[Determination of Asulam in Livestock Products by LC-MS/MS].
Shokuhin Eiseigaku Zasshi
; 62(1): 1-7, 2021.
Article
de Ja
| MEDLINE
| ID: mdl-33658458
ABSTRACT
An analytical method based on LC-MS/MS was developed for the determination of asulam in livestock products. Asulam in livestock products was extracted with acetone. The crude extracts were defatted by acetonitrile and n-hexane partitioning. Cleanup was carried out using a combination of ethylene diamine-N-propyl silylation silica gel (PSA) and octadecyl silylated silica gel (C18) mini columns with acidic condition. The sample solution was subjected to LC-MS/MS using an external solvent calibration curve. The average recovery (n=5) of Asulam from four types of livestock products (bovine muscle, bovine fat, bovine liver and milk) spike at the maximum residue limits (MRLs) or at a uniform limit of 0.01 mg/kg was 92.7-98.7%, with a relative standard deviation of 3.1-11.6%. The limit of quantitation of the developed method was calculated to be 0.01 mg/kg.
Mots clés
Texte intégral:
1
Collection:
01-internacional
Base de données:
MEDLINE
Sujet principal:
Spectrométrie de masse en tandem
/
Bétail
Limites:
Animals
Langue:
Ja
Journal:
Shokuhin Eiseigaku Zasshi
Année:
2021
Type de document:
Article