[Determination of thirteen metal elements in the plant Foeniculum vulgare Mill. by flame atomic absorption spectrophotometry].
Guang Pu Xue Yu Guang Pu Fen Xi
; 26(10): 1935-8, 2006 Oct.
Article
de Zh
| MEDLINE
| ID: mdl-17205757
ABSTRACT
The objective of the paper is to determine the amount of metal elements of Na, K, Mg, Ca, Cu, Zn, Mn, Fe, Co, Ni, Cd, Cr and Pb in the planted Foeniculum vulgare Mill. by flame atomic absorption spectrophotometry (FAAS), after the cinefaction and the digestion with HNO3-HClO4 (phi 41) at 90-95 degrees C and normal pressure. The optimum parameters of FAAS and the effects of solution medium on the results were investigated. The analytical results show that the amount of Na, K, Mg, Ca, Mn, Fe, Cu, Zn and Pb was 1508.7, 27653.0, 2036.0, 4848.1, 24.8, 323.5, 15.2, 23.7 and 10.8 microg x g(-1), respectively, and that of Co, Ni, Cd and Cr was not checked out in the samples. The recovery of standard addition is 97.45%-102.50%, the relative standard deviation (n=9) was 0.34%-2.77%. The characteristic method is quick, simple and convenient and the results are satisfactory.
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Collection:
01-internacional
Base de données:
MEDLINE
Sujet principal:
Spectrophotométrie atomique
/
Foeniculum
/
Métaux
Langue:
Zh
Journal:
Guang Pu Xue Yu Guang Pu Fen Xi
Année:
2006
Type de document:
Article
Pays d'affiliation:
Chine