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Synthesis of isothiocyanato alkyl sulfides from alkenes using KSCN and DMTSM.
Jiang, Shixuan; Zhuang, Daijiao; Liu, Peihua; Xu, Qiyang; Luo, Xiaofeng; Wang, Tianqiang; Zhang, Chengcheng; Yan, Rulong.
Afiliação
  • Jiang S; State Key Laboratory of Applied Organic Chemistry, College of Chemistry and Chemical Engineering, Lanzhou University, Lanzhou 73000, Gansu, China. yanrl@lzu.edu.cn.
  • Zhuang D; State Key Laboratory of Applied Organic Chemistry, College of Chemistry and Chemical Engineering, Lanzhou University, Lanzhou 73000, Gansu, China. yanrl@lzu.edu.cn.
  • Liu P; Research Institute of Oil and Gas Technology of Changqing Oilfield Company, Xian 710018, Shanxi, China.
  • Xu Q; State Key Laboratory of Applied Organic Chemistry, College of Chemistry and Chemical Engineering, Lanzhou University, Lanzhou 73000, Gansu, China. yanrl@lzu.edu.cn.
  • Luo X; Chengdu Guibao Science and Technology Co., Ltd, Chengdu 610041, Sichuan, China.
  • Wang T; Chengdu Guibao Science and Technology Co., Ltd, Chengdu 610041, Sichuan, China.
  • Zhang C; State Key Laboratory of Applied Organic Chemistry, College of Chemistry and Chemical Engineering, Lanzhou University, Lanzhou 73000, Gansu, China. yanrl@lzu.edu.cn.
  • Yan R; State Key Laboratory of Applied Organic Chemistry, College of Chemistry and Chemical Engineering, Lanzhou University, Lanzhou 73000, Gansu, China. yanrl@lzu.edu.cn.
Org Biomol Chem ; 22(22): 4472-4477, 2024 Jun 05.
Article em En | MEDLINE | ID: mdl-38775306
ABSTRACT
A method for the synthesis of isothiocyanato alkyl sulfides from KSCN and DMTSM under metal-free conditions has been developed. The features of this reaction are low-cost, readily accessible starting materials and the use of KSCN as nucleophiles for C-NCS bond formation. Alkenes with various substituted groups react smoothly and the desired products are obtained in moderate to good yields.
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Texto completo: 1 Base de dados: MEDLINE Idioma: En Ano de publicação: 2024 Tipo de documento: Article
Texto completo
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PubMed Links
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Texto completo: 1 Base de dados: MEDLINE Idioma: En Ano de publicação: 2024 Tipo de documento: Article