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[Confirmation of non-permitted dyes detected in Akasu (red vinegar) by LC/MS].
Shokuhin Eiseigaku Zasshi ; 46(5): 228-33, 2005 Oct.
Artigo em Japonês | MEDLINE | ID: mdl-16305179
ABSTRACT
Suitable liquid chromatography/mass spetrometry (LC/MS) conditions were examined for Amaranth, Red 2G (R2G), Azo Rubine (Azo), Fast Red E (FRE) and Brilliant Blue FCF, which were detected in Akasu, a red vinegar made in Hong Kong from sake lees, on both thin layer chromatography (TLC) and photodiode array high-performance liquid chromatography (PDA-HPLC). Molecular-related ions for each dye were detected with excellent sensitivity by LC/MS using electro-spray ionization with negative ion mode, capillary voltage 3.00 kV, cone voltage 50 V and desolvation temperature 400 degrees C. LC/MS analysis of refined Akasu under these conditions enabled us to obtain clear mass spectra of R2G, Azo and FRE, which were present at trace levels in the Akasu. The results were consistent with those from TLC and PDA-HPLC. These experiments suggested that LC/MS analysis is applicable for confirmation of dyes in food.
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Coleções: Bases de dados internacionais Base de dados: MEDLINE Assunto principal: Espectrometria de Massas / Cromatografia Líquida / Ácido Acético / Corantes Idioma: Japonês Revista: Shokuhin Eiseigaku Zasshi Ano de publicação: 2005 Tipo de documento: Artigo País de afiliação: Japão