Your browser doesn't support javascript.
loading
In situ spin coater for multimodal grazing incidence x-ray scattering studies.
Coffey, Aidan H; Slack, Jonathan; Cornell, Earl; Yang, Lee L; Anderson, Kevan; Wang, Kang; Dou, Letian; Zhu, Chenhui.
Affiliation
  • Coffey AH; Advanced Light Source, Lawrence Berkeley National Laboratory, Berkeley, California 94720, USA.
  • Slack J; Davidson School of Chemical Engineering, Purdue University, West Lafayette, Indiana 47907, USA.
  • Cornell E; Advanced Light Source, Lawrence Berkeley National Laboratory, Berkeley, California 94720, USA.
  • Yang LL; Advanced Light Source, Lawrence Berkeley National Laboratory, Berkeley, California 94720, USA.
  • Anderson K; Advanced Light Source, Lawrence Berkeley National Laboratory, Berkeley, California 94720, USA.
  • Wang K; Advanced Light Source, Lawrence Berkeley National Laboratory, Berkeley, California 94720, USA.
  • Dou L; Davidson School of Chemical Engineering, Purdue University, West Lafayette, Indiana 47907, USA.
  • Zhu C; Davidson School of Chemical Engineering, Purdue University, West Lafayette, Indiana 47907, USA.
Rev Sci Instrum ; 94(9)2023 Sep 01.
Article in En | MEDLINE | ID: mdl-37756552
We present herein a custom-made, in situ, multimodal spin coater system with an integrated heating stage that can be programmed with spinning and heating recipes and that is coupled with synchrotron-based, grazing-incidence wide- and small-angle x-ray scattering. The spin coating system features an adaptable experimental chamber, with the ability to house multiple ancillary probes such as photoluminescence and visible optical cameras, to allow for true multimodal characterization and correlated data analysis. This system enables monitoring of structural evolutions such as perovskite crystallization and polymer self-assembly across a broad length scale (2 Å-150 nm) with millisecond temporal resolution throughout a complete thin film fabrication process. The use of this spin coating system allows scientists to gain a deeper understanding of temporal processes of a material system, to develop ideal conditions for thin film manufacturing.

Full text: 1 Collection: 01-internacional Database: MEDLINE Type of study: Incidence_studies / Risk_factors_studies Language: En Journal: Rev Sci Instrum Year: 2023 Document type: Article Affiliation country: United States Country of publication: United States

Full text: 1 Collection: 01-internacional Database: MEDLINE Type of study: Incidence_studies / Risk_factors_studies Language: En Journal: Rev Sci Instrum Year: 2023 Document type: Article Affiliation country: United States Country of publication: United States