In situ spin coater for multimodal grazing incidence x-ray scattering studies.
Rev Sci Instrum
; 94(9)2023 Sep 01.
Article
in En
| MEDLINE
| ID: mdl-37756552
We present herein a custom-made, in situ, multimodal spin coater system with an integrated heating stage that can be programmed with spinning and heating recipes and that is coupled with synchrotron-based, grazing-incidence wide- and small-angle x-ray scattering. The spin coating system features an adaptable experimental chamber, with the ability to house multiple ancillary probes such as photoluminescence and visible optical cameras, to allow for true multimodal characterization and correlated data analysis. This system enables monitoring of structural evolutions such as perovskite crystallization and polymer self-assembly across a broad length scale (2 Å-150 nm) with millisecond temporal resolution throughout a complete thin film fabrication process. The use of this spin coating system allows scientists to gain a deeper understanding of temporal processes of a material system, to develop ideal conditions for thin film manufacturing.
Full text:
1
Collection:
01-internacional
Database:
MEDLINE
Type of study:
Incidence_studies
/
Risk_factors_studies
Language:
En
Journal:
Rev Sci Instrum
Year:
2023
Document type:
Article
Affiliation country:
United States
Country of publication:
United States