Design and Fabrication of a Flexible Gravimetric Sensor Based on a Thin-Film Bulk Acoustic Wave Resonator.

Sensing systems are becoming less and less invasive. In this context, flexible materials offer new opportunities that are impossible to achieve with bulky and rigid chips. Standard silicon sensors cannot be adapted to curved shapes and are susceptible to big deformations, thus discouraging their use in wearable applications. Another step forward toward minimising the impacts of the sensors can be to avoid the use of cables and connectors by exploiting wireless transmissions at ultra-high frequencies (UHFs). Thin-film bulk acoustic wave resonators (FBARs) represent the most promising choice among all of the piezoelectric microelectromechanical system (MEMS) resonators for the climbing of radio frequencies. Accordingly, the fabrication of FBARs on flexible and wearable substrates represents a strategic step toward obtaining a new generation of highly sensitive wireless sensors. In this work, we propose the design and fabrication of a flexible gravimetric sensor based on an FBAR on a polymeric substrate. The resonator presents one of the highest electromechanical coupling factors in the category of flexible AlN-based FBARs, equal to 6%. Moreover, thanks to the polymeric support layer, the presence of membranes can be avoided, which leads to a faster and cheaper fabrication process and higher robustness of the structure. The mass sensitivity of the device was evaluated, obtaining a promising value of 23.31 ppm/pg. We strongly believe that these results can pave the way to a new class of wearable MEMS sensors that exploit ultra-high-frequency (UHF) transmissions.

Holographic Manipulation of Nanostructured Fiber Optics Enables Spatially-Resolved, Reconfigurable Optical Control of Plasmonic Local Field Enhancement and SERS.

Integration of plasmonic structures on step-index optical fibers is attracting interest for both applications and fundamental studies. However, the possibility to dynamically control the coupling between the guided light fields and the plasmonic resonances is hindered by the turbidity of light propagation in multimode fibers (MMFs). This pivotal point strongly limits the range of studies that can benefit from nanostructured fiber optics. Fortunately, harnessing the interaction between plasmonic modes on the fiber tip and the full set of guided modes can bring this technology to a next generation progress. Here, the intrinsic wealth of information of guided modes is exploited to spatiotemporally control the plasmonic resonances of the coupled system. This concept is shown by employing dynamic phase modulation to structure both the response of plasmonic MMFs on the plasmonic facet and their response in the corresponding Fourier plane, achieving spatial selective field enhancement and direct control of the probe's work point in the dispersion diagram. Such a conceptual leap would transform the biomedical applications of holographic endoscopic imaging by integrating new sensing and manipulation capabilities.

Design of vanadium-dioxide-based resonant structures for tunable optical response.

Phase change materials are suitable for tunable photonic devices where the optical response can be altered under external stimuli, such as heat, an electrical or an optical signal. In this scenario, we performed numerical simulations to study the optical properties of a flat unpatterned resonant structure and a grating, both coated with a thin film of vanadium dioxide (VO2). Our results suggest that it is possible to modulate broadband and narrowband reflectance spectra of the resonant structures in the visible to near-infrared range by more than 40 % when the VO2 undergoes an insulator-to-metal phase transition. Resonant devices with a tunable spectral response may find application in sensors, filters, absorbers, and detectors.

Multifunctional and reconfigurable graphene/liquid crystal-assisted asymmetrical Fabry-Pérot cavity for reflected light control.

Multifunctional and reconfigurable devices are crucial for compact and smart optoelectronic devices. In this paper, we propose a multifunctional and spectrally reconfigurable asymmetric 1D PhC Fabry-Pérot cavity filled with nematic liquid crystal and bounded by two graphene monolayers. Due to the large number of available degrees of freedom, such a structure can behave as either a notch filter, an absorber, an amplitude modulator, or a phase shifter for the reflected electromagnetic waves. The chemical potential of one or both graphene monolayers can be exploited to modulate the amplitude and phase-shift angle of the reflected electromagnetic waves. Furthermore, all functions are narrowband (1 nm linewidth) and are spectrally tunable over a range of about 200 nm around the working wavelength of 1550 nm by controlling the orientation of the elongated molecules of the liquid crystal. This structure may be advantageously exploited for the realization of optical modulators and beamsteering systems.

High transmission from 2D periodic plasmonic finite arrays with sub-20 nm gaps realized with Ga focused ion beam milling.

Fabricating plasmonic nanostructures with good optical performances often requires lengthy and challenging patterning processes that can hardly be transferred to unconventional substrates, such as optical fiber tips or curved surfaces. Here we investigate the use of a single Ga focused ion beam process to fabricate 2D arrays of gold nanoplatelets for nanophotonic applications. While observing that focused ion beam milling of crossing tapered grooves inherently produces gaps below 20 nm, we provide experimental and theoretical evidence for the spectral features of grooves terminating with a sharp air gap. We show that transmission near 10% can be obtained via two-dimensional nano-focusing in a finite subset of 2D arrays of gold nanoplatelets. This enables the application of our nanostructure to detect variations in the refractive index of thin films using either reflected or transmitted light when a small number of elements are engaged.

Characterization of a COTS-Based RF Receiver for Cubesat Applications.

This paper reports the experimental results of a test campaign performed on the radio-frequency (RF) receiver prototype operating at a 2025-2110 MHz frequency range, designed and fabricated for CubeSat applications. The prototype has been tested through a board-level test approach for the verification of the functional requirements and a component-level one for specific characterization measures. The tests have shown the following results: a -115--70 dBm sensitivity range, 390 MHz intermediate frequency, a 0 dBm output power level with ±1 dB error, a 2.34 dB noise figure, and a 4.86 W power absorption. Such results have been largely achieved implementing an automatic gain control system by cascading two Commercial Off-The-Shelf (COTS) amplifiers. Moreover, an innovative technique based on RF test points has been successfully experimented and validated to measure the S-parameters of a custom low-pass filter integrated on the receiver, showing the possibility of even characterizing the single COTS components exposed to radiation through a unique board-level test setup. The technique may have a great impact on the cost reduction of electronic boards for space applications, since it would avoid using expensive evaluation boards for each COTS component that needs a radiation test.

Mesoscopic self-collimation along arbitrary directions and below the light line.

Self-collimation (SC) and mesoscopic self-collimation (MSC) have been successfully demonstrated along the directions of high symmetry of photonic crystals. Indeed, wide angular acceptances are obtained only in these directions which offer extremely flat isofrequencies. In this article, we numerically demonstrate that mesoscopic self-collimation with large angular acceptance can be achieved along arbitrary directions that are not of high symmetry. In particular, we propose a simple method that allows to easily find all the non-trivial collimation directions and corresponding frequencies. Thanks to the double periodicity of the mesoscopic crystal, these solutions can be effectively tailored in terms of direction and frequency. Moreover, non-trivial MSC solutions can be found well below the light cone. These MSC features open up the possibility of designing complex systems by combining different configurations, such as high reflection (HR) or anti reflection (AR) ones, or active materials.

Link budget analysis of bi-directional LEO and GEO optical feeder links advancing the beam wander model's accuracy.

The telecommunications of the future rely on the concept of a three-dimensional architecture able to integrate terrestrial and non-terrestrial networks with the goal to ensure a reliable and high-speed connectivity to users located anywhere. In this context, free space optical communications constitute a candidate technology for feeder links, thanks to their advantages in terms of bandwidth and achievable data rates. Nonetheless, due to the propagation impediments encountered by an optical beam travelling through atmosphere, flexible and accurate instruments able to support the design of optical feeder links are needed. Therefore, in this paper a link budget numerical tool able to meet these requirements is presented and the link budget analysis for real optical feeder links is performed demonstrating its prediction accuracy by means of the comparison with experimental results for both low Earth orbit and geostationary Earth orbit based configurations. Finally, the limits of the conventional beam wander model are analyzed and overcome.

Numerical analysis of the coupling mechanism in long-range plasmonic couplers at 1.55 µm.

We study the coupling mechanism between a high refractive index contrast waveguide and a plasmonic thin-film waveguide in the IR range. We also propose a novel design of a vertical coupler based on loading the plasmonic waveguide with a high refractive index contrast medium on each side. We achieve a coupling efficiency and an insertion loss of about 95% and 0.2 dB, respectively, with a coupling length of only 2.85 µm at the working wavelength of 1.55 µm.

Gold strip gratings with binary supercell.

In this Letter, the study of a periodic structure composed of gold strips arranged in double-period unit cells, in a symmetric and asymmetric environment, is reported. The spectral maps show that the formation of the plasmonic bandgap and the extraordinary optical transmission are subjected to the proportion between the strip widths. Moreover, when the asymmetric environment is considered, high-transmittance and high-absorbance states arise. Hence, by controlling the geometrical parameters of the binary-periodic structure, it is possible to tailor the spectral response of the grating enhancing the desired features and exploiting them for different applications.

Design of optically transparent metasurfaces based on CVD graphene for mmWave applications.

We propose and numerically investigate a smart, optically transparent digital metasurface reflective in the mmWave range, based on CVD graphene programmable elements. For both TM and TE polarizations, we detail the optimization of the unit cells, designed to exhibit two distinct states that correspond to those of binary encoding. The whole metasurface encoding can be customized to provide different electromagnetic functions, such as wide-band beam splitting at a controlled angle and reduction of the Radar Cross Section. Optically transparent metasurfaces could be integrated and exploited in windows and transparent surfaces in future Beyond-5G and 6G ecosystems.

Wearable Heart Rate Monitoring Device Communicating in 5G ISM Band for IoHT.

Advances in wearable device technology pave the way for wireless health monitoring for medical and non-medical applications. In this work, we present a wearable heart rate monitoring platform communicating in the sub-6GHz 5G ISM band. The proposed device is composed of an Aluminium Nitride (AlN) piezoelectric sensor, a patch antenna, and a custom printed circuit board (PCB) for data acquisition and transmission. The experimental results show that the presented system can acquire heart rate together with diastolic and systolic duration, which are related to heart relaxation and contraction, respectively, from the posterior tibial artery. The overall system dimension is 20 mm by 40 mm, and the total weight is 20 g, making this device suitable for daily utilization. Furthermore, the system allows the simultaneous monitoring of multiple subjects, or a single patient from multiple body locations by using only one reader. The promising results demonstrate that the proposed system is applicable to the Internet of Healthcare Things (IoHT), and particularly Integrated Clinical Environment (ICE) applications.

Localized surface plasmon resonances in gold nano-patches on a gallium nitride substrate.

In this paper we describe the design, fabrication and characterization of gold nano-patches, deposited on gallium nitride substrate, acting as optical nanoantennas able to efficiently localize the electric field at the metal-dielectric interface. We analyse the performance of the proposed device, evaluating the transmission and the electric field localization by means of a three-dimensional finite difference time domain (FDTD) method. We detail the fabrication protocol and show the morphological characterization. We also investigate the near-field optical transmission by means of scanning near-field optical microscope measurements, which reveal the excitation of a localized surface plasmon resonance at a wavelength of 633 nm, as expected by the FDTD calculations. Such results highlight how the final device can pave the way for the realization of a single optical platform where the active material and the metal nanostructures are integrated together on the same chip.

Effective hole conductivity in nitrogen-doped CVD-graphene by singlet oxygen treatment under photoactivation conditions.

Nitrogen substitutional doping in the π-basal plane of graphene has been used to modulate the material properties and in particular the transition from hole to electron conduction, thus enlarging the field of potential applications. Depending on the doping procedure, nitrogen moieties mainly include graphitic-N, combined with pyrrolic-N and pyridinic-N. However, pyridine and pyrrole configurations of nitrogen are predominantly introduced in monolayer graphene:N lattice as prepared by CVD. In this study, we investigate the possibility of employing pyridinic-nitrogen as a reactive site as well as activate a reactive center at the adjacent carbon atoms in the functionalized C-N bonds, for additional post reaction like oxidation. Furthermore, the photocatalytic activity of the graphene:N surface in the production of singlet oxygen (1O2) is fully exploited for the oxidation of the graphene basal plane with the formation of pyridine N-oxide and pyridone structures, both having zwitterion forms with a strong p-doping effect. A sheet resistance value as low as 100 Ω/□ is reported for a 3-layer stacked graphene:N film.

Experimental demonstration of a novel bio-sensing platform via plasmonic band gap formation in gold nano-patch arrays.

In this paper we discuss the possibility of implementing a novel bio-sensing platform based on the observation of the shift of the leaky surface plasmon mode that occurs at the edge of the plasmonic band gap of metal gratings, when an analyte is deposited on top of the metallic structure. We report numerical calculations, fabrication and experimental measurements to prove the sensing capability of a two-dimensional array of gold nano-patches in the detection of a small quantity of Isopropyl Alcohol (IPA) deposited on top of sensor surface. The calculated sensitivity of our device approaches a value of 1000 nm/RIU with a corresponding Figure of Merit (FOM) of 222 RIU(-1). The presence of IPA can also be visually estimated by observing a color variation in the diffracted field. We show that color brightness and intensity variations can be ascribed to a change in the aperture size, keeping the periodicity constant, and to different types of analyte deposited on the sample, respectively. Moreover, we demonstrate that unavoidable fabrication imperfections revealed by the presence of rounded corners and surface roughness do not significantly affect device performance.

Plasmonic bandgap formation in two-dimensional periodic arrangements of gold patches with subwavelength gaps.

We report on the formation of plasmonic bandgaps in two-dimensional periodic arrangements of gold patches. Orthogonal arrays of subwavelength slits with different periodicities have been studied by means of a three-dimensional finite-difference time-domain (FDTD) code, changing incident polarization and geometrical parameters. Spectral response of gold patches having different a form factor and surrounded by different media have been also investigated and compared in order to give a full description of bandgap shifts paving the way for the design of polarization-sensitive devices.

Rapid Prototyping of Bio-Inspired Dielectric Resonator Antennas for Sub-6 GHz Applications.

Bio-inspired Dielectric Resonator Antennas (DRAs) are engaging more and more attention from the scientific community due to their exceptional wideband characteristic, which is especially desirable for the implementation of 5G communications. Nonetheless, since these antennas exhibit peculiar geometries in their micro-features, high dimensional accuracy must be accomplished via the selection of the most suitable fabrication process. In this study, the challenges to the manufacturing process presented by the wideband Spiral shell Dielectric Resonator Antenna (SsDRA), based on the Gielis superformula, are addressed. Three prototypes, made of three different photopolymer resins, were manufactured by bottom-up micro-Stereolithography (SLA). This process allows to cope with SsDRA's fabrication criticalities, especially concerning the wavy features characterizing the thin spiral surface and the micro-features located in close proximity to the spiral origin. The assembly of the SsDRAs with a ground plane and feed probe was also accurately managed in order to guarantee reliable and repeatable measurements. The scattering parameter S11 trends were then measured by means of a Vector Network Analyzer, while the realized gains and 3D radiation diagrams were measured in the anechoic chamber. The experimental results show that all SsDRAs display relevant wideband behavior of 2 GHz at -10 dB in the sub-6 GHz range.

Optical filter based on two coupled PhC GaAs-membranes.

We demonstrate an ultracompact optical filter based on two coupled high-index contrast GaAs photonic crystal (PhC) membranes. The PhC membranes consist of a square lattice of air holes and behave as a Fabry-Perot cavity whose reflectivity and transmissivity depend on the air gap between the two membranes. The normal-incidence reflectance measurements and the numerical simulation of reflection spectra show a high sensitivity to the geometrical parameters, such as the distance between the slabs, whose control would make the device suitable for a new class of tunable optical filters.

Reconfigurable and optically transparent microwave absorbers based on deep eutectic solvent-gated graphene.

Electrolytically tunable graphene "building blocks" for reconfigurable and optically transparent microwave surfaces and absorbers have been designed and fabricated by exploiting Deep Eutectic Solvents (DESs). DESs have been first explored as electrolytic and environmentally friendly media for tuning sheet resistance and Fermi level of graphene together with its microwave response (reflection, transmission and absorption). We consider the tunability of the reconfigurable surfaces in terms of transmittance, absorption and reflectance, respectively, over the X and Ku bands when the gate voltage is varied in the -1.4/+1.4 V range. The numerical simulations and experimental measurements also show the ability of the absorber, in the Salisbury screen configuration, to achieve near perfect absorption with a modulation of about 20%. These results could find applications in several technological fields, ranging from electromagnetic pollution to integrated multi-physical regulation systems, thereby helping the advance of the performance of microwave cloaking systems, stealth windows, frequency selective surfaces, modulators and polarizers.

Analysis of microwave thermal treatment of antique books with metallic insets.

The electromagnetic and thermal analyses of a mode-stirred chamber designed for the heat treatment of antique and precious books are proposed. In particular, the electromagnetic and thermal perturbations due to the presence of metallic insets inside the treated material (paper) are investigated. The temperature measurement results obtained by thermography and by temperature fiber-optic sensor are also reported. Finally, metallic shields are experimentally demonstrated to prevent the overheating of the treated material and the consequent damage of the antique tomes.