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Molten Salt-Assisted Synthesis of Titanium Nitride.
Parvizian, Mahsa; Reichholf, Nico; Riaz, Aysha A; Bhatt, Prajna; Regoutz, Anna; De Roo, Jonathan.
Affiliation
  • Parvizian M; Department of Chemistry, University of Basel, CH-4058, Basel, Switzerland.
  • Reichholf N; Department of Chemistry, University of Basel, CH-4058, Basel, Switzerland.
  • Riaz AA; Department of Chemistry, University College London, 20 Gordon Street, WC1H 0AJ, London, UK.
  • Bhatt P; Department of Chemistry, University College London, 20 Gordon Street, WC1H 0AJ, London, UK.
  • Regoutz A; Department of Chemistry, University College London, 20 Gordon Street, WC1H 0AJ, London, UK.
  • De Roo J; Department of Chemistry, University of Basel, CH-4058, Basel, Switzerland.
Small Methods ; : e2400228, 2024 Jun 10.
Article in En | MEDLINE | ID: mdl-38859636
ABSTRACT
Titanium nitride is an exciting plasmonic material, with optical properties similar to gold. However, synthesizing TiN nanocrystals is highly challenging and typically requires solid-state reactions at very high temperatures (800-1000°C). Here, the synthesis of TiN nanocrystals is achieved at temperatures as low as 350°C, in just 1 h. The strategy comprises molten salt, Mg as reductant and Ca3N2 as nitride source. This brings TiN from the realm of solid-state chemistry into the field of solution-based synthesis in regular, borosilicate glassware.
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Full text: 1 Collection: 01-internacional Database: MEDLINE Language: En Journal: Small Methods Year: 2024 Document type: Article Affiliation country: Switzerland
Fulltext
Add to My VHL
Print
XML
PubMed Links
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Full text: 1 Collection: 01-internacional Database: MEDLINE Language: En Journal: Small Methods Year: 2024 Document type: Article Affiliation country: Switzerland