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Construction of Phenanthridinone Skeletons through Palladium-Catalyzed Annulation.
Geng, Xin; He, Heng; Shatskiy, Andrey; Stepanova, Elena V; Alvey, Gregory R; Liu, Jian-Quan; Kärkäs, Markus D; Wang, Xiang-Shan.
  • Geng X; School of Chemistry and Materials Science, Jiangsu Key Laboratory of Green Synthesis for Functional Materials Jiangsu Normal University, Xuzhou, Jiangsu 221116, China.
  • He H; School of Chemistry and Materials Science, Jiangsu Key Laboratory of Green Synthesis for Functional Materials Jiangsu Normal University, Xuzhou, Jiangsu 221116, China.
  • Shatskiy A; Department of Chemistry, KTH Royal Institute of Technology, SE-100 44 Stockholm, Sweden.
  • Stepanova EV; Department of Chemistry, KTH Royal Institute of Technology, SE-100 44 Stockholm, Sweden.
  • Alvey GR; Tomsk Polytechnic University, Lenin Avenue 30, 634050 Tomsk, Russia.
  • Liu JQ; Department of Chemistry, KTH Royal Institute of Technology, SE-100 44 Stockholm, Sweden.
  • Kärkäs MD; School of Chemistry and Materials Science, Jiangsu Key Laboratory of Green Synthesis for Functional Materials Jiangsu Normal University, Xuzhou, Jiangsu 221116, China.
  • Wang XS; Department of Chemistry, KTH Royal Institute of Technology, SE-100 44 Stockholm, Sweden.
J Org Chem ; 88(17): 12738-12743, 2023 Sep 01.
Article en En | MEDLINE | ID: mdl-37611263
Herein, a straightforward synthetic approach for the construction of phenanthridin-6(5H)-one skeletons is disclosed. The developed protocol relies on palladium catalysis, providing controlled access to a range of functionalized phenanthridin-6(5H)-ones in 59-88% yields. Furthermore, plausible reaction pathways are proposed based on mechanistic experiments.
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Texto completo: 1 Banco de datos: MEDLINE Idioma: En Año: 2023 Tipo del documento: Article
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Texto completo: 1 Banco de datos: MEDLINE Idioma: En Año: 2023 Tipo del documento: Article