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Iron-catalyzed alkoxyl radical-mediated C-C bond cleavage/phosphorothiolation: a new approach to functionalized S-alkyl phosphorothioates.
Bai, Ming; Liu, Shuai; Xin, Hong; Yang, Xu; Duan, Xin-Hua; Guo, Li-Na.
Afiliação
  • Bai M; Department of Chemistry, School of Chemistry, Xi'an Key Laboratory of Sustainable Energy Material Chemistry and Engineering Research Center of Energy Storage Materials and Devices, Ministry of Education, Xi'an Jiaotong University, Xi'an 710049, P. R. China. guoln81@xjtu.edu.cn.
  • Liu S; Department of Chemistry, School of Chemistry, Xi'an Key Laboratory of Sustainable Energy Material Chemistry and Engineering Research Center of Energy Storage Materials and Devices, Ministry of Education, Xi'an Jiaotong University, Xi'an 710049, P. R. China. guoln81@xjtu.edu.cn.
  • Xin H; Department of Chemistry, School of Chemistry, Xi'an Key Laboratory of Sustainable Energy Material Chemistry and Engineering Research Center of Energy Storage Materials and Devices, Ministry of Education, Xi'an Jiaotong University, Xi'an 710049, P. R. China. guoln81@xjtu.edu.cn.
  • Yang X; School of Electrical Engineering, Xi'an Jiaotong University, Xi'an, 710049, P. R. China.
  • Duan XH; Department of Chemistry, School of Chemistry, Xi'an Key Laboratory of Sustainable Energy Material Chemistry and Engineering Research Center of Energy Storage Materials and Devices, Ministry of Education, Xi'an Jiaotong University, Xi'an 710049, P. R. China. guoln81@xjtu.edu.cn.
  • Guo LN; School of Electrical Engineering, Xi'an Jiaotong University, Xi'an, 710049, P. R. China.
Org Biomol Chem ; 21(28): 5855-5860, 2023 Jul 19.
Article em En | MEDLINE | ID: mdl-37401815
An efficient iron-catalyzed alkoxyl radical-mediated C-C bond cleavage/phosphorothiolation cascade is presented. This protocol features mild and redox neutral conditions, wide substrate scope and easy scalability, allowing straightforward access to functionalized S-alkyl organophosphorus compounds in moderate to good yields.
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Texto completo: 1 Base de dados: MEDLINE Idioma: En Ano de publicação: 2023 Tipo de documento: Article
Texto completo
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Texto completo: 1 Base de dados: MEDLINE Idioma: En Ano de publicação: 2023 Tipo de documento: Article