlation spectroscopy on a 500k pixel detector enabled by data-management workflow.
Zhang, Qingteng; Dufresne, Eric M; Nakaye, Yasukazu; Jemian, Pete R; Sakumura, Takuto; Sakuma, Yasutaka; Ferrara, Joseph D; Maj, Piotr; Hassan, Asra; Bahadur, Divya; Ramakrishnan, Subramanian; Khan, Faisal; Veseli, Sinisa; Sandy, Alec R; Schwarz, Nicholas; Narayanan, Suresh.
Affiliation
  • Zhang Q; X-ray Science Division, Argonne National Laboratory, 9700 South Cass Avenue, Lemont, IL 60439, USA.
  • Dufresne EM; X-ray Science Division, Argonne National Laboratory, 9700 South Cass Avenue, Lemont, IL 60439, USA.
  • Nakaye Y; XRD Design and Engineering Department, Rigaku Corporation, 3-9-12 Matsubara-cho, Akishima-shi, Tokyo, Japan.
  • Jemian PR; X-ray Science Division, Argonne National Laboratory, 9700 South Cass Avenue, Lemont, IL 60439, USA.
  • Sakumura T; XRD Design and Engineering Department, Rigaku Corporation, 3-9-12 Matsubara-cho, Akishima-shi, Tokyo, Japan.
  • Sakuma Y; XRD Design and Engineering Department, Rigaku Corporation, 3-9-12 Matsubara-cho, Akishima-shi, Tokyo, Japan.
  • Ferrara JD; XRD Design and Engineering Department, Rigaku Corporation, 3-9-12 Matsubara-cho, Akishima-shi, Tokyo, Japan.
  • Maj P; AGH University of Science and Technology, av. Mickiewicza 30, Krakow 30-059, Poland.
  • Hassan A; Chemical and Biomedical Engineering, FAMU-FSU College of Engineering, Tallahassee, FL 32310, USA.
  • Bahadur D; Chemical and Biomedical Engineering, FAMU-FSU College of Engineering, Tallahassee, FL 32310, USA.
  • Ramakrishnan S; Chemical and Biomedical Engineering, FAMU-FSU College of Engineering, Tallahassee, FL 32310, USA.
  • Khan F; X-ray Science Division, Argonne National Laboratory, 9700 South Cass Avenue, Lemont, IL 60439, USA.
  • Veseli S; X-ray Science Division, Argonne National Laboratory, 9700 South Cass Avenue, Lemont, IL 60439, USA.
  • Sandy AR; X-ray Science Division, Argonne National Laboratory, 9700 South Cass Avenue, Lemont, IL 60439, USA.
  • Schwarz N; X-ray Science Division, Argonne National Laboratory, 9700 South Cass Avenue, Lemont, IL 60439, USA.
  • Narayanan S; X-ray Science Division, Argonne National Laboratory, 9700 South Cass Avenue, Lemont, IL 60439, USA.
J Synchrotron Radiat ; 28(Pt 1): 259-265, 2021 Jan 01.
Article in En | MEDLINE | ID: mdl-33399576
ABSTRACT
The performance of the new 52 kHz frame rate Rigaku XSPA-500k detector was characterized on beamline 8-ID-I at the Advanced Photon Source at Argonne for X-ray photon correlation spectroscopy (XPCS) applications. Due to the large data flow produced by this detector (0.2 PB of data per 24 h of continuous operation), a workflow system was deployed that uses the Advanced Photon Source data-management (DM) system and high-performance software to rapidly reduce area-detector data to multi-tau and two-time correlation functions in near real time, providing human-in-the-loop feedback to experimenters. The utility and performance of the workflow system are demonstrated via its application to a variety of small-angle XPCS measurements acquired from different detectors in different XPCS measurement modalities. The XSPA-500k detector, the software and the DM workflow system allow for the efficient acquisition and reduction of up to ∼109 area-detector data frames per day, facilitating the application of XPCS to measuring samples with weak scattering and fast dynamics.
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Full text: 1 Collection: 01-internacional Database: MEDLINE Language: En Journal: J Synchrotron Radiat Journal subject: RADIOLOGIA Year: 2021 Document type: Article Affiliation country: United States
Fulltext
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Full text: 1 Collection: 01-internacional Database: MEDLINE Language: En Journal: J Synchrotron Radiat Journal subject: RADIOLOGIA Year: 2021 Document type: Article Affiliation country: United States