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Integrated multi-analytical screening approach for reliable radiocarbon dating of ancient mortars.
Ricci, Giulia; Secco, Michele; Addis, Anna; Pistilli, Anna; Preto, Nereo; Brogiolo, Gian Pietro; Arnau, Alexandra Chavarria; Marzaioli, Fabio; Passariello, Isabella; Terrasi, Filippo; Artioli, Gilberto.
Afiliación
  • Ricci G; Department of Geosciences, University of Padova, Via Giovanni Gradenigo 6, 35131, Padua, Italy. giulia.ricci@unipd.it.
  • Secco M; Inter-Departmental Research Centre for the Study of Cement Materials and Hydraulic Binders (CIRCe), University of Padova, Via Giovanni Gradenigo 6, 35131, Padua, Italy. giulia.ricci@unipd.it.
  • Addis A; Inter-Departmental Research Centre for the Study of Cement Materials and Hydraulic Binders (CIRCe), University of Padova, Via Giovanni Gradenigo 6, 35131, Padua, Italy.
  • Pistilli A; Department of Cultural Heritage (DBC), University of Padova, Piazza Capitaniato 7, 35139, Padua, Italy.
  • Preto N; Bruker Italia S.R.L. Daltonics Division, Via Cluentina 26/R, 62010, Macerata, Italy.
  • Brogiolo GP; Department of Geosciences, University of Padova, Via Giovanni Gradenigo 6, 35131, Padua, Italy.
  • Arnau AC; Department of Geosciences, University of Padova, Via Giovanni Gradenigo 6, 35131, Padua, Italy.
  • Marzaioli F; Department of Cultural Heritage (DBC), University of Padova, Piazza Capitaniato 7, 35139, Padua, Italy.
  • Passariello I; Department of Cultural Heritage (DBC), University of Padova, Piazza Capitaniato 7, 35139, Padua, Italy.
  • Terrasi F; Centre for Isotopic Research on Cultural and Environmental Heritage (CIRCE), University of Campania "Luigi Vanvitelli", Viale Carlo III 153, San Nicola La Strada, 81020, Caserta, Italy.
  • Artioli G; Centre for Isotopic Research on Cultural and Environmental Heritage (CIRCE), University of Campania "Luigi Vanvitelli", Viale Carlo III 153, San Nicola La Strada, 81020, Caserta, Italy.
Sci Rep ; 12(1): 3339, 2022 02 28.
Article en En | MEDLINE | ID: mdl-35228646
ABSTRACT
Radiocarbon dating of the carbonate binder of historical mortars is a strategic research topic not lacking in complexities. The critical step is the separation of anthropogenic CaCO3-binder from other carbonate sources that could severely affect the resulting dates. Here we present a complete procedure for the processing and characterization of difficult mortars and of the separated binder fractions in order to assess a priori the chances of positively dating the mortar, and produce a binder fraction yielding the most reliable radiocarbon dates possible. Two complex architectural case studies from Northern Italy are presented and discussed in detail the churches of Santa Maria Maggiore (Lomello, Pavia) and Santa Maria (Torba, Varese). The results support that both the reliability assessment and the successful radiocarbon dating are possible through a multi-analytical approach encompassing mineralogical and petrographic characterization, X-ray powder diffraction, scanning electron microscopy, measurement of carbon and oxygen stable isotopes, and optical cathodoluminescence.
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Carbono / Datación Radiométrica Tipo de estudio: Diagnostic_studies / Screening_studies Idioma: En Revista: Sci Rep Año: 2022 Tipo del documento: Article País de afiliación: Italia
Texto completo
Añadir a Mi BVS
Imprimir
XML
PubMed Links
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Carbono / Datación Radiométrica Tipo de estudio: Diagnostic_studies / Screening_studies Idioma: En Revista: Sci Rep Año: 2022 Tipo del documento: Article País de afiliación: Italia