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1.
Sci Rep ; 13(1): 16166, 2023 Sep 27.
Artigo em Inglês | MEDLINE | ID: mdl-37759080

RESUMO

In this study, microstructural features direct metal laser melted (DMLM) aluminium-silicon-magnesium (AlSi10Mg) are investigated using advanced transmission electron microscopy (TEM) and high-resolution TEM (HRTEM). The focus is on post-processing by ECAP (Equal Channel Angular Pressing) and its effects on grain refinement, stacking fault formation and dislocation accumulation. In addition, the strength enhancing role of stacking faults is for the first time quantified. The results show that ECAP can increase the yield strength from 294 to 396 MPa, while the elongation increases from 2.4% to 6%. These results show that ECAP processing offers a new approach for producing AlSi10Mg products with improved strength and ductility.

2.
Materials (Basel) ; 15(22)2022 Nov 10.
Artigo em Inglês | MEDLINE | ID: mdl-36431429

RESUMO

With the aim of improving the excellent mechanical properties of the SLM-produced AlSi10Mg alloy, this research focuses on post-processing using ECAP (Equal Channel Angular Pressing). In our article, two different post-processing strategies were investigated: (1) low-temperature annealing (LTA) and subsequent ECAP processing at 150 °C; (2) no heat treatment and subsequent ECAP processing at 350 °C, 400 °C and 450 °C. The microstructure and mechanical properties of this alloy were analyzed at each stage of post-treatment. Metallographic observations, combined with SEM and EBSD studies, showed that the alloys produced by SLM have a unique cellular microstructure consisting of Si networks surrounding the Al-based matrix phase. Low-temperature annealing (LTA), followed by ECAP treatment, facilitated the microstructural evolution of the alloy with partial breakup of the Si network and observed nucleation of ß-Si precipitates throughout the Al matrix. This resulted in a Vickers microhardness of 153 HV and a yield strength of 415 MPa. The main results show that post-processing of SLM-produced AlSi10Mg alloys using ECAP significantly affects the microstructural evolution and mechanical properties of the alloy.

3.
Materials (Basel) ; 14(22)2021 Nov 14.
Artigo em Inglês | MEDLINE | ID: mdl-34832266

RESUMO

It is well-known that cracks are observed around the impression during indentation of brittle materials. The cracks inception depends on load conditions, material and indenter geometry. The paper aims to use experimental micro-indentation data, FE simulations with cohesive zone modelling, and an optimisation procedure to determine the cohesive energy density of silicon single crystals. While previous studies available in the literature, which use cohesive zone finite element techniques for simulation of indentation cracks in brittle solids, tried to improve methods for the evaluation of material toughness from the indentation load, crack size, hardness, elastic constants, and indenter geometry, this study focuses on the evaluation of the cohesive energy density 2Γ from which the material toughness can be easily determined using the well-known Griffith-Irwin formula. There is no need to control the premise of the linear fracture mechanics that the cohesive zone is much shorter than the crack length. Hence, the developed approach is suitable also for short cracks for which the linear fracture mechanics premise is violated.

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