Gastric acid challenge of lithium disilicate-reinforced glass-ceramics and zirconia-reinforced lithium silicate glass-ceramic after polishing and glazing-impact on surface properties.

OBJECTIVES: To investigate the impact of simulated gastric acid on the surface properties of lithium disilicate-reinforced glass-ceramics and zirconia-reinforced lithium silicate glass-ceramic after certain polishing and glazing procedures. MATERIALS AND METHODS: Four different types of square-shaped specimens (10 × 10 × 2 mm3, n = 13) were manufactured: lithium disilicate-reinforced glass-ceramic milled and polished (LDS-P); milled, polished, and glazed (LDS-PG); milled, glazed, and no polishing (LDS-G); and milled and polished zirconia-reinforced lithium silicate glass-ceramic (ZR-LS). Specimens were immersed in hydrochloride acid (HCl 0.06 M, pH 1.2) to simulate gastric acid irritation and stored in the acid for 96 h in 37 °C. Specimen weight, surface gloss, Vickers surface microhardness and surface roughness (Ra, Rq, with optical profilometer), and surface roughness on nanometer level (Sq, Sal, Sq/Sal, Sdr, Sds with atomic force microscope) were measured before and after the acid immersion. RESULTS: ZR-LS specimens lost significantly more weight after acid immersion (p = 0.001), also surface microhardness of ZR-LS was significantly reduced (p = 0.001). LDS-G and LDS-PG showed significantly lower surface roughness (Sa, Sq) values compared to LDS-P before (p ≤ 0.99) and after (p ≤ 0.99) acid immersion and ZR-LS after acid immersion (p ≤ 0.99). CONCLUSIONS: Gastric acid challenge affects the surface properties of lithium disilicate-reinforced glass-ceramic and zirconia-reinforced lithium silicate glass-ceramic. Glazing layer provides lower surface roughness, and the glazed surface tends to smoothen after the gastric acid challenge. CLINICAL RELEVANCE: Surface finish of lithium disilicate-reinforced glass-ceramic and zirconia-reinforced lithium silicate glass-ceramic has a clear impact on material's surface properties. Gastric acidic challenge changes surface properties but glazing seems to function as a protective barrier. Nevertheless, also glazing tends to smoothen after heavy gastric acid challenge. Glazing can be highly recommended to all glass-ceramic restorations but especially in patients with gastroesophageal reflux disease (GERD) and eating disorders like bulimia nervosa.

Midline denture base strains of glass fiber-reinforced single implant-supported overdentures.

STATEMENT OF PROBLEM: The fracture incidence of implant-supported overdentures is more frequent in the area of attachment because of stress concentration and denture deformation in this area. How E-glass fiber reinforcement can address this problem is unclear. PURPOSE: The purpose of this in vitro study was to evaluate the influence of unidirectional E-glass fiber reinforcement on the mid-line denture base strains of single implant-supported overdentures. MATERIAL AND METHODS: An experimental acrylic resin cast was constructed with a single implant placed in the mid-line area and a ball attachment screwed to the implant. Twenty-four experimental overdentures were constructed and divided into 4 groups: group AP fabricated from autopolymerizing acrylic resin without fiber reinforcement, group APF fabricated from autopolymerizing acrylic resin with unidirectional E-glass fiber reinforcement running over the residual ridge and the ball matrix, group HP fabricated from heat-polymerized acrylic resin without fiber reinforcement, and group HPF fabricated from heat-polymerized acrylic resin with unidirectional E-glass fiber reinforcement running over the residual ridge and the ball matrix. A biaxial rosette strain gauge was attached to the incisor areas of each overdenture above the attachment level (Ch1, Ch2) and to a multichannel digital strain meter. A static vertical load of 100 N was applied to the first molar area bilaterally by using a universal testing device during strain measurement procedures. The differences in the mean strain and deflection values among the investigated groups were evaluated for statistical significance using 1-way analysis of variance (ANOVA) with the Tukey post hoc multiple comparison (α=.05). RESULTS: The type of acrylic resin did not have a statistically significant effect on the mean strain values among groups (P=.350), while the reinforcement did significantly affect them (P<.001). The interaction between reinforcement and acrylic resin was not statistically significant (P=.552). Both strain gauge channels in group APF and group HPF recorded significantly lower strain values by almost 50% than those of group AP and group HP (P<.05). CONCLUSIONS: Unidirectional E-glass fiber reinforcement placed over the residual ridge and implant attachment significantly reduced denture base strains and deformation of single implant-supported overdentures.

A Polymer for Application as a Matrix Phase in a Concept of In Situ Curable Bioresorbable Bioactive Load-Bearing Continuous Fiber Reinforced Composite Fracture Fixation Plates.

The use of bioresorbable fracture fixation plates made of aliphatic polyesters have good potential due to good biocompatibility, reduced risk of stress-shielding, and eliminated need for plate removal. However, polyesters are ductile, and their handling properties are limited. We suggested an alternative, PLAMA (PolyLActide functionalized with diMethAcrylate), for the use as the matrix phase for the novel concept of the in situ curable bioresorbable load-bearing composite plate to reduce the limitations of conventional polyesters. The purpose was to obtain a preliminary understanding of the chemical and physical properties and the biological safety of PLAMA from the prospective of the novel concept. Modifications with different molecular masses (PLAMA-500 and PLAMA-1000) were synthesized. The efficiency of curing was assessed by the degree of convergence (DC). The mechanical properties were obtained by tensile test and thermomechanical analysis. The bioresorbability was investigated by immersion in simulated body fluid. The biocompatibility was studied in cell morphology and viability tests. PLAMA-500 showed better DC and mechanical properties, and slower bioresorbability than PLAMA-1000. Both did not prevent proliferation and normal morphological development of cells. We concluded that PLAMA-500 has potential for the use as the matrix material for bioresorbable load-bearing composite fracture fixation plates.

Effect of interface surface design on the fracture behavior of bilayered composites.

This study aimed to evaluate the effect of different interface designs on the load-bearing capacity of bilayered composite structures (BLS). Cylindrical specimens of BLS were prepared from base composite of 3.5 mm thickness and surface composite of 1.5 mm thickness (n = 80). Two different base composites - flowable bulk-fill (FBF) [smart dentin replacement (SDR)] and short fiber-reinforced (FRC) (everX Posterior) - were evaluated, and conventional composite (G-aenial Posterior) was used as the surface layer. Four different interface designs were used: (i) pyramidal; (ii) mesh; (iii) linear grooves; and (iv) flat surface (control). Three-dimensional printed molds were fabricated to standardize the interface design between the surface and the base composites. The specimens were then statically loaded with a steel ball until fracture using a universal testing machine. Fracture types were classified into catastrophic, complete, and partial bulk. ANOVA revealed that both the material and the interface design had a statistically significant effect on the load-bearing capacity. Flowable bulk-fill showed lower mean load-bearing capacity than FRC in all the interface designs tested, except for the flat surface design. Fracture analysis showed that FRC demonstrated up to 100% partial bulk fractures with the pyramid interface design, but no incidence of catastrophic bulk fracture. By contrast, FBF demonstrated up to 84.6% and 40% catastrophic bulk fractures with the flat interface design but no incidence of partial bulk fracture. Consequently, the interface designs studied enhanced the fracture behavior of BLS.

Effect of Long-Term Brushing on Deflection, Maximum Load, and Wear of Stainless Steel Wires and Conventional and Spot Bonded Fiber-Reinforced Composites.

Fiber-reinforced composite (FRC) retainers are an aesthetic alternative to conventional Stainless Steel splints. They are generally used with a full bonded technique, but some studies demonstrated that they could be managed with a spot bonding technique to significantly decrease their rigidity. In order to propose this FRC spot bonding technique for clinical use, the aim of this study was to evaluate mechanical properties and surface wear of fibers left uncovered. Tests were made by simulating tooth brushing, comparing FRC spot bonding technique splints with stainless steel and FRC traditional technique splints. Specimens were tested both at 0.1 mm of deflection and at maximum load, showing higher values of rigidity for the FRC full bonded technique. After tooth brushing, no significant reduction in values at 0.1 mm deflection was reported, while we found a similar reduction in these values for the Stainless Steel and FRC spot bonding technique at maximum load, and no significant variation for the FRC full bonded technique. SEM images after tooth brushing showed wear for FRC fibers left uncovered, while no relevant wear signs in metal and conventional FRC fibers were noticed. Results showed that FRC spot bonding technique has advantages in mechanical properties when compared to the FRC traditional full bonding technique, also after tooth brushing. However, the surface wear after tooth brushing in the FRC spot bonding technique is considerable and other tests must be performed before promoting this technique for routine clinical use.

Fatigue resistance of a simulated single LOCATOR overdenture system.

STATEMENT OF PROBLEM: The incidence of fracture in a single-implant overdenture base increases in the region adjacent to the fulcrum implant. PURPOSE: The purpose of this in vitro study was to evaluate the effect of bidirectional woven electrical glass (E-glass) fiber reinforcements on the fatigue resistance of a simulated single LOCATOR-retained overdenture. MATERIAL AND METHODS: Test specimens with a centrally positioned metal housing for a LOCATOR stud attachment were fabricated from autopolymerizing acrylic resin. Specimens for the control group were fabricated without glass fiber reinforcements. The 4L group specimens had 4 layers of E-glass fiber weaves and were divided according to the fiber location into the following 3 subgroups: 4L-A with 4 fiber layers above the metal housing; 4L-N with 4 fiber layers adjacent to the metal housing; and 4L-A+4L-N with 4 fiber layers above and 4 fiber layers adjacent to the housing. Specimens were stored in distilled water for 1 week at 23 °C before cyclic fatigue testing at 10 000 cycles by using a staircase approach (n=12). The results were analyzed with 1-way ANOVA and the Tukey multiple comparisons post hoc analysis (α=.05). A 2-way ANOVA (α=.05) was conducted to detect the effect of fatigue cyclic loading and the position of the fiber layers and their interaction on the fatigue resistance. RESULTS: The results of the investigated compressive fatigue limits for the test groups were 190 ±15.9 N for the control group, 265 ±15.9 N for the 4L-A subgroup, 220 ±15.9 N for the 4L-N subgroup, and 275 ±15.9 N for the 4L-A+4L-N subgroup. A nonsignificant difference was found for creep values between the control group and reinforced subgroups (P>.05). The postfatigue flexural strength values in the 4L-A and 4L-A+4L-N subgroups were significantly higher than those in the control group (P<.001) and the 4L-N subgroup (P=.004 and P=.005). However, no significant difference was found in postfatigue flexural strength between the control group and the 4L-N subgroup (P=.828). CONCLUSIONS: Placing 4 layers of bidirectional E-glass fiber weaves above the metal housing can increase the fatigue resistance and the postfatigue flexural strength of single LOCATOR-retained overdentures.

Immediate Repair Bond Strength of Fiber-reinforced Composite after Saliva or Water Contamination.

PURPOSE: This in vitro study aimed to evaluate the shear bond strength (SBS) of particulate filler composite (PFC) to saliva- or water-contaminated fiber-reinforced composite (FRC). MATERIALS AND METHODS: One type of FRC substrate with semi-interpenetrating polymer matrix (semi-IPN) (everStick C&B) was used in this investigation. A microhybrid PFC (Filtek Z250) substrate served as control. Freshly cured PFC and FRC substrates were first subjected to different contamination and surface cleaning treatments, then the microhybrid PFC restorative material (Filtek Z250) was built up on the substrates in 2-mm increments and light cured. Uncontaminated and saliva- or water-contaminated substrate surfaces were either left untreated or were cleaned via phosphoric acid etching or water spray accompanied with or without adhesive composite application prior applying the adherent PFC material. SBS was evaluated after thermocycling the specimens (6000 cycles, 5°C and 55°C). RESULTS: Three-way ANOVA showed that both the surface contamination and the surface treatment signficantly affected the bond strength (p < 0.05). Saliva contamination reduced the SBS more than did the water contamination. SBS loss after saliva contamination was 73.7% and 31.3% for PFC and FRC, respectively. After water contamination, SBS loss was 17.2% and 13.3% for PFC and FRC, respectively. The type of surface treatment was significant for PFC (p < 0.05), but not for FRC (p = 0.572). CONCLUSION: Upon contamination of freshly cured PFC or semi-IPN FRC, surfaces should be re-prepared via phosphoric acid etching, water cleaning, drying, and application of adhesive composite in order to recover optimal bond strength.

Load-bearing capacity of simulated Locator-retained overdenture system.

STATEMENT OF PROBLEM: Acrylic resin overdenture bases usually fracture because of stress concentrations at the area of the abutments. PURPOSE: The purpose of this study was to evaluate the reinforcing effect of bidirectional woven electrical glass (E-glass) fiber weaves with a different number of layers and different locations on the load-bearing capacity of simulated Locator-retained overdenture specimens. MATERIAL AND METHODS: Test specimens with a centrally located metal housing for a Locator stud attachment were fabricated from autopolymerizing acrylic resin (polymethylmethacrylate based) and reinforced with bidirectional woven E-glass fiber layers. The control group specimens were fabricated without fiber reinforcement. The 2L group had 2 layers of E-glass fiber weaves and was divided according to the fiber location within the specimens as follows: 2L-A subgroup with 2 fiber layers above the metal housing; 2L-N subgroup with 2 fiber layers adjacent to the housing; and 2L-A+2L-N subgroup with 2 fiber layers above and 2 fiber layers adjacent to the housing. The 4L group had 4 layers of E-glass fiber weaves and was divided according to the fiber location as follows: 4L-A subgroup with 4 fiber layers above the housing; 4L-N subgroup with 4 fiber layers adjacent to the housing; and 4L-A+4L-N subgroup with 4 fiber layers above and 4 fiber layers adjacent to the housing. Dry specimens were submitted to a 3-point static loading test, and the mean flexural strength, flexural modulus, and strain values were analyzed with 1-way ANOVA and Tukey post hoc tests (α=.05). Two-way ANOVA was conducted to detect the influence of the number and location of the reinforcing layers (α=.05). RESULTS: The results revealed a significant difference (P<.001) in flexural strength values between the control group (92.4 ±14 MPa) and the 2 subgroups, 4L-A (116 ±7.3 MPa) and 4L-A+4L-N (117.1 ±6 MPa), with a significant effect only from the number of the reinforcing layers (P<.001) and not the location (P=.153). No significant differences were found with flexural modulus (P=.195) and strain values (P=.174) among the tested groups. CONCLUSIONS: The load-bearing capacity of a Locator-retained overdenture can be significantly increased by placing 4 layers of bidirectional woven E-glass fiber weaves either only above the metal housing or in both locations above and adjacent to the metal.

Fracture Strength and Precision of Fit of Implant-Retained Monolithic Zirconia Crowns.

New monolithic zirconia materials can be used to fabricate full-contour fixed dental prostheses with the computer-aided design/computer-aided manufacturing (CAD/CAM) method. The aim of this study was to examine the fracture strength and precision of fit of screw-retained monolithic zirconia crowns made directly on implants or by cementing on prefabricated titanium (Ti) bases. Monolithic screw-retained implant crowns (n = 6) were produced by CAD/CAM method using partially (PSZ) and fully stabilized (FSZ) zirconia. Industrially produced zirconia crowns were used as a reference. A lateral incisor study model was made onto an implant replica. Crowns were produced either directly on the implant or through cementing on a prefabricated titanium base (PSZ+Ti, FSZ+Ti). The crowns were tightened to implant replicas with a torque of 35 Ncm. The gap between the replica and the abutment or crown was measured from ×400 scanning electron microscope images for precision of fit. Mechanical testing until failure was completed with a universal testing machine with loading angle of 45°. Statistical analysis was performed (analysis of variance). Mean (±SD) failure loads were 259 ± 23 (PSZ), 140 ± 13 (FSZ), 453 ± 25 (PSZ+Ti), 439 ± 41 (FSZ+Ti), and 290 ± 39 (Procera). Mean (±SD) gap values were 2.2 ± 0.2 (PSZ), 2.5 ± 1.0 (FSZ), 7.0 ± 1.0 (PSZ+Ti), 7.7 ± 1.6 (FSZ+Ti), and 6.7 ± 1.7 (Procera). Monolithic zirconia crowns with a Ti base clearly show higher fracture strengths than the crowns fixed directly on the implant surface. Better marginal fit can be achieved with direct zirconia crowns than with crowns on a titanium base or industrially produced zirconia crowns.

The effect of smear layer removal on E. faecalis leakage and bond strength of four resin-based root canal sealers.

BACKGROUND: The aim of the study was to assess bacterial sealability and bonding ability of methacrylate-based Resilon (RS, SybronEndo), Endo Rez (ER, Ultradent Products Inc), and epoxy-based AH Plus (AH, Dentsply/DeTrey), MTA Fill Apex (MTAF, Angelus Soluções Odontológicas) root canal sealers, and the effect of the smear layer removal on the sealability. METHODS: One hundred thirty root segments were instrumented up to apical size #60 and rinsed with 2.5% NaOCl. Half of the roots were rinsed with 5ml 17% EDTA to remove the smear layer. All the roots were filled with AH, ER, MTAF sealers and gutta-percha, or RS with Resilon cones. After storage at 37°C for 7 days the samples were mounted into bacterial leakage assay for 50 days. Another 100 roots were instrumented and rinsed as described above, split longitudinally, cut into the cervical, middle and apical parts. The sealers were injected through the plastic mould on the dentin surface. After 7 days of incubation at 37°C, bond strength was tested using a notched-edge test fixture (Crosshead, Ultradent Products Inc.) and a universal testing machine (Lloyd Instruments). RESULTS: AH revealed the longest mean time for bacterial resistance by 29.4 and 36.8 days (with and without smear layer, respectively) followed by RS (15.1 and 24.7 days, respectively). The difference between materials was significant (p<0.001). Bond strength values ranged from 0.2± 0.1 to 3.5± 0.7 MPa and increased from the apical to the cervical third. In the apical third, AH showed the highest mean (SD) bond values 1.4 (0.4) MPa and 1.7 (0.6) MPa (with and without smear, respectively, followed by RS, 0.5 (0.1) MPa and 0.8 (0.1) MPa, respectively. The difference between materials was significant (p=0.001). CONCLUSION: The effect of the smear layer removal on the sealability was material-dependent.

Light Transmission of Novel CAD/CAM Materials and Their Influence on the Degree of Conversion of a Dual-curing Resin Cement.

PURPOSE: To evaluate the light transmission characteristics of different types, shades, and thicknesses of novel CAD/CAM materials and their effect on the degree of conversion (DC) of a dual-curing resin cement. MATERIALS AND METHODS: Square specimens (12 × 12 mm2) of three CAD/CAM materials - GC Cerasmart, Lava Ultimate, Vita Enamic - of different thicknesses (1.00, 1.50, and 2.00 mm, n = 5 per thickness) were irradiated with an LED unit. The amount of transmitted light was quantified. Thereafter, the DC% of the dual-curing resin cement (RelyX Ultimate) was recorded after 15 min using Fourier transform infrared spectroscopy. Statistical analysis was performed using two-way ANOVA followed by the Tukey's HSD post-hoc test at a significance level of p < 0.05. Regression analysis was performed to investigate the correlation between the DC and radiant energy, and the DC and thickness. RESULTS: Although the type and shade of CAD/CAM material significantly affect transmitted light irradiation (p < 0.0001), degrees of conversion are similar when the CAD/CAM material or material shade were taken into consideration (p > 0.05). Conversely, material thickness significantly affected light transmission (p < 0.0001) and DC (p < 0.0001). Multiple effects of material, shade, and thickness did not significantly affect the evaluated parameters (p = 0.638 for light irradiation; p = 0.637 for DC). Linear regression analysis showed a correlation between delivered energy and DC% results of the Vita Enamic (R²â€¯= 0.4169, p < 0.0001). CONCLUSION: Reduced light transmission in 2-mm-thick specimens of all CAD/CAM materials indicates that proper curing of the cement beneath CAD/CAM materials should be ensured.

Influence of increment thickness on dentin bond strength and light transmission of composite base materials.

OBJECTIVES: Bulk-fill resin composites (BFCs) are gaining popularity in restorative dentistry due to the reduced chair time and ease of application. This study aimed to evaluate the influence of increment thickness on dentin bond strength and light transmission of different BFCs and a new discontinuous fiber-reinforced composite. MATERIALS AND METHODS: One hundred eighty extracted sound human molars were prepared for a shear bond strength (SBS) test. The teeth were divided into four groups (n = 45) according to the resin composite used: regular particulate filler resin composite: (1) G-ænial Anterior [GA] (control); bulk-fill resin composites: (2) Tetric EvoCeram Bulk Fill [TEBF] and (3) SDR; and discontinuous fiber-reinforced composite: (4) everX Posterior [EXP]. Each group was subdivided according to increment thickness (2, 4, and 6 mm). The irradiance power through the material of all groups/subgroups was quantified (MARC® Resin Calibrator; BlueLight Analytics Inc.). Data were analyzed using two-way ANOVA followed by Tukey's post hoc test. RESULTS: SBS and light irradiance decreased as the increment's height increased (p < 0.05), regardless of the type of resin composite used. EXP presented the highest SBS in 2- and 4-mm-thick increments when compared to other composites, although the differences were not statistically significant (p > 0.05). Light irradiance mean values arranged in descending order were (p < 0.05) EXP, SDR, TEBF, and GA. CONCLUSIONS: As increment thickness increased, the light transmission decreased for all tested resin composites. Discontinuous fiber-reinforced composite showed the highest value of curing light transmission, which was also seen in improved bonding strength to the underlying dentin surface. CLINICAL RELEVANCE: Discontinuous fiber-reinforced composite can be applied safely in bulks of 4-mm increments same as other bulk-fill composites, although, in 2-mm thickness, the investigated composites showed better performance.

Mechanical properties, fracture resistance, and fatigue limits of short fiber reinforced dental composite resin.

STATEMENT OF PROBLEM: Cycling masticatory loads decrease the strength of particulate filler composites (PFCs) and initiate the failure process by fatigue. The life expectancy of a composite resin restoration under stress remains difficult to predict. PURPOSE: The purpose of this study was to determine the fracture resistance and the compressive fatigue limits (CFL) of anterior crown restorations made of a short-fiber reinforced composite resin (SFC), to investigate selected mechanical properties of the material following standard test methods, and to observe their correlation with the CFL. MATERIAL AND METHODS: Specimens (n=10) were fabricated either from SFC (everX Posterior, GC Corp) or PFC (G-ænial anterior, GC Corp). The properties investigated were flexural strength (FS), compression strength (CS), diametral-tensile strength (DTS), and single-edge-notched-bend fracture toughness (FT) following ISO standards. Fracture resistance was determined by static load (n=10) and the CFL at 10000 cycles was determined using a staircase approach (n=20), both on anterior composite resin crowns. The results were analyzed with 1-way ANOVA (α=.05) or 2-way ANOVA (α=.05) followed by a Tukey B post hoc test and the Pearson-correlation analysis. RESULTS: The SFC crowns had higher fracture resistance (954 ±121 N) than the PFC crowns (415 ±75 N) (P<.001) and higher CFL (267 ±23 N) than the PFC crowns (135 ±64 N) (P<.001). SFC revealed also higher FT (2.6 ±0.6 MPa·m(1/2)) than the PFC (1.0 ±0.2 MPa·m(1/2)) (F=69.313, P<.001). A significant correlation was observed only between the FT and the CFL (r(2)=0.899; P<.001). CONCLUSIONS: SFC crowns showed good performance under static and fatigue loading. FT was the only in vitro test method that filtered as a clinically relevant parameter.

Surface roughness and the flexural and bend strength of zirconia after different surface treatments.

STATEMENT OF PROBLEM: Different surface treatments are commonly used during the fabrication of zirconia fixed dental prostheses. However, such treatments can affect the properties of the zirconia framework material. PURPOSE: The purpose of this in vitro study was to determine the effect of different surface treatments on the surface roughness and flexural and bend strength of zirconia. MATERIAL AND METHODS: Seventy-two zirconia disks (n=8) and 72 zirconia bars (n=8) were sintered and divided into 9 groups for different surface treatments: sintered control, airborne-particle abraded with 50-µm aluminum oxide, airborne-particle abraded with Rocatec soft (30 µm), airborne-particle abraded with Rocatec (105 µm), grinding dry with a micromotor, turbine grinding under water cooling, grinding with silicon carbide paper, diamond paste polishing, and steam cleaning. The biaxial flexural strength of the disks (diameter 19 mm, thickness 1.6 mm) and 3-point bend test of the bars (thickness 2 mm, height 2 mm, length 25 mm) were measured dry at room temperature. One-way ANOVA followed by the Tukey HSD test (α=.05) and Pearson correlation test were used for statistical analysis. RESULTS: Airborne-particle abrasion and silicon carbide paper grinding increased the flexural and bend strength of zirconia specimens (P<.05). The 3-point bend test gave 20% to 30% higher strength values than the biaxial test, but a strong correlation was shown between the test types. Surface roughness had a statistically significant negative effect on the strength values in the 3-point bend test. CONCLUSIONS: The surface treatments tested affected the strength and surface roughness of zirconia framework material.

Oxygen inhibition layer of composite resins: effects of layer thickness and surface layer treatment on the interlayer bond strength.

An oxygen inhibition layer develops on surfaces exposed to air during polymerization of particulate filling composite. This study assessed the thickness of the oxygen inhibition layer of short-fiber-reinforced composite in comparison with conventional particulate filling composites. The effect of an oxygen inhibition layer on the shear bond strength of incrementally placed particulate filling composite layers was also evaluated. Four different restorative composites were selected: everX Posterior (a short-fiber-reinforced composite), Z250, SupremeXT, and Silorane. All composites were evaluated regarding the thickness of the oxygen inhibition layer and for shear bond strength. An equal amount of each composite was polymerized in air between two glass plates and the thickness of the oxygen inhibition layer was measured using a stereomicroscope. Cylindrical-shaped specimens were prepared for measurement of shear bond strength by placing incrementally two layers of the same composite material. Before applying the second composite layer, the first increment's bonding site was treated as follows: grinding with 1,000-grit silicon-carbide (SiC) abrasive paper, or treatment with ethanol or with water-spray. The inhibition depth was lowest (11.6 µm) for water-sprayed Silorane and greatest (22.9 µm) for the water-sprayed short-fiber-reinforced composite. The shear bond strength ranged from 5.8 MPa (ground Silorane) to 36.4 MPa (water-sprayed SupremeXT). The presence of an oxygen inhibition layer enhanced the interlayer shear bond strength of all investigated materials, but its absence resulted in cohesive and mixed failures only with the short-fiber-reinforced composite. Thus, more durable adhesion with short-fiber-reinforced composite is expected.

Three-dimensional finite element analysis of anterior two-unit cantilever resin-bonded fixed dental prostheses.

The aim of this study was to evaluate the influence of different framework materials on biomechanical behaviour of anterior two-unit cantilever resin-bonded fixed dental prostheses (RBFDPs). A three-dimensional finite element model of a two-unit cantilever RBFDP replacing a maxillary lateral incisor was created. Five framework materials were evaluated: direct fibre-reinforced composite (FRC-Z250), indirect fibre-reinforced composite (FRC-ES), gold alloy (M), glass ceramic (GC), and zirconia (ZI). Finite element analysis was performed and stress distribution was evaluated. A similar stress pattern, with stress concentrations in the connector area, was observed in RBFDPs for all materials. Maximal principal stress showed a decreasing order: ZI>M>GC>FRC-ES>FRC-Z250. The maximum displacement of RBFDPs was higher for FRC-Z250 and FRC-ES than for M, GC, and ZI. FE analysis depicted differences in location of the maximum stress at the luting cement interface between materials. For FRC-Z250 and FRC-ES, the maximum stress was located in the upper part of the proximal area of the retainer, whereas, for M, GC, and ZI, the maximum stress was located at the cervical outline of the retainer. The present study revealed differences in biomechanical behaviour between all RBFDPs. The general observation was that a RBFDP made of FRC provided a more favourable stress distribution.

Degree of conversion of dual-polymerizing cements light polymerized through monolithic zirconia of different thicknesses and types.

STATEMENT OF PROBLEM: Monolithic zirconia restorations are increasingly common. Dual-polymerizing cements have been advocated for cementation. The opacious nature of zirconia restoration can attenuate light, compromising optimal resin polymerization and eventually restoration debonding. PURPOSE: The purpose of this in vitro study was to evaluate the influence of material thickness on light irradiance, radiant exposure, and the degree of monomer conversion (DC) of 2 dual-polymerizing resin cements light-polymerized through different brands of monolithic zirconia. MATERIAL AND METHODS: Dual-polymerizing resin cements (RelyX Ultimate; 3M-ESPE, and Variolink II; Ivoclar, Vivadent) were mixed according to the manufacturers' instructions with a film thickness of 40 µm, placed under a 10 × 10 mm specimen of monolithic zirconia (Prettau Anterior by Zirkonzahn, Katana by Noritake, BruxZir by Glidewell, and Zenostar by Wieland) and a zirconia core control (ICE zirkon by Zirkonzahn) at various thicknesses (0.50, 1.00, 1.50, and 2.00 mm, n = 5 of each thickness). Each specimen was irradiated for 20 seconds (RelyX Ultimate) and 40 seconds (Variolink II) with Elipar S10 (3M-ESPE, 1200 mW/cm(2)). The amount of irradiance and radiant exposure was quantified for each specimen. Fourier transform infrared spectroscopy was used to measure the DC from the bottom surface of the resin. Statistical analysis was performed with 2-way ANOVA and post hoc Tukey honest significant difference (HSD) tests (α = .05). RESULTS: Light irradiance and radiant exposure decreased as the thickness of the specimen increased (P < .05) regardless of the brand. The ranking from least to highest was BruxZir < ICE zircon = Wieland < Katana = Prettau Anterior. The zirconia brand, thickness, and cement type had a significant effect on the DC (P < .001). The DC decreased significantly as the thickness of the zirconia increased (P < .001). Katana and Prettau Anterior showed the highest DC and BruxZir showed the lowest. CONCLUSION: The thickness of zirconia affects the DC of resin-based cements. The DC of the resin cements differed significantly between cements and among zirconia brands. More polymerizing time may be needed to deliver sufficient energy through some brands of zirconia.

Load-Bearing Capacity of Fiber-Reinforced Composite Abutments and One-Piece Implants.

Fiber-reinforced composites (FRC) can potentially help in a physiologic stress transmission due to its excellent biomechanical matching with living tissues. Novel one-piece FRC implants and abutments with two different fiber orientations were loaded until failure to assess the load-bearing capacity, fracture patterns, and precision of fit. The one-piece FRC implants showed significantly higher load-bearing capacity compared to FRC abutments regardless of the fiber orientation (p < 0.001). For FRC abutments, bidirectional abutments showed significantly higher loads compared to unidirectional abutments (p < 0.001). The type of structure and fiber orientation are strong determinant factors of the load-bearing capacity of FRC implants and abutments.

Optimizing the concentration of quaternary ammonium dimethacrylate monomer in bis-GMA/TEGDMA dental resin system for antibacterial activity and mechanical properties.

Four novel quaternary ammonium dimethacrylate monomers named IMQ (side alkyl chain length from 12 to 18) were synthesized with the aim to synthesize dental resin with antibacterial activity. All of IMQs were added into bis-GMA/TEGDMA dental resin system with a series of mass ratio (5, 10, and 20 wt%), double bond conversion (DC), flexural strength (FS), modulus of elasticity (FM) and biofilm formation inhibitory effect were studied. According to the results of DC, FS, FM, and the biofilm inhibitory effect, IMQ-16 containing polymer had the best comprehensive properties, and the optimal concentration of IMQ-16 in bis-GMA/TEGDMA dental resin would be in the range of 5-10 wt%.

Fiber-reinforced composite fixed dental prostheses with various pontics.

PURPOSE: To evaluate the load-bearing capacities of fiber-reinforced composite (FRC) fixed dental prostheses (FDP) with pontics of various materials and thicknesses. MATERIALS AND METHODS: Inlay preparations for retaining FDPs were made in a polymer phantom model. Seventy-two FDPs with frameworks made of continuous unidirectional glass fibers (everStick C&B) were fabricated. Three different pontic materials were used: glass ceramics, polymer denture teeth, and composite resin. The FDPs were divided into 3 categories based on the occlusal thicknesses of the pontics (2.5 mm, 3.2 mm, and 4.0 mm). The framework's vertical positioning varied respectively. Each pontic material category contained 3 groups (n = 8/group). In group 1, pontics were fabricated conventionally with composite resin (G-ӕnial, GC) with one additional transversal fiber reinforcement. In group 2, the pontics were polymer denture teeth (Heraeus- Kulzer). Group 3 had an IPS-Empress CAD pontic (Ivoclar Vivadent) milled using a Cerec CAD/CAM unit. Groups 1 and 2 served as controls. Each FDP was statically loaded from the pontic until initial fracture (IF) and final fracture (FF). Initial-fracture data were collected from the load-deflection graph. RESULTS: ANOVA indicated statistically significant differences between the materials and occlusal thicknesses (p < 0.001). Quadratic analysis demonstrated the highest correlation between the thickness of the pontic and IF and FF values with ceramic pontics (IF: p < 0.001; R2 = 0.880; FF: p < 0.001; R2 = 0.953). CONCLUSION: By increasing the occlusal thickness of the pontic, the load-bearing capacity of the FRC FDPs may be increased. The highest load-bearing capacity was obtained with 4.0 mm thickness in the ceramic pontic. However, with thinner pontics, polymer denture teeth and composite pontics resulted in higher load-bearing values.