Development of a Green Single Drop Microextraction Based on Deep Eutectic Solvent and HPLC-UV for Trace Residue Analysis of Three Frequent-Used Pesticides.
Iran J Public Health
; 52(11): 2440-2449, 2023 Nov.
Article
de En
| MEDLINE
| ID: mdl-38106827
ABSTRACT
Background:
A green sample preparation method named deep eutectic solvent-based single drop microextraction (DES-SDME) was developed and optimized for determining trace metribuzin, dichlorvos, and fenthion.Methods:
Two hundred seventy experimental runs were performed, and the optimal values of the five influential factors in the DES-SDME method were determined. The design of the study was based on one factor at a time and the peak area of high-performance liquid chromatography was used as a benchmark for comparing analysis results.Results:
After optimizing the effective factors, the linearity range, detection limit and quantification limit of the method were determined by drawing calibration curves for the studied analytes.Conclusion:
The results indicated the success of the developed method in obtaining acceptable figures of merit as a green preparation method with accuracy and precision.
Texte intégral:
1
Collection:
01-internacional
Base de données:
MEDLINE
Langue:
En
Journal:
Iran J Public Health
/
Iran. j. public health (Print)
/
Iranian journal of public health (Print)
Année:
2023
Type de document:
Article
Pays d'affiliation:
Iran
Pays de publication:
Iran