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Direct Molar Mass Determination of Self-Assembled Amphiphilic Block Copolymer Nanoobjects Using Electrospray-Charge Detection Mass Spectrometry.
Doussineau, Tristan; Bao, Cong Yu; Antoine, Rodolphe; Dugourd, Philippe; Zhang, Wenjing; D'Agosto, Franck; Charleux, Bernadette.
Afiliación
  • Doussineau T; Université de Lyon, 69622, Lyon, France; Université Lyon 1, 69622 Villeurbanne Cedex, France, and CNRS, UMR5579, LASIM, Villeurbanne Cedex, France.
  • Bao CY; Université de Lyon, 69622, Lyon, France; Université Lyon 1, 69622 Villeurbanne Cedex, France, and CNRS, UMR5579, LASIM, Villeurbanne Cedex, France.
  • Antoine R; Université de Lyon, 69622, Lyon, France; Université Lyon 1, 69622 Villeurbanne Cedex, France, and CNRS, UMR5579, LASIM, Villeurbanne Cedex, France.
  • Dugourd P; Université de Lyon, 69622, Lyon, France; Université Lyon 1, 69622 Villeurbanne Cedex, France, and CNRS, UMR5579, LASIM, Villeurbanne Cedex, France.
  • Zhang W; Université de Lyon 69622, Lyon, France; Université Lyon 1, 69622 Villeurbanne Cedex, CPE Lyon, France, and CNRS, UMR 5265, C2P2 (Chemistry, Catalysis, Polymers & Processes), Team LCPP Bat 308F, 43 Bd du 11 novembre 1918, 69616 Villeurbanne, France.
  • D'Agosto F; Université de Lyon 69622, Lyon, France; Université Lyon 1, 69622 Villeurbanne Cedex, CPE Lyon, France, and CNRS, UMR 5265, C2P2 (Chemistry, Catalysis, Polymers & Processes), Team LCPP Bat 308F, 43 Bd du 11 novembre 1918, 69616 Villeurbanne, France.
  • Charleux B; Université de Lyon 69622, Lyon, France; Université Lyon 1, 69622 Villeurbanne Cedex, CPE Lyon, France, and CNRS, UMR 5265, C2P2 (Chemistry, Catalysis, Polymers & Processes), Team LCPP Bat 308F, 43 Bd du 11 novembre 1918, 69616 Villeurbanne, France.
ACS Macro Lett ; 1(3): 414-417, 2012 Mar 20.
Article en En | MEDLINE | ID: mdl-35578513
Charge detection mass spectrometry (CD-MS) combined with electrospray ionization was used to determine, in a direct way and for the first time, the molar mass of self-assembled amphiphilic block copolymer nanoobjects prepared via living radical emulsion polymerization. CD-MS supplies enough data for calculating statistically significant measurements of the mass of particles in the megadalton to gigadalton range and their resulting mass distribution.

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Tipo de estudio: Diagnostic_studies Idioma: En Revista: ACS Macro Lett Año: 2012 Tipo del documento: Article País de afiliación: Francia Pais de publicación: Estados Unidos

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Tipo de estudio: Diagnostic_studies Idioma: En Revista: ACS Macro Lett Año: 2012 Tipo del documento: Article País de afiliación: Francia Pais de publicación: Estados Unidos