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Transition-Metal-Free Upscaling of 2,5-Furandicarboxylic Acid Synthesis and Investigation of the Reaction Mechanism.
Lee, Tae Woo; Lee, Won Jung; Kim, Young Sug; Do, Taeyang; Choi, Ji-Eun; Han, Young Kwang; Oh, Chunrim; Lee, Chi-Wan; Yum, Eul Kgun; Yang, Jung Woon.
Afiliação
  • Lee TW; Department of Energy Science, Sungkyunkwan University, Suwon, 16419, South Korea.
  • Lee WJ; Chemical Research Center, Samyang Corp., Daejeon, 34055, South Korea.
  • Kim YS; Department of Chemistry, Chungnam National University, Daejeon, 34134, South Korea.
  • Do T; Department of Energy Science, Sungkyunkwan University, Suwon, 16419, South Korea.
  • Choi JE; Department of Energy Science, Sungkyunkwan University, Suwon, 16419, South Korea.
  • Han YK; Chemical Research Center, Samyang Corp., Daejeon, 34055, South Korea.
  • Oh C; Department of Energy Science, Sungkyunkwan University, Suwon, 16419, South Korea.
  • Lee CW; Chemical Research Center, Samyang Corp., Daejeon, 34055, South Korea.
  • Yum EK; Chemical Research Center, Samyang Corp., Daejeon, 34055, South Korea.
  • Yang JW; Department of Chemistry, Chungnam National University, Daejeon, 34134, South Korea.
Chemistry ; 29(36): e202300903, 2023 Jun 27.
Article em En | MEDLINE | ID: mdl-37060216
ABSTRACT
An environmentally friendly oxidation system has proposed for the practical and scalable production of value-added 2,5-furandicarboxylic acid from 1 kg of 5-hydroxymethylfurfural. The system is composed of a simple base, oxygen, and a green solvent, thereby providing a sustainable and economical approach to organic synthesis. To gain insight into the mechanism of this oxidation process, NMR spectroscopic analysis and kinetic study are used for the mechanistic investigation of this environmentally friendly oxidation process.
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Texto completo: 1 Base de dados: MEDLINE Idioma: En Ano de publicação: 2023 Tipo de documento: Article
Texto completo
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PubMed Links
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Texto completo: 1 Base de dados: MEDLINE Idioma: En Ano de publicação: 2023 Tipo de documento: Article