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An environmentally benign protocol for the synthesis of sugar 1,2-orthoesters in poly(ethylene glycol) dimethyl ether (DMPE).
Yang, Jian; Wei, Shanqiao; Zhao, Jinzhong; Zeng, Wei; Shao, Huawu; Ma, Xiaofeng.
Afiliación
  • Yang J; Natural Products Research Centre, Chengdu Institute of Biology, Chinese Academy of Sciences, Chengdu, 610041, PR China; University of Chinese Academy of Sciences, Beijing, 100049, PR China.
  • Wei S; Natural Products Research Centre, Chengdu Institute of Biology, Chinese Academy of Sciences, Chengdu, 610041, PR China; University of Chinese Academy of Sciences, Beijing, 100049, PR China.
  • Zhao J; Natural Products Research Centre, Chengdu Institute of Biology, Chinese Academy of Sciences, Chengdu, 610041, PR China; University of Chinese Academy of Sciences, Beijing, 100049, PR China.
  • Zeng W; Natural Products Research Centre, Chengdu Institute of Biology, Chinese Academy of Sciences, Chengdu, 610041, PR China; University of Chinese Academy of Sciences, Beijing, 100049, PR China.
  • Shao H; Natural Products Research Centre, Chengdu Institute of Biology, Chinese Academy of Sciences, Chengdu, 610041, PR China. Electronic address: shaohw@cib.ac.cn.
  • Ma X; Natural Products Research Centre, Chengdu Institute of Biology, Chinese Academy of Sciences, Chengdu, 610041, PR China; University of Chinese Academy of Sciences, Beijing, 100049, PR China. Electronic address: maxf@cib.ac.cn.
Carbohydr Res ; 534: 108902, 2023 Dec.
Article en En | MEDLINE | ID: mdl-38006705
An environmentally benign procedure has been developed for the synthesis of sugar orthoesters using anhydrous sodium acetate in poly (ethylene glycol)dimethyl ether (DMPE). Various sugar orthoesers were prepared without using volatile organic solvent and quaternary ammonium salt. The sugar orthoesters were obtained in good to excellent yields.
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Polietilenglicoles / Azúcares Idioma: En Revista: Carbohydr Res Año: 2023 Tipo del documento: Article Pais de publicación: Países Bajos
Texto completo
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XML
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Polietilenglicoles / Azúcares Idioma: En Revista: Carbohydr Res Año: 2023 Tipo del documento: Article Pais de publicación: Países Bajos