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A Photoreactor-Interfaced Mass Spectrometer: An Online Platform to Monitor Photochemical Reactions.
Shiels, Oisin J; Menti-Platten, Maria; Bokosi, Fostino R B; Burns, Brett R; Keaveney, Sinead T; Keller, Paul A; Barker, Philip J; Trevitt, Adam J.
Afiliación
  • Shiels OJ; Molecular Horizons and School of Chemistry and Molecular Bioscience, University of Wollongong, Wollongong NSW 2522, Australia.
  • Menti-Platten M; Molecular Horizons and School of Chemistry and Molecular Bioscience, University of Wollongong, Wollongong NSW 2522, Australia.
  • Bokosi FRB; Molecular Horizons and School of Chemistry and Molecular Bioscience, University of Wollongong, Wollongong NSW 2522, Australia.
  • Burns BR; Molecular Horizons and School of Chemistry and Molecular Bioscience, University of Wollongong, Wollongong NSW 2522, Australia.
  • Keaveney ST; Molecular Horizons and School of Chemistry and Molecular Bioscience, University of Wollongong, Wollongong NSW 2522, Australia.
  • Keller PA; Molecular Horizons and School of Chemistry and Molecular Bioscience, University of Wollongong, Wollongong NSW 2522, Australia.
  • Barker PJ; Molecular Horizons and School of Chemistry and Molecular Bioscience, University of Wollongong, Wollongong NSW 2522, Australia.
  • Trevitt AJ; Molecular Horizons and School of Chemistry and Molecular Bioscience, University of Wollongong, Wollongong NSW 2522, Australia.
Anal Chem ; 95(42): 15472-15476, 2023 Oct 24.
Article en En | MEDLINE | ID: mdl-37830912
An experimental platform is reported that allows for the online characterization of photochemical reactions by coupling a continuous flow photoreactor, equipped with LED light irradiation and a dual-tipped ESI source, directly to a mass spectrometer with electrospray ionization. The capabilities of this platform are demonstrated with two classes of photoreactions: (1) the photopolymerization of methyl methacrylate and (2) photocatalyzed alkyne insertion into a 1,2,3-benzotriazinone. The online technique provides rapid information to inform the underlying photochemical mechanism and evaluate the overall photochemistry.
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: Anal Chem Año: 2023 Tipo del documento: Article País de afiliación: Australia Pais de publicación: Estados Unidos
Texto completo
Añadir a Mi BVS
Imprimir
XML
PubMed Links
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: Anal Chem Año: 2023 Tipo del documento: Article País de afiliación: Australia Pais de publicación: Estados Unidos