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Anodic C(sp3)-H Acyloxylation of Indolin-3-ones Enabled by Oxidant-Free Cross-Dehydrogenative C(sp3)-O Coupling.
Zou, Canlin; Wu, Hongting; He, Jiangtao; Hu, Yunfei; Deng, Weijie; Li, Xinling; Hu, Jinhui; Li, Yibiao; Huang, Yubing.
  • Zou C; School of Biotechnology and Health Sciences, Wuyi University, Jiangmen 529090, P. R. China.
  • Wu H; School of Biotechnology and Health Sciences, Wuyi University, Jiangmen 529090, P. R. China.
  • He J; School of Biotechnology and Health Sciences, Wuyi University, Jiangmen 529090, P. R. China.
  • Hu Y; School of Biotechnology and Health Sciences, Wuyi University, Jiangmen 529090, P. R. China.
  • Deng W; School of Biotechnology and Health Sciences, Wuyi University, Jiangmen 529090, P. R. China.
  • Li X; School of Biotechnology and Health Sciences, Wuyi University, Jiangmen 529090, P. R. China.
  • Hu J; School of Biotechnology and Health Sciences, Wuyi University, Jiangmen 529090, P. R. China.
  • Li Y; School of Biotechnology and Health Sciences, Wuyi University, Jiangmen 529090, P. R. China.
  • Huang Y; School of Biotechnology and Health Sciences, Wuyi University, Jiangmen 529090, P. R. China.
J Org Chem ; 87(2): 1335-1347, 2022 01 21.
Article en En | MEDLINE | ID: mdl-34985264
ABSTRACT
An efficient anodic C(sp3)-H acyloxylation protocol has been established via intermolecular cross-dehydrogenative C(sp3)-O coupling. The protocol provides various C2-acyloxy indolin-3-ones without the addition of metal catalysts and external oxidants because indolin-3-ones can be directly oxidized at the anode. The effective application of several medical drugs and the realization of the gram-scale experiment have proven the practicality of this protocol.
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Texto completo: 1 Banco de datos: MEDLINE Asunto principal: Oxidantes Tipo de estudio: Guideline Idioma: En Año: 2022 Tipo del documento: Article
Texto completo
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PubMed Links
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Texto completo: 1 Banco de datos: MEDLINE Asunto principal: Oxidantes Tipo de estudio: Guideline Idioma: En Año: 2022 Tipo del documento: Article