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J Org Chem ; 85(16): 10846-10857, 2020 08 21.
Artigo em Inglês | MEDLINE | ID: mdl-32677439

RESUMO

The ability to alter optoelectronic and magnetic properties of molecules at a late stage in their preparation is in general a nontrivial feat. Here, we report the late-stage oxidation of benzothiophene-fused indacenes and dicyclopentanaphthalenes to their corresponding sulfone derivatives. We find that while such modifications increase the highest occupied molecular orbital (HOMO)-lowest unoccupied molecular orbital (LUMO) energy gap to a small degree, other properties such as HOMO and LUMO energy levels, molecule paratropicity, and singlet-triplet energy gaps are influenced to a greater degree. The most surprising finding is a change of the bond alternation pattern within the s-indacene core of the sulfones. Computations corroborate the experimental findings and offer plausible explanations for these changes in molecular properties.


Assuntos
Eletrônica , Fluorenos , Modelos Moleculares , Enxofre
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