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Synthesis of ß-iodovinyl sulfones via direct photoinitiated difunctionalization of internal alkynes.
Abramov, Vladimir A; Topchiy, Maxim A; Rasskazova, Maria A; Drokin, Egor A; Sterligov, Grigorii K; Shurupova, Olga V; Malysheva, Anna S; Rzhevskiy, Sergey A; Beletskaya, Irina P; Asachenko, Andrey F.
Afiliación
  • Abramov VA; A. V. Topchiev Institute of Petrochemical Synthesis, Russian Academy of Sciences, Moscow 119991, Russia. aasachenko@ips.ac.ru.
  • Topchiy MA; A. V. Topchiev Institute of Petrochemical Synthesis, Russian Academy of Sciences, Moscow 119991, Russia. aasachenko@ips.ac.ru.
  • Rasskazova MA; A. V. Topchiev Institute of Petrochemical Synthesis, Russian Academy of Sciences, Moscow 119991, Russia. aasachenko@ips.ac.ru.
  • Drokin EA; A. V. Topchiev Institute of Petrochemical Synthesis, Russian Academy of Sciences, Moscow 119991, Russia. aasachenko@ips.ac.ru.
  • Sterligov GK; A. V. Topchiev Institute of Petrochemical Synthesis, Russian Academy of Sciences, Moscow 119991, Russia. aasachenko@ips.ac.ru.
  • Shurupova OV; A. V. Topchiev Institute of Petrochemical Synthesis, Russian Academy of Sciences, Moscow 119991, Russia. aasachenko@ips.ac.ru.
  • Malysheva AS; A. V. Topchiev Institute of Petrochemical Synthesis, Russian Academy of Sciences, Moscow 119991, Russia. aasachenko@ips.ac.ru.
  • Rzhevskiy SA; A. V. Topchiev Institute of Petrochemical Synthesis, Russian Academy of Sciences, Moscow 119991, Russia. aasachenko@ips.ac.ru.
  • Beletskaya IP; Department of Chemistry, M. V. Lomonosov Moscow State University, Leninskie Gory, 1-3, Moscow 119991, Russia.
  • Asachenko AF; A. V. Topchiev Institute of Petrochemical Synthesis, Russian Academy of Sciences, Moscow 119991, Russia. aasachenko@ips.ac.ru.
Org Biomol Chem ; 21(18): 3844-3849, 2023 May 10.
Article en En | MEDLINE | ID: mdl-37092257
ABSTRACT
The reaction of direct photoinitiated iodosulfonylation of internal acetylenes with p-tolylsulfonyl iodide and its regioselectivity of the products was studied. Methods for the subsequent functionalization of ß-iodovinylsulfones using cross-coupling reactions to obtain valuable and non-available compounds are proposed.
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: Org Biomol Chem Asunto de la revista: BIOQUIMICA / QUIMICA Año: 2023 Tipo del documento: Article País de afiliación: Rusia
Texto completo
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Imprimir
XML
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: Org Biomol Chem Asunto de la revista: BIOQUIMICA / QUIMICA Año: 2023 Tipo del documento: Article País de afiliación: Rusia