Assigning the configuration of amino alcohols by NMR: a single derivatization method.
Org Lett
; 10(13): 2733-6, 2008 Jul 03.
Article
em En
| MEDLINE
| ID: mdl-18522389
ABSTRACT
The chirality of sec/prim- and prim/sec-1,2-amino alcohols can be determined by (1)H NMR of just one MPA derivative--either (R) or (S)--by comparison of two spectra at different temperatures and analysis of the evolution of the easily observable singles of the CalphaH signals.
Texto completo:
1
Base de dados:
MEDLINE
Assunto principal:
Espectroscopia de Ressonância Magnética
/
Amino Álcoois
Idioma:
En
Ano de publicação:
2008
Tipo de documento:
Article