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Effect of Solvent on the Rate of Ozonolysis: Development of a Homogeneous Flow Ozonolysis Protocol.
Arriaga, Danniel K; Kang, Seokmin; Thomas, Andy A.
Affiliation
  • Arriaga DK; Department of Chemistry, Texas A&M University, College Station, Texas 77842-0001, United States.
  • Kang S; Department of Chemistry, Texas A&M University, College Station, Texas 77842-0001, United States.
  • Thomas AA; Department of Chemistry, Texas A&M University, College Station, Texas 77842-0001, United States.
J Org Chem ; 88(19): 13720-13726, 2023 Oct 06.
Article in En | MEDLINE | ID: mdl-37747787
ABSTRACT
Herein, we describe the effect of organic solvents on ozone solubility and the rate of ozonolysis reactions using rapid injection NMR spectroscopy. The tabulated solubility and kinetic data allowed for the design of a homogeneous ozonolysis flow reactor capable of delivering precise quantities of dissolved ozone to various olefin substrates.
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Full text: 1 Collection: 01-internacional Database: MEDLINE Language: En Journal: J Org Chem Year: 2023 Document type: Article Affiliation country: United States
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Full text: 1 Collection: 01-internacional Database: MEDLINE Language: En Journal: J Org Chem Year: 2023 Document type: Article Affiliation country: United States