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1.
Materials (Basel) ; 17(16)2024 Aug 17.
Artigo em Inglês | MEDLINE | ID: mdl-39203266

RESUMO

In the serviced components of a 7075 aluminum alloy, the propagation of fatigue crack can be retarded because of the overload effect; however, the corresponding retardation mechanisms are complex. To provide further insights into the retardation mechanisms of 7075 aluminum alloys, this study addresses the crack tip damage response of a cracked 7075 aluminum alloy under an overload effect. Based on the dual-scale modeling approach and the damage-coupled crystal plasticity model, the effect of the microstructure of a 7075 aluminum alloy on the damage behavior ahead of the crack tip under an overload was studied. The factors affecting fatigue damage accumulation ahead of the crack tip, such as dislocation density, the variation in the activities of slip systems, and the orientation effect of the nearest neighbor grains, are described. The results show that for the 7075 aluminum alloy, the compressive residual stress induced by the overload effect not only decreases the number of activated slip systems, but also lowers the rate of increase in dislocation density. This causes a decrease in fatigue damage accumulation during deformation. Moreover, the overload effect decreases the slip system activity as well as the resultant plastic slip; however, the decrease in plastic slip varies with the grain orientation, indicating that the overload effect depends on the grain orientation. It can also be found that both the damage strain energy release rate and lattice strain are influenced by the orientation of the nearest neighbor grains, which can eventually affect the overload effect. These findings contribute to understanding the retardation mechanisms from a microscopic perspective and provide guidance on improving the material design of a 7075 aluminum alloy to some extent.

2.
Micromachines (Basel) ; 14(11)2023 Oct 30.
Artigo em Inglês | MEDLINE | ID: mdl-38004874

RESUMO

The Ni60-SiC-CeO2 strengthening layer with deep remelting pools was constructed on the surface of 7075 aluminum alloy using the laser remelting-cladding processing method, and a soft and hard interphase was prepared on the matrix by the interval of laser remelting, which was inspired by soft-hard interphase structure with excellent crack inhibition performance from the natural world. The microstructure and microhardness of the remelting region and the remelting-cladding region of the strengthening layer were studied. The tensile characteristics of two distinct strengthening layers were investigated in the laboratory. The results showed that the grain size of remelting pools is finer, and the microhardness is higher than that of the matrix, which makes crack propagation more difficult. In addition, the results show that the strengthening layer has compact and flawless microstructure and has been metallurgically integrated with the matrix, and the microhardness of the regions treated by laser cladding and laser remelting-cladding has been improved obviously. Toughness has improved, as has the problem of toughness reduction after cladding ceramic particles. The sample's strength is also significantly greater than that of the untreated sample.

3.
Materials (Basel) ; 16(18)2023 Sep 10.
Artigo em Inglês | MEDLINE | ID: mdl-37763423

RESUMO

The non-dendritic microstructure plays a crucial role in determining the rheological properties of semi-solid alloys, which are of the utmost importance for the successful industrial application of the thixoforging process. To further understand the impact of the reheating process on the evolution of microstructure and thixotropic deformation behavior in the semi-solid state, a hot extruded and T6 treated 7075 aluminum alloy was reheated to the selected temperature ranges using varying heating rates. Subsequently, thixo-compression tests were performed. The study found that during reheating and isothermal holding, the elongated microstructure of the as-supplied alloy can transform into equiaxed or spherical grains. The presence of recrystallized grains was found to be closely linked to the penetration of the liquid phase into the recrystallized grain boundaries. Furthermore, it was observed that higher heating rates resulted in smaller grain sizes. The thixotropic flow behavior of the alloy with various microstructures was analyzed using the true stress-strain curves obtained by thixo-compression experiments, which exhibited three stages: a rapid increase in true stress to a peak value, followed by a decrease in true stress and a steady stress until the end of compression. The stress fluctuated with strain during the formation of the slurry at a strain rate of 10 s-1, indicating the significant role of strain rate in material flow during semisolid formation.

4.
Materials (Basel) ; 16(23)2023 Nov 29.
Artigo em Inglês | MEDLINE | ID: mdl-38068175

RESUMO

The investigation of thermal deformation behavior plays a significant role in guaranteeing the overall performance of alloy materials. In this manuscript, a series of isothermal compression tests at different temperatures (300, 350, 400, and 450 °C) and strain rates (0.001, 0.01, 0.1, and 1 s-1) were conducted to study the thermal deformation behavior of 7075 aluminum alloy. Subsequently, processing maps at a strain from 0.4 to 1.39 were established according to the stress-strain data obtained from various deformation parameters. The microstructural evolution of the target alloy was observed with an optical microscope and transmission electron microscope. The results reveal the unstable regions are located at (360-450 °C, 0.04-1 s-1) and (300-315 °C, 0.01-0.22 s-1). Precipitation particles, pinned dislocations, and highly dislocated areas can be observed in the microstructure of the alloy in the unstable regions. This is a potential crack and defect formation point. The identified optimum processing parameters are located at (375-450 °C, 0.001-0.03 s-1), with a maximum dissipation efficiency of 0.6.

5.
Micromachines (Basel) ; 14(2)2023 Feb 10.
Artigo em Inglês | MEDLINE | ID: mdl-36838118

RESUMO

In the context of energy conservation and emission reduction, more and more attention has been paid to the development of lightweight metal materials with both high strength and high toughness. Inspired by the non-smooth surface of natural organisms, a biomimetic surface with various spacing reticulate units of 7075 aluminum alloys was modified by laser cladding. The microstructure, microhardness and tensile properties of the various spacing units with CeO2-SiC-Ni60 were studied. The finer microstructure and the higher microhardness of various spacing units in comparison with that of 7075 aluminum alloys were obtained, no matter the strip-like treated region or the cross-junction region. Moreover, the best combination of strength and toughness of the biomimetic sample with 2.5 mm spacing reticulate unit was discussed. Finally, by combining the microstructure, XRD phase change, thermal gradient effect, thermal expansion coefficient difference and hard phase strengthening mechanism, it was concluded that the 2.5 mm spacing reticulate unit had the best ability to inhibit crack propagation, and the dispersive hard phases of Al3Ni2 and SiC played a major role in stress release of the matrix.

6.
Materials (Basel) ; 16(16)2023 Aug 14.
Artigo em Inglês | MEDLINE | ID: mdl-37629906

RESUMO

The materials with grain size gradient variation on the surface, which were prepared with mechanical-induced severe plastic deformation, always show high resistance to high and low cycle fatigue and frictional wear because of their good strength-ductility synergy. The ultrasonic surface rolling treatment (USRT) has the advantages of high processing efficiency, good surface quality, and large residual compressive stress introduced to the surface after treatment. The USRT was used to prepare aluminum alloy (AA7075) samples with a surface gradient structure; meanwhile, the microstructural evolution mechanism of the deformation layers on the gradient structure was studied with XRD, SEM, and TEM. The microstructure with gradient distribution of grain size and dislocation density formed on the surface of AA7075 aluminum alloy after USRT. The surface layer consists of nanocrystals with random orientation distribution, and high-density dislocation cells and subgrains formed in some grains in the subsurface layer, while the center of the material is an undeformed coarse-grained matrix. The results show that the dislocation slip dominates the grain refinement process, following the continuous cutting and refinement of dislocation cells, subgrains, and fragmentation of the second precipitates. This study systematically clarified the mechanism of grain refinement and nanocrystallization on the surface of high-strength aluminum alloys and laid a theoretical foundation for further research on mechanical behavior and surface friction and wear properties of high-strength non-ferrous materials with gradient structure.

7.
Materials (Basel) ; 16(3)2023 Jan 27.
Artigo em Inglês | MEDLINE | ID: mdl-36770118

RESUMO

Multiple cold expansion holes are widely used in connection areas of aircraft structures, in order to achieve uniform load transfer of the skin or connection parts. Split sleeve cold expansion (SSCE) is widely used to enhance the fatigue life of fastener holes by applying compressive residual stresses around the holes. In this study, the finite element method (FEM) was used to research the distribution and variation of residual stresses along the hole edges of 7075AA single-hole and multi-hole cold expansion (CE) specimens. Full-field strain measurements of single-hole and multi-hole specimens were performed using two-dimensional digital image correlation (DIC), and the residual stress and strain at the hole edge of the specimens measured by FEM and DIC were compared. FEM results shows that the maximum circumferential and radial residual stresses of three-hole specimens with three-hole spacing are increased by 5.37% and 31.53% compared with single-hole specimens. The maximum circumferential residual stress of three-hole specimens with four-hole spacing increases by 7.25% compared with a single hole, but the radial residual stress decreases by 12.98%. In addition, for three-hole specimens with hole spacing three times the hole diameter, the strengthening effect of SSCE in the order of middle hole, then left hole, and, finally, right hole is better than that of SSCE in the order of left to right hole. FEM and DIC full-field strain results are basically consistent.

8.
Micromachines (Basel) ; 14(12)2023 Nov 30.
Artigo em Inglês | MEDLINE | ID: mdl-38138353

RESUMO

The 7075 aluminum alloy deep hole pipe finds extensive applications in the aerospace industry due to its remarkable attributes, such as high strength, exceptional wear resistance, and favorable mechanical properties. However, traditional boring processes for 7075 aluminum alloy deep hole pipes tend to generate elevated cutting forces, potentially leading to deformation issues in these deep holes. In response to these challenges, this study introduces a novel approach involving the use of a two-dimensional ultrasonic elliptical vibration tool. This tool features a single excitation asymmetric structure and aims to enhance the deep hole machining process in 7075 aluminum alloy. The research methodology involved several key steps. First, theoretical analysis and simulation were performed to study the motion trajectory of the cutting edge of the tool. Second, practical experiments were conducted comparing two-dimensional ultrasonic elliptical vibration boring with conventional boring for 7075 aluminum alloy deep hole pipes. The results demonstrate that, in contrast to conventional boring, two-dimensional ultrasonic vibration boring could achieve a maximum reduction of 54.1% and an average reduction of 50.4% in the roundness value of the deep holes. The impact of machining parameters on deep hole roundness is assessed through experimental analysis, leading to the determination of optimal processing parameters. In summary, this experimental research has a certain reference significance for the application of 7075 aluminum alloy deep hole parts in the aerospace field.

9.
Materials (Basel) ; 16(20)2023 Oct 21.
Artigo em Inglês | MEDLINE | ID: mdl-37895782

RESUMO

In this study, 7075 aluminum alloy welding wire with TiB2 nanoparticle reinforcement as an additive together with the variable polarity TIG welding arc as a heat source were applied to produce thin-walled deposited layer samples. Results indicated that the performance of the deposited structure of 7075 aluminum alloy with a TiB2 reinforcement phase was significantly improved compared to the deposited structure of ordinary 7075 aluminum alloy welding wire. Meanwhile, the precipitation of the TiB2 reinforcement phase was insufficient within the structure, and the enhancing effect could not be fully exerted. Moreover, the 7-series aluminum alloy contained a large amount of Zn and Mg elements inside. If the soluble crystalline phase was not fully dissolved, severe stress corrosion could be caused, which inevitably led to a decrease in the mechanical properties. To further improve the performance of the deposited layer, a T6 heat treatment process was performed at 470 °C for 2 h, followed by rapid cooling with distilled water and artificial aging at 120 °C for 24 h. After heat treatment, many second phases appeared in the microstructure of the deposited layer, and the tensile strength increased from (361.8 ± 4.8) MPa to (510.2 ± 5.4) MPa together with the elongation which increased from (9.5 ± 0.5) % to (10.2 ± 0.4) %. The fracture mode of the fracture was a ductile fracture along grain boundaries. The microhardness increased from (145 ± 5) HV to (190 ± 4) HV and exhibited good corrosion resistance in a 3.5% NaCl solution corrosion test.

10.
Materials (Basel) ; 15(24)2022 Dec 17.
Artigo em Inglês | MEDLINE | ID: mdl-36556850

RESUMO

The optimization of a broach surface is of great significance to improve the cutting performance of the tool. However, the traditional optimization method (surface texture, coating, etc.) destroys the stress distribution of the tool and reduces the service life of the tool. To avoid these problems, four kinds of flocking surfaces (FB1, FB2, FB3, and FB4), imitating the biological structure of Daphniphyllum calycinum Benth (DCB), were fabricated on the rake face of the broach by electrostatic flocking. The broaching experiment, wettability, and spreading experiment were then conducted. Moreover, the mathematical model of the friction coefficient of the bionic broach was built. The effect of broaches with different flocking surfaces on the broaching force, chip morphology, and surface quality of workpieces was studied. The results indicate that the flocked broaches (FB) with good lubricity and capacity of microchips removal (CMR) present a smaller cutting force (Fc) and positive pressure (Ft) compared to the unflocked broach (NB), and reduce the friction coefficient (COF). The chip curl was decreased, and the shear angle was increased by FB, which were attributed to the function of absorbing lubricant, storing, and sweeping microchips. Its vibration suppression effect enhanced the stability in the broaching process and improved the surface quality of the workpiece. More importantly, the FB2 with the most reasonable fluff area and spacing exhibited the best cutting performance. The experimental conclusions and methods of this paper can provide a new research idea for functional structure tools.

11.
Materials (Basel) ; 15(20)2022 Oct 12.
Artigo em Inglês | MEDLINE | ID: mdl-36295160

RESUMO

The necking phenomenon of metal sheet under high temperatures is serious and continues over a longer duration. It is difficult to describe the high-temperature mechanical properties of materials only on the basis of hardening behavior before necking. To obtain the high-temperature stress-strain curve considering diffuse necking stage, a forward identification method based on strain measurement is proposed in this study. Here, the strain field of the minimum cross-section in the necking region of the specimen is obtained using a DIC (digital image correlation) measurement technique, and the average axial true stress-strain curve is calculated. Then, the average axial true stress-strain curve is modified using the modified Bridgeman formula. Taking 7075 aluminum alloy as an example, the high temperature equivalent stress-strain curve considering the diffuse necking stage is obtained. Compared with the traditional method, the maximum effective strain range is expanded from 0.05 to 0.8 due to the consideration of the necking stage. The obtained curve is characterized by a coupled viscoplastic-damage constitutive model and embedded in ABAQUS through the user subroutine VUMAT to simulate the hot tensile process. The relative error of force-displacement between the simulation and the experiment was 2.4%, validating the ability of the presented method. This study provides theoretical guidance and a scientific basis for the application and forming control of hot stamping processes.

12.
Materials (Basel) ; 15(7)2022 Apr 02.
Artigo em Inglês | MEDLINE | ID: mdl-35407965

RESUMO

A rolled plate of 7075 aluminum alloy was friction-stir-processed (FSP) with simultaneous cooling by an air stream cooled to -11 °C with a jet cooling nozzle. Two variants of air blowing were used: at an angle of 45° to the sample surface and at an angle of 90°. The reference material was a sample subjected to analogous treatment but naturally cooled in still air. The microstructural tests revealed strong grain refinement in all the samples, with higher grain refinement obtained in the air-cooled friction-stir-processed samples. For the naturally cooled samples, the average grain size in the near-surface area was 7.6 µm, while for the air-cooled sample, it was 1.4 µm for the 45° airflow variant and 3.2 µm for the 90° airflow variant. A consequence of the greater grain refinement was that the hardness of the air-cooled friction-stir-processed samples was higher than that of the naturally cooled samples. The improvement in abrasive wear resistance was achieved only in the case of the friction-stir-processed specimens with air cooling. It was found that the change in the air blowing angle affects not only the degree of grain refinement in the stirring zone, but also the geometrical structure of the surface. In all the samples, FSP caused redistribution of the intermetallic precipitates combined with their partial dissolution in the matrix.

13.
Materials (Basel) ; 15(12)2022 Jun 20.
Artigo em Inglês | MEDLINE | ID: mdl-35744404

RESUMO

In this paper, the corrosion resistance and mechanical properties of the 7075 aluminum alloy are studied. The alloy was deformed by hydrostatic extrusion and then aged both naturally and artificially. Results are compared with those of coarse-grained material subjected to T6 heat treatment. The aim of the research is to find the optimal correlation between the mechanical properties and the corrosion resistance of the alloy. To this end, static tensile tests with subsequent fractography, open circuit potential, and potentiodynamic polarization tests in 0.05 M NaCl were conducted. Obtained results show that a combination of precipitate hardening and a deformed microstructure leads to increased mechanical strength with high anisotropy due to the presence of fibrous grains. Plastic deformation increases susceptibility to corrosion due to the increased number of grain boundaries, which act as paths along that corrosion propagates. However, further artificial aging incurs a positive effect on corrosion resistance due to changes in the chemical composition of the matrix as a result of the precipitation process.

14.
Materials (Basel) ; 14(19)2021 Sep 22.
Artigo em Inglês | MEDLINE | ID: mdl-34639883

RESUMO

The stress strain curve of 7075 aluminum alloy in the temperature range of 310 °C to 410 °C was obtained by Gleeble-3800. By Nakazima test, the isothermal thermoforming limit diagrams of 7075 aluminum alloy at different deformation temperatures and stamping speeds were acquired. Moreover, the parameters of automotive S-rail hot stamping process were optimized by GA-BP neural network. The results show that the forming limit curve of 7075 aluminum alloy increases as the deformation temperature and stamping speed increase. The predicted optimal parameters for hot stamping of automotive S-rails by GA-BP neural network are: stamping speed is 50 mm/s, friction coefficient between die and blank is 0.1, and blank holder force is 5 kN. The maximum thinning rate at this process parameter is 9.37%, which provided a reference for 7075 aluminum alloy automotive S-rail hot stamping.

15.
Materials (Basel) ; 14(11)2021 May 22.
Artigo em Inglês | MEDLINE | ID: mdl-34067372

RESUMO

To improve the loose structure and serious porosity of (Al-Zn-Mg-Cu) 7075 aluminum alloy laser-welded joints, aging treatment, double-sided ultrasonic impact treatment (DSUIT), and a combination of aging and DSUIT (A-DSUIT) were used to treat joints. In this experiment, the mechanism of A-DSUIT on the microstructure and properties of welded joints was analyzed. The microstructure of the welded joints was observed using optical microscopy, scanning electron microscopy, and electron backscatter diffraction (EBSD). The hardness and tensile properties of the welded components under the different processes were examined via Vickers hardness test and a universal tensile testing machine. The results showed that, after the aging treatment, the dendritic structure of the welded joints transformed into an equiaxed crystal structure. Moreover, the residual tensile stress generated in the welding process was weakened, and the hardness and tensile strength were significantly improved. After DSUIT, a plastic deformation layer of a certain thickness was generated from the surface downward, and the residual compressive stress was introduced to a certain depth of the joint. However, the weld zone unaffected by DSUIT still exhibited residual tensile stress. The inner microhardness of the joint surface improved; the impact surface hardness was the largest and gradually decreased inward to the weld zone base metal hardness, with a small improvement in the tensile strength. Compared with the single treatment process, the microstructural and mechanical properties of the welded joint after A-DSUIT were comprehensively improved. The microhardness and tensile strength of the welded joint reached 200 HV and 615 MPa, respectively, for an increase of 45.8% and 61.8%, respectively. Observation of the fractures of the tensile specimens under the different treatment processes showed that the fractures before the aging treatment were mainly ductile fractures while those after were mainly brittle fractures. After DSUIT of the welded joints, a clear and dense plastic deformation layer was observed in the fracture of the tensile specimens and effectively improved the tensile properties of the welded joints. Under the EBSD characterization, the larger the residual compressive stress near the ultrasonic impact surface, the smaller the grain diameter and misorientation angle, and the lower the texture strength. Finally, after A-DSUIT, the hardness and tensile properties improved the most.

16.
Materials (Basel) ; 14(6)2021 Mar 20.
Artigo em Inglês | MEDLINE | ID: mdl-33804797

RESUMO

The deformation and fracture mechanism in 7075 aluminum alloy is discussed based on a field theoretical approach. A pair of peak-aged and overaged plate specimens are prepared under the respective precipitation conditions, and their plastic deformation behaviors are visualized with two-dimensional electronic speckle pattern interferometry (ESPI). The in-plane velocity field caused by monotonic tensile loading is monitored continuously via the contour analysis method of ESPI. In the plastic regime, the peak-aged specimen exhibits a macroscopically uniform deformation behavior, while the annealed specimen exhibits non-uniform deformation characterized by a localized shear band. The occurrence of the shear band is explained by the transition of the material's elastic resistive mechanism from the longitudinal force dominant to shear force dominant mode. The shear force is interpreted as the frictional force that drives mobile dislocations along the shear band. The dynamic behavior of the shear band is explained as representing the motion of a solitary wave. The observed decrease in the solitary wave's velocity is accounted for by the change in the acoustic impedance with the advancement of plastic deformation.

17.
Materials (Basel) ; 13(18)2020 Sep 15.
Artigo em Inglês | MEDLINE | ID: mdl-32942777

RESUMO

Direct soldering of the aluminum alloy 7075 is very difficult or even impossible. In order to make it possible, galvanic coatings and the procedures for their application on alloy surfaces were developed. The paper presents structures and mechanical properties of soldered joints of the 7075 alloy, made in indirect way with use of electrolytically deposited Ni-P and Cu-Cr coatings. Application of the newly developed Ni-P and Cu-Cr coatings on base surfaces of the 7075 alloy is described. The results of wettability examination of the S-Sn97Cu3 solder in the droplet test and by spreading on the coatings applied on the 7075 substrates are presented. The wettability angle of both coatings was lower than 30°. The results of metallographic examinations with use of light and electron microscopy are presented. It was shown that adhesion of metallic coatings to the aluminum alloy is good, exceeding shear strength of the S-Sn97Cu3 solder. Shear strength of soldered joint was equal to 35 ± 3 MPa. Measured hardness of the Ni-P interlayer reached high value of 471 HV 0.025.

18.
Materials (Basel) ; 13(18)2020 Sep 21.
Artigo em Inglês | MEDLINE | ID: mdl-32967311

RESUMO

The corrosion fatigue properties and fracture characteristics of friction stir welding joints of 7075 aluminum alloys were studied via corrosion fatigue tests, electrochemical measurements, and corrosion fatigue morphology and microstructure observations. The results show that the corrosion fatigue crack of the friction stir welding (FSW) joint of 7075 aluminum alloys originated in the junction zone between the thermomechanically affected zone and the weld nugget zone. The corrosion fatigue life of the joint decreased with increasing stress amplitude, with an S-N curve equation of lgN = 5.845 - 0.014S. Multiple crack sources were observed in the corrosion fatigue fracture. The main crack source originated from the corrosion pits at the interface between the thermomechanically affected zone and the weld nugget zone due to the influence of the coarse microstructure and the large potential difference between both zones. Corrosion morphologies of a rock candy block and an ant nest appeared in the crack propagation zone and the grain boundary of the weld nugget zone. In addition, fatigue speckles and intergranular fractures were observed, as well as brittle fracture characterized by cleavage steps and secondary cracks in the final fracture zone.

19.
Materials (Basel) ; 13(5)2020 Mar 06.
Artigo em Inglês | MEDLINE | ID: mdl-32155731

RESUMO

When hot forging 7075 aluminum alloy, as a military material durable enough for most of its applications, it needs to be heat-treated to ensure the target material property achieves the application requirements. However, the material properties change because of heat throughout usage. In this study, a new approach was devised to heat treat the alloy to prevent material property changes. The study further clarified the effect of rapid heat treatment on the high-temperature resistance of a hot forging 7075 aluminum alloy. Infrared (IR) heat treatment was used as a rapid heating technique to effectively replace the conventional resistance heat (RH) treatment method. Our experimental result showed that IR heat treatment resulted in better age hardening at the initial aging stage, where its tensile strength and elongation appeared like that of a resistance heat treatment. More so, based on hardness and tensile test results, the IR-heated treatment process inhibited the phase transformation of precipitations at a higher temperature, improving high-temperature softening resistance and enhancing the thermal stability of the hot forging 7075 aluminum alloy.

20.
Materials (Basel) ; 12(17)2019 Aug 26.
Artigo em Inglês | MEDLINE | ID: mdl-31455008

RESUMO

Simulation of the material failure under high strain rate conditions is one of the most difficult problems in the finite element analyses, and many researchers have tried to understand and reproduce dynamic material fracture. In this study, we investigate a failure criterion that minimizes the mesh dependency at high strain rates and incorporates the criterion into the Johnson-Cook constitutive relationship by developing a user-defined material model. Impact tests were performed using a gas-gun system in order to investigate the response of the 7075-T651 aluminum plate in high-speed collision. On the other hand, numerical simulations are carried out by considering various element sizes and the relationship between element size and failure strain is inversely obtained using numerical results. By accommodating the relationship into the damage model and implementing in the user-defined material model, mesh dependency is significantly reduced, and sufficient accuracy is achieved with alleviated computational cost than the existing damage model. This study suggests an element size-dependent damage criterion that is applicable for impact simulation and it is expected that the criterion is useful to obtain accurate impact responses with a small computational cost.

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